IP Library Granted Patent US 10,252,231
Granted Patent B2
US 10,252,231 · App. 14/929,117 · Granted Apr 9, 2019

Compositions and methods for forming emulsions

Inventors: Timothy M. Swager (Newton, MA); Edmundo Daniel Blankschtein (Brookline, MA); Lauren Dell Zarzar (Cambridge, MA); Vishnu Sresht (Cambridge, MA); Ellen Sletten (Somerville, MA); Julia Ann Kalow (Cambridge, MA)
Assignee: Massachusetts Institute of Technology
B01F17/00B01F17/0014B01F17/0035B01F17/0071C08L35/02A23V2002/00
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Quick Facts
Patent No.
US 10,252,231
App. No.
14/929,117
Granted
Apr 9, 2019
Kind
B2
Abstract

The present invention generally relates to compositions and methods for forming droplets and/or emulsions. In some embodiments, the compositions and methods comprise two or more components miscible at a first temperature and immiscible at a second temperature, dispersed in an outer phase.

Claims (17)

1. A method of forming an emulsion, comprising:

adjusting the temperature of a fluid to a first temperature, wherein the fluid at the first temperature comprises an outer phase and a second phase immiscible in the outer phase, wherein the second phase comprises a first component and a second component that are miscible with each other;

after adjusting the temperature of the fluid to the first temperature, emulsifying the fluid thereby forming a droplet comprising the first component and the second component, the droplet dispersed within the outer phase; and

after emulsifying the fluid, adjusting the temperature of the fluid to a second temperature, such that the first component and the second component within the droplet become immiscible.

2. The method of claim 1 , wherein the first temperature is greater than an upper consolute temperature of the two or more components.

3. The method of claim 1 , wherein the second temperature is less than an upper consolute temperature of the two or more components.

4. The method of claim 1 , wherein the first temperature is less than the second temperature.

5. The method of claim 4 , wherein the first temperature is less than a lower consolute temperature of the two or more components.

6. The method of claim 4 , wherein the second temperature is greater than a lower consolute temperature of the two or more components.

7. The method of claim 1 , wherein at least one of the two or more components comprises a hydrocarbon, a fluorocarbon, a silicone, a thermotropic liquid crystal, water, an ionic liquid, or combinations thereof.

8. The method of claim 1 , wherein each of the two or more components is a liquid.

9. The method of claim 1 , wherein the temperature of the fluid to the second temperature is adjusted such that the two or more components comprise a first component and a second component at least partially encapsulated within the first component.

10. The method of claim 1 , wherein emulsifying the fluid comprises emulsifying the fluid after adjusting the temperature of a fluid to the first temperature.

11. The method of claim 1 , wherein the outer phase is an aqueous phase.

12. The method of claim 11 , wherein the outer phase comprises a surfactant.

13. The method of claim 1 , wherein the outer phase is a non-aqueous phase.

14. The method of claim 1 , wherein after adjusting the temperature of the fluid to the second temperature, the droplet is a Janus droplet.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 11, 2016
From: SWAGER, TIMOTHY M.; BLANKSCHTEIN, EDMUNDO DANIEL; ZARZAR, LAUREN DELL; SRESHT, VISHNU; SLETTEN, ELLEN; KALOW, JULIA ANN
To: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
Reel/Frame 039300/0170 →
Continuity (2)
Provisional Application 62073896 · Oct 31, 2014
Related Publication 20160151753A1 · Jun 2, 2016
Cited By (2)
US 12,274,993 US 12,625,134