IP Library Granted Patent US 10,604,871
Granted Patent B2
US 10,604,871 · App. 14/900,459 · Granted Mar 31, 2020

Process for steam drawing carbon-fiber precursor acrylic fiber bundle

Inventors: Akishige Tada (Otake, JP); Yukihiro Mizutori (Otake, JP)
Assignee: Mitsubishi Chemical Corporation
D02J1/222B29C55/005D01D11/02D01F6/38D01F9/21D01F9/22D02J1/18D02J1/225D02J13/005B29K2033/08B29L2031/731D01D5/16D01F6/18D01F9/225D06B3/045D06C3/00
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Quick Facts
Patent No.
US 10,604,871
App. No.
14/900,459
Granted
Mar 31, 2020
Kind
B2
Abstract

This process for manufacturing a carbon-fiber precursor acrylic fiber bundle and this steam drawing apparatus are characterized in that the drawing of an acrylic fiber bundle with a pressured-steam drawing apparatus is conducted by: opening an acrylic fiber bundle by blowing a fluid thereto; supplying humidifying steam to the opened acrylic fiber bundle at a fiber temperature of 80 to 130° C. to adjust the water content of the fiber bundle to 3 to 7%; and thereafter drawing the resulting acrylic fiber bundle in a pressurized-steam atmosphere. Thus, the present invention can prevent the breaking of a single fiber, the fluffing of the fiber bundle, and the breaking of the whole of the fiber bundle, though such defects are susceptible to occurring in a case where an acrylic fiber bundle is drawn by steam drawing at a high draw ratio, at a higher speed, or into a fiber having a small denier.

Claims (20)

1. A process for manufacturing a carbon-fiber precursor acrylic fiber bundle, comprising:

drawing an acrylic fiber bundle in a pressurized steam atmosphere, and in the following order:

opening the acrylic fiber bundle by spraying a fluid to the acrylic fiber bundle;

preheating the opened acrylic fiber bundle to 80° C. to 130° C.;

supplying a humidifying steam to the preheated acrylic fiber bundle thereby making the moisture content of the acrylic fiber bundle to be 3% to 7%; and

drawing the humidified acrylic fiber bundle in a pressurized steam atmosphere.

2. The process according to claim 1 , wherein the preheating is performed with a preheating roll or a heating plate.

3. The process according to claim 1 ,

wherein the humidifying steam is supplied to the preheated acrylic fiber bundle by introducing the preheated acrylic fiber bundle into a yarn humidifying device to which the humidifying steam is supplied.

4. The process according to claim 1 ,

wherein the humidifying steam is supplied to the preheated acrylic fiber bundle by spraying the humidifying steam to the preheated acrylic fiber bundle.

5. The process according to claim 1 ,

wherein the humidifying steam supplied to the preheated acrylic fiber bundle is a saturated steam.

6. The process according to claim 1 , comprising preheating the opened acrylic fiber bundle to 80° C. to 120° C.

7. The process according to claim 6 , wherein the moisture content of the acrylic fiber bundle is made to be 4% to 6%.

8. The process according to claim 1 , comprising preheating the opened acrylic fiber bundle to 80° C. to 100° C.

9. The process according to claim 8 , wherein the moisture content of the acrylic fiber bundle is made to be 4% to 6%.

10. The process according to claim 9 , comprising opening the acrylic fiber bundle by spraying air or steam to the acrylic fiber bundle at a flow rate of 300 to 700 NL/min and a pressure of 1 to 5 kgf/cm 2 .

11. The process according to claim 1 , wherein the moisture content of the acrylic fiber bundle is made to be 4% to 6%.

12. The process according to claim 1 , comprising opening the acrylic fiber bundle by spraying air or steam to the acrylic fiber bundle at a flow rate of 300 to 700 NL/min and a pressure of 1 to 5 kgf/cm 2 .

Assignments (2)
CHANGE OF NAME Recorded Jul 6, 2017
From: MITSUBISHI RAYON CO., LTD.
To: MITSUBISHI CHEMICAL CORPORATION
Reel/Frame 043098/0486 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 21, 2015
From: TADA, AKISHIGE; MIZUTORI, YUKIHIRO
To: MITSUBISHI RAYON CO., LTD.
Reel/Frame 037343/0085 →
Priority Claims (1)
JP 2013-130970 · Jun 21, 2013 · national
Continuity (1)
Related Publication 20160151959A1 · Jun 2, 2016