High density grids
View Patent ↗An X-ray data collection grid device is provided that includes a magnetic base that is compatible with robotic sample mounting systems used at synchrotron beamlines, a grid element fixedly attached to the magnetic base, where the grid element includes at least one sealable sample window disposed through a planar synchrotron-compatible material, where the planar synchrotron-compatible material includes at least one automated X-ray positioning and fluid handling robot fiducial mark.
1. An X-ray data collection grid device, comprising:
a. a magnetic base, wherein said magnetic base is compatible with robotic sample mounting systems used at synchrotron beamlines;
b. a grid element fixedly attached to said magnetic base, wherein said grid element comprising a planar synchrotron-compatible material, wherein said grid element comprises at least one sealable sample window disposed through said planar synchrotron-compatible material, wherein said planar synchrotron-compatible material comprises at least one automated X-ray positioning and fluid handling robot fiducial mark.
2. The X-ray data collection grid device of claim 1 , wherein said magnetic base comprises a shape that is compatible with sample goniometers disposed at synchrotron beam lines and is compatible with automated sample-pin exchange robotic systems.
3. The X-ray data collection grid device of claim 2 , wherein said magnetic base is compatible with an ALS puck, a uni-puck, an MSC magazine, or an SSRL cassette.
4. The X-ray data collection grid device of claim 2 , wherein said automated sample-pin exchange robotic systems comprise SSRL Automated Mounter, ALS Sample Exchange Robot, ACTOR, or a CATs robotic system.
5. The X-ray data collection grid device of claim 1 , wherein said planar synchrotron-compatible material comprises polycarbonate, acrylonitrile butadiene styrene, cyclic olefin copolymer or other polymer material.
6. The X-ray data collection grid device of claim 1 , wherein said at least one sealable sample window comprises a single window, an array of sample holes, or an array of windows, wherein said array of sample holes or said array of windows comprise a diameter in a range of 50 μm to 2.5 mm.
7. The X-ray data collection grid device of claim 1 , wherein said at least one automated X-ray positioning and fluid handling robot fiducial mark comprises a hole, a mark, a dimple, a corner or an edge of said planar synchrotron-compatible material.
8. The X-ray data collection grid device of claim 7 , wherein said hole has a diameter in a range of 5 μm to 300 μm.
9. The X-ray data collection grid device of claim 1 , wherein said planar synchrotron-compatible material comprises a thickness in a range of 25 μm to 300 μm.
10. The X-ray data collection grid device of claim 1 , wherein said at least one sealable sample window comprises a transparent sheet selected from the group consisting of graphene, holey carbon, mylar, polyamide, polyimide film with silicone adhesive, and polymers.
11. The X-ray data collection grid device of claim 10 , wherein said transparent sheet comprises a thickness in a range of 100 nm to 20 μm.