IP Library › Granted Patent US 9,708,490
Granted Patent B2
US 9,708,490 · App. 14/988,515 · Granted Jul 18, 2017

Derivatives of native lignin

Inventors: Mikhail Yurevich Balakshin (North Vancouver, CA); Alex Berlin (Burnaby, CA); Humbert Thomas Dellicolli (Hanahan, SC); Chadrick Adam Nathaniel Jordan Grunert (Vancouver, CA); Vera Maximenko Gutman (Burnaby, CA); Darwin Ortiz (Delta, CA); Edward Kendall Pye (Media, PA)
Assignee: Fibria Innovations Inc.
C08L97/005A23K10/32A23L33/105A61K36/15A61K36/48A61K36/54A61K36/76C07G1/00C08H6/00C08J3/00C08K5/13C08L23/02C08L57/00C09K15/06D21C11/0007D21H11/00C08J2397/00C08L2207/04Y02P20/582Y02P60/877
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Quick Facts
Patent No.
US 9,708,490
App. No.
14/988,515
Granted
Jul 18, 2017
Kind
B2
Abstract

The present invention provides derivatives of native lignin having a certain aliphatic hydroxyl content. Surprisingly, it has been found that consistent and predictable antioxidant activity may be provided by selecting for derivatives of native lignin having a certain aliphatic hydroxyl content.

Claims (16)

1. A lignin derivative recovered from a pulping process of a lignocellulosic biomass, wherein said lignin derivative has an aliphatic hydroxyl content of from 0.001 mmol/g to 2.35 mmol/g, and an ethoxyl content of from 0.001 mmol/g to 2 mmol/g.

2. The lignin derivative according to claim 1 , wherein the derivative has an aliphatic hydroxyl content of about 2.25 mmol/g or less.

3. The lignin derivative according to claim 1 , wherein the derivative has an aliphatic hydroxyl content of about 1.75 mmol/g or less.

4. The lignin derivative according to claim 1 , wherein the derivative has an aliphatic hydroxyl content of about 0.1 mmol/g or greater.

5. The lignin derivative according to claim 1 , wherein the derivative has a normalized RSI of 15 or greater.

6. The lignin derivative according to claim 1 , wherein the lignin is derived from softwood biomass.

7. The lignin derivative according to claim 1 , wherein the lignin is derived from annual fibre biomass.

8. The lignin derivative according to claim 1 , wherein the lignin is derived from hardwood biomass.

9. The lignin derivative according to claim 1 , wherein the pulping process is selected from the group consisting of steam explosion, dilute acid hydrolysis, ammonia fiber expansion, autohydrolysis, kraft and modifications thereof, soda pulping and modifications thereof, sulphite pulping, and organosolv processes.

10. The lignin derivative according to claim 1 , wherein the pulping process is a kraft process or a modification thereof.

11. The lignin derivative according to claim 1 , wherein the pulping process is an organosolv process.

12. A composition comprising the lignin derivative according to claim 1 and a polymer-forming component.

13. The lignin derivative according to claim 1 , wherein the ethoxyl content is from 0.05 mmol/g to 2 mmol/g.

14. The lignin derivative according to claim 1 , wherein the ethoxyl content is from 0.1 mmol/g to 2 mmol/g.

15. The lignin derivative according to claim 1 , wherein the ethoxyl content is from 0.001 mmol/g to 1.4 mmol/g.

16. The lignin derivative according to claim 1 , wherein said lignin derivative further has a phenolic hydroxyl content from 2 mmol/g to 8 mmol/g.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 28, 2019
From: FIBRIA INNOVATIONS INC.
To: SUZANO CANADA INC.
Reel/Frame 051135/0966 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 20, 2016
From: BALAKSHIN, MIKHAIL YUREVICH; BERLIN, ALEX; DELLICOLLI, HUMBERT THOMAS; GRUNERT, CHADRICK ADAM NATHANIEL JORDAN; GUTMAN, VERA MAXIMENKO; ORTIZ, DARWIN; PYE, EDWARD KENDALL
To: LIGNOL INNOVATIONS LTD.
Reel/Frame 040696/0583 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 20, 2016
From: LIGNOL INNOVATIONS LTD.
To: FIBRIA INNOVATIONS INC.
Reel/Frame 040697/0038 →
Continuity (6)
Continuation 14297360 · Jun 5, 2014
Continuation 13896254 · May 16, 2013
Continuation 12705934 · Feb 15, 2010
Provisional Application 61233345 · Aug 12, 2009
Provisional Application 61182044 · May 28, 2009
Related Publication 20160145399A1 · May 26, 2016