IP Library Granted Patent US 10,414,891
Granted Patent B2
US 10,414,891 · App. 14/964,773 · Granted Sep 17, 2019

Polyurethane curatives

Inventors: Tod C. Duvall (West Chester, OH); Jeffrey Sullivan (Goshen, OH); Nathan Eckert (Loveland, OH)
Assignee: The Shepherd Chemical Company
C08J9/00C07F5/003C08G18/161C08G18/2081C08G18/227C08G18/4027C08G18/42C08G18/48C08G18/546C08G18/7621C08G2101/0008C08G2101/0016C08G2101/0025C08G2101/0083C08G2290/00C08J2475/04C08J2475/06C08J2475/08
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Quick Facts
Patent No.
US 10,414,891
App. No.
14/964,773
Granted
Sep 17, 2019
Kind
B2
Abstract

A class of alkanol amine ligands reacted with bismuth carboxylates lends unique curability properties to isocyanate and polyols for production of polyurethane for CASE applications, including growing demand for polyurethane spray-foam. The amino-alcohol ligand, when associated with bismuth neodecanoate, offers improved moisture and solvent resistance during B-side (polyol) storage, cure rates analogous to tin-based curatives, and overall good final physical properties of the cured polyurethane.

Claims (2)

1. A spray-foam polyurethane catalyst produced by the reaction between a bismuth carboxylate with an alkanolamine and a polyol, wherein polyol is selected from polyethylene glycols, polypropylene glycols and polybutylene ether glycols, wherein the bismuth carboxylate is bismuth neodecanoate, and wherein the alkanolamine is tetrakis(2-hydroxyethyl)ethylenediamine.

2. A polyurethane catalyst produced by the reaction between a bismuth carboxylate with an alkanolamine and a polyol, wherein polyol is selected from polyethylene glycols, polypropylene glycols and polybutylene ether glycols, wherein the bismuth carboxylate is bismuth neodecanoate, and wherein the alkanolamine is ethylenedinitrilo-tetra-2-propanol.

Assignments (2)
NOTICE OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Jun 23, 2022
From: THE SHEPHERD CHEMICAL COMPANY
To: BANK OF AMERICA, N.A., AS THE ADMINISTRATIVE AGENT
Reel/Frame 060436/0042 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 3, 2016
From: DUVALL, TOD C.; SULLIVAN, JEFFREY; ECKERT, NATHAN
To: THE SHEPHERD CHEMICAL COMPANY
Reel/Frame 040215/0903 →
Continuity (2)
Provisional Application 62102726 · Jan 13, 2015
Related Publication 20160200888A1 · Jul 14, 2016