IP Library Granted Patent US 10,039,311
Granted Patent B2
US 10,039,311 · App. 14/884,914 · Granted Aug 7, 2018

Tobacco extract for non-combustible smoking devices

Inventors: Donald J. Muehlbauer (West Bend, WI); Ryan Jenson (Waukesha, WI); S. Anthony Pace (Delafield, WI)
Assignee: Securience, LLC
A24B15/26A24F47/008
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,039,311
App. No.
14/884,914
Granted
Aug 7, 2018
Kind
B2
Abstract

Systems and methods for manufacturing and vaporizing a tobacco extract for use in a non-combustible smoking device are described. These methods include a solution having a volume of a liquid tobacco extract suspended in a hygroscopic liquid glycerol solvent. The systems and methods provide advantages in that the method is substantially free of water and results in an improved tobacco flavor extract.

Claims (32)

1. A method for manufacturing a liquid tobacco extract configured for vaporization in a non-combustible smoking device, the method comprising the steps of:

combining a predetermined mass of ground tobacco in a predetermined mass of a hygroscopic liquid glycerol solvent to form a mixture;

increasing the temperature of the mixture from a first temperature to an elevated second temperature, the second temperature being approximately 250 degrees Fahrenheit;

maintaining the mixture at the elevated second temperature for a predetermined period of time of between 100 and 150 minutes to a form a solution having a volume of a liquid tobacco extract suspended in the liquid glycerol solvent;

filtering the mixture to remove the ground tobacco from the solution of the liquid tobacco extract suspended in the solvent having a percentage nicotine of approximately 0.05, a pH of approximately 5.5, and a volume of tobacco specific a nitrosamines of less than 100 nanograms per 35 puffs; and

lowering the temperature of the solution from the second temperature to the first temperature.

2. The method of claim 1 , further comprising the step of pressing the ground tobacco after filtered to remove additional solution therefrom.

3. The method of claim 1 , wherein the predetermined period of time is approximately 120 minutes.

4. The method of claim 1 , wherein a ratio of the hygroscopic liquid glycerol solvent to ground tobacco is approximately 20:1.

5. The method of claim 1 , wherein the predetermined mass of hygroscopic liquid glycerol solvent is approximately 20 times greater than the predetermined mass of ground tobacco.

6. The method of claim 1 , wherein the hygroscopic liquid glycerol solvent is approximately a vegetable glycerol.

7. The method of claim 1 , further comprising the step of adding a predetermined mass of a solvent to the solution to form a liquid tobacco extract having a final percentage nicotine of approximately 0.05%.

8. The method of claim 1 , further comprising the step of adding a predetermined mass of a nicotine extract to the solution to form a liquid tobacco extract having a final percentage nicotine of approximately between 1% and 3%.

9. The method of claim 1 , further comprising the step of adding a predetermined mass of a non-tobacco flavor additive to the solution.

10. The method of claim 1 , wherein the solution is substantially free of water.

11. The method of claim 1 , wherein the first mixture is filtered at a pressure of greater than 1,500 KPa.

12. The method of claim 1 , wherein the solution is substantially free of solid particulates.

13. The method of claim 1 , wherein the solution has an absorbance of between 0.4 AU and 0.6 AU when exposed to a 500 nm wavelength light.

14. A method for vaporizing a liquid tobacco extract configured in a non-combustible smoking device, the method comprising the steps of:

combining a predetermined mass of ground tobacco in a predetermined mass of a hygroscopic liquid glycerol solvent to form a mixture;

increasing the temperature of the mixture from a first temperature to an elevated second temperature, the second temperature being approximately 250 degrees Fahrenheit;

maintaining the mixture at the elevated second temperature for a predetermined period of time of between 100 and 150 minutes to a form a solution having a volume of a liquid tobacco extract suspended in the liquid glycerol solvent;

filtering the mixture to remove the ground tobacco from the solution of the liquid tobacco extract suspended in the solvent having a percentage nicotine of approximately 0.05%, a pH of approximately 5.5, and a volume of tobacco specific a nitrosaimines of less than 100 nanograms per 35 puffs;

lowering the temperature of the solution from the second temperature to the first temperature;

placing a volume of the solution into a cartridge within the non-combustible smoking device adjacent a wicking material;

drawing the solution into the wicking material; and

vaporizing the solution in the wicking material by passing an electrical current through an atomizer.

15. The method of claim 14 , wherein the atomizer is a wire located around at least a portion of the wicking material.

16. The method of claim 15 , wherein the wire has an electrical resistance that causes the temperature of the solution in the wicking material to rise to a third temperature that is at least equal to a vaporization temperature of the solution.

17. The method of claim 14 , further comprising the step of adding a predetermined mass of a nicotine extract to the solution to form a liquid tobacco extract having a final percentage nicotine of approximately between 1% and 3% prior to placing the volume of the solution into a cartridge within the electronic cigarette adjacent the wicking material.

18. The method of claim 14 , further comprising the step of adding a predetermined mass of a non-tobacco flavor additive to the solution prior to placing the volume of the solution into a cartridge within the electronic cigarette adjacent the wicking material.

19. The method of claim 14 , wherein the solution has an absorbance of between 0.4 AU and 0.6 AU when exposed to a 500 nm wavelength light.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 18, 2021
From: SECURIENCE, LLC
To: VAPINUSA-WI, LLC
Reel/Frame 056587/0584 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 16, 2015
From: MUEHLBAUER, DONALD J.; JENSON, RYAN; PACE, S. ANTHONY
To: SECURIENCE, LLC
Reel/Frame 036807/0773 →
Continuity (2)
Provisional Application 62065285 · Oct 17, 2014
Related Publication 20160106144A1 · Apr 21, 2016
Cited By (1)
US 12,628,862