IP Library Granted Patent US 10,003,059
Granted Patent B2
US 10,003,059 · App. 14/882,127 · Granted Jun 19, 2018

Ion conductive inks and solutions for additive manufacturing of lithium microbatteries

Inventors: Eric B. Duoss (Dublin, CA); Patrick G. Campbell (Oakland, CA); William C. Floyd, III (Oakland, CA); Julie A. Jackson (Livermore, CA); Matthew Merrill (Dublin, CA); Conner T. Sharpe (Tracy, CA); Christopher M. Spadaccini (Oakland, CA); Michael Stadermann (Pleasanton, CA); Cheng Zhu (Livermore, CA)
Assignee: Lawrence Livermore National Security, LLC
H01M2/1653C09D11/00H01M2/145H01M2/1673H01M2/18H01M6/40H01M10/0436H01M10/0525H01M2220/30
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,003,059
App. No.
14/882,127
Granted
Jun 19, 2018
Kind
B2
Abstract

A separator made of ion conductive ink is produced by additive manufacturing. A micro-battery is produced with the separator made of ion conductive ink located between the battery's anode and cathode. The separator functions to keep the anode and cathode apart and to facilitate the transport of ions to produce an operative micro-battery.

Claims (19)

1. A method of making a micro-battery, comprising the steps of:

creating a three dimensional model of a micro-battery separator, wherein said three dimensional model of a micro-battery separator has sides, a top, and a bottom, and comprises anode micro-channels extending from said top to said sides and cathode micro-channels extended from said bottom to said sides;

using said three dimensional model of a micro-battery separator to produce a micro-battery separator by additive manufacturing, wherein said additive manufacturing uses ion conductive ink to produce said micro-battery separator, and wherein said micro-battery separator has sides, a top, and a bottom, and comprises anode micro-channels extending from said top to said sides and cathode micro-channels extended from said bottom to said sides;

creating a seal for the micro-battery by adding a material that seals said sides of said micro-battery separator leaving said top and said bottom unsealed;

positioning a top electrical conductive plate on said top of said micro-battery separator;

adding a top electrode connected to said top electrical conductive plate;

positioning a bottom electrical conductive plate on said bottom of said micro-battery separator;

adding a bottom electrode connected to said bottom electrical conductive plate;

filling said anode micro-channels in said micro-battery separator with anode material;

filling said cathode micro-channels in said micro-battery separator with cathode material; and

adding an outer casing.

2. The method of making a micro-battery of claim 1 , wherein said additive manufacturing is projection micro-stereolithography.

3. The method of making a micro-battery of claim 1 , wherein said additive manufacturing is 3D printing.

4. The method of making a micro-battery of claim 1 , wherein said ion conductive ink is Lithium Bis(trifluoromethane)sulfonimide, LiTFSI) and tetraglyme solvent.

5. The method of making a micro-battery of claim 1 , wherein said ion conductive ink is methacrylpropylsulfate (MPS) salts and PEGDA.

6. The method of making a micro-battery of claim 1 , wherein said ion conductive ink is methacrylpropylsulfate salts and PEGDA/PEGMA having a

chemical structure.

7. The method of making a micro-battery of claim 1 , wherein said micro-battery separator has a matrix of anode micro-channels and a matrix of cathode micro-channels wherein said matrix of anode micro-channels and said matrix of cathode micro-channels do not interconnect and form self-contained matrices for said anode material in said anode micro-channels and said cathode material in said cathode micro-channels.

8. The method of making a micro-battery of claim 7 , wherein said matrix of anode micro-channels and said matrix of cathode micro-channels are interwoven to provide an interpenetrating network.

Assignments (2)
CONFIRMATORY LICENSE Recorded May 9, 2018
From: LAWRENCE LIVERMORE NATIONAL SECURITY, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 045751/0019 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 13, 2015
From: DUOSS, ERIC B.; CAMPBELL, PATRICK G.; FLOYD, WILLIAM C., III; JACKSON, JULIE A.; MERRILL, MATTHEW; SHARPE, CONNER T.; SPADACCINI, CHRISTOPHER M.; STADERMANN, MICHAEL; ZHU, CHENG
To: LAWRENCE LIVERMORE NATIONAL SECURITY, LLC.
Reel/Frame 036785/0052 →
Continuity (1)
Related Publication 20170104198A1 · Apr 13, 2017