Nickel based superalloy with high volume fraction of precipitate phase
A process includes solution heat treating a nickel based superalloy with greater than about 40% by volume of gamma prime precipitate to dissolve the gamma prime precipitate in the nickel based superalloy; cooling the nickel based superalloy to about 85% of a solution temperature measured on an absolute scale to coarsen the gamma prime precipitate such that a precipitate structure is greater than about 0.7 micron size; and wrought processing the nickel based superalloy at a temperature below a recrystallization temperature of the nickel based superalloy. A material includes a nickel based superalloy with greater than about 40% by volume of gamma prime precipitate in which the precipitate structure is greater than about 0.7 micron size.
1. A process, comprising:
solution heat treating a nickel based superalloy with greater than about 40% by volume of gamma prime precipitate to dissolve the gamma prime precipitate in the nickel based superalloy;
cooling the nickel based superalloy to about 85% of a solution temperature measured on an absolute scale to coarsen the gamma prime precipitate such that a precipitate structure is greater than about 0.7 micron size; and
wrought processing the nickel based superalloy at a temperature below a recrystallization temperature of the nickel based superalloy.
2. The process as recited in claim 1 , wherein the nickel based superalloy includes at least 50% by volume of gamma prime precipitate.
3. The process as recited in claim 1 , wherein the cooling is performed at a rate slower than about 10° F./minute.
4. The process as recited in claim 1 , wherein the cooling is a rapid cooling, then the temperature held for a period of time until the precipitate structure is greater than about 0.7 micron size.
5. The process as recited in claim 1 , wherein the wrought processing includes at least one of swaging, rolling, ring-rolling, forging, extruding, and shape forming operations.
6. The process as recited in claim 1 , further comprising annealing intermittently at temperatures no higher than the recrystallization temperature subsequent to the wrought processing to partially recover dislocation structure.
7. The process as recited in claim 6 , wherein the recrystallization temperature has an upper limit of about 90% of a solution temperature measured on an absolute scale.
8. The process as recited in claim 1 , further comprising heat treating at temperatures no higher than the recrystallization temperature subsequent to the wrought processing.
9. The process as recited in claim 8 , wherein the recrystallization temperature has an upper limit of about 90% of a solution temperature measured on an absolute scale.
10. The process as recited in claim 1 , wherein no additional precipitation is performed to the nickel based superalloy subsequent to the wrought processing.
11. The process as recited in claim 1 , wherein no additional heat treating is performed to the nickel based superalloy subsequent to the wrought processing.
12. The process as recited in claim 1 , wherein the nickel based superalloy is subjected to a solution heat treatment and slow cooled.
13. The process as recited in claim 1 , wherein the nickel based superalloy is subjected to a sub-solution temperature annealing cycle.
14. The process as recited in claim 1 , wherein the nickel based superalloy is subjected to isothermal over-aging.