IP Library Granted Patent US 12,438,121
Granted Patent B2
US 12,438,121 · App. 15/017,975 · Granted Oct 7, 2025

Sintering materials and attachment methods using same

Inventors: Oscar Khaselev (Monmouth Junction, NJ); Bawa Singh (Marlton, NJ); Bin Mo (East Brunswick, NJ); Michael T. Marczi (Chester, NJ); Monnir Boureghda (East Stroudsburg, PA)
Assignee: ALPHA ASSEMBLY SOLUTIONS INC.
H01L24/83B22F1/05H01L24/27H01L24/29B22F1/10H01L2224/27436H01L2224/29101H01L2224/2919H01L2224/29324H01L2224/29339H01L2224/29344H01L2224/29347H01L2224/29364H01L2224/29399H01L2224/83192H01L2224/8384H01L2924/01047H01L2924/01079H01L2924/014
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 12,438,121
App. No.
15/017,975
Granted
Oct 7, 2025
Kind
B2
Abstract

Methods for die attachment of multichip and single components may involve printing a sintering paste on a substrate or on the back side of a die. Printing may involve stencil printing, screen printing, or a dispensing process. Paste may be printed on the back side of an entire wafer prior to dicing, or on the back side of an individual die. Sintering films may also be fabricated and transferred to a wafer, die or substrate. A post-sintering step may increase throughput.

Claims (25)

1. A method for attachment, comprising:

applying a film of metal particles to a polymeric, glass, metal, paper, or ceramic substrate, wherein applying the film comprises casting the film;

drying the film on the polymeric, glass, metal, paper, or ceramic substrate;

transferring the dried film by a lamination process at a temperature of from about 50 to about 175° C. and a pressure of from about 0.05 to about 3 MPa directly from the polymeric, glass, metal, paper, or ceramic substrate to a substrate which will subsequently receive one or more components comprising a die, wherein the dried film is in contact with the polymeric, glass, metal, paper, or ceramic substrate during lamination to the substrate which will subsequently receive said one or more components;

placing said one or more components on the transferred film to form an assembly;

applying a pressure of from about 0.5 MPa to about 20 MPa to the assembly; and

sintering the assembly at a temperature of about 175 to about 400° C. for about 0.25 seconds to about 30 minutes;

wherein the film comprises a composition comprising:

a metal powder having a d 50 range of 0.001 to 10 micrometers, the metal powder comprising 30 to 95 wt. % of the composition; and

a binder having a softening point between about 90° C. and 170° C., the binder comprising 0.1 to 0.8 wt. % of the composition;

wherein the composition has a viscosity of from about 10 to about 200,000 cP.

2. The method of claim 1 wherein the binder comprises a resin or a rosin.

3. The method of claim 1 , wherein the applied pressure is from about 2.0 to about 10 MPa.

4. The method of claim 1 , wherein the metal particles comprise coated or capped metal particles.

5. The method of claim 1 , wherein the metal particles are selected from the group consisting of gold, palladium, silver, copper, aluminum, silver palladium alloy, and gold palladium alloy.

6. The method of claim 1 , wherein the metal particles comprise silver particles.

7. The method according to claim 1 , wherein the composition further comprises one or more functional additives, the functional additives comprising 0.1 to 2 wt. % of the paste.

8. The method according to claim 7 , wherein the functional additives are selected from the group consisting of organic acids, amines, chlorinated diols, brominated diols, and metalorganic compounds.

9. The method of claim 1 wherein the polymeric, glass, metal, paper, or ceramic substrate comprises a release layer or coating.

10. The method of claim 1 wherein the polymeric, glass, metal, paper, or ceramic substrate comprises silicone.

11. The method of claim 1 wherein the transferred film is released from the polymeric, glass, metal, paper, or ceramic substrate as a result of the lamination process.

12. The method of claim 1 wherein the substrate which will subsequently receive one or more components is a direct bonded copper (DBC) substrate, silicon wafer substrate, heat spreader, or piezoelectric substrate.

13. The method of claim 1 wherein the polymeric, glass, metal, paper, or ceramic substrate is a flexible polyester substrate.

14. The method of claim 1 wherein the substrate which will subsequently receive one or more components is a lead frame.

15. The method of claim 1 wherein the substrate which will subsequently receive one or more components is a wafer.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 28, 2025
From: KHASELEV, OSCAR; SINGH, BAWA; MO, BIN; MARCZI, MICHAEL T.; BOUREGHDA, MONNIR
To: FRY'S METAL, INC.
Reel/Frame 070362/0977 →
CHANGE OF NAME Recorded Feb 28, 2025
From: FRY'S METALS INC.
To: ALPHA METALS, INC.
Reel/Frame 070366/0695 →
ASSIGNMENT OF SECURITY INTEREST IN PATENT COLLATERAL Recorded Nov 17, 2022
From: BARCLAYS BANK PLC
To: CITIBANK, N.A.
Reel/Frame 061956/0643 →
CHANGE OF NAME Recorded Feb 20, 2019
From: ALPHA METALS, INC.
To: ALPHA ASSEMBLY SOLUTIONS INC.
Reel/Frame 048389/0389 →
SECURITY INTEREST Recorded Feb 5, 2019
From: ALPHA ASSEMBLY SOLUTIONS INC. (F/K/A ALPHA METALS, INC.)
To: BARCLAYS BANK PLC, AS COLLATERAL AGENT
Reel/Frame 048260/0683 →
Continuity (3)
Division 13287820 · Nov 2, 2011
Provisional Application 61409775 · Nov 3, 2010
Related Publication 20160225737A1 · Aug 4, 2016
References Cited (63)
US 3192086A · Gyurk · 1965 [cited by examiner]
US 4494688A · Hatada · 1985 [cited by examiner]
US 4810672A · Schwarzbauer · 1989 [cited by applicant]
US 4856185A · Baumgartner · 1989 [cited by examiner]
US 4906596A · Joslin · 1990 [cited by examiner]
US 5030308A · Sheyon · 1991 [cited by examiner]
US 5049434A · Wasulko · 1991 [cited by examiner]
US 6517656B1 · DiCaprio · 2003 [cited by examiner]
US 6652804B1 · Neumann · 2003 [cited by examiner]
US 7682875B2 · Guth et al. · 2010 [cited by applicant]
US 7968008B2 · Parashar et al. · 2011 [cited by applicant]
US 20020158328A1 · Hiramatsu · 2002 [cited by examiner]
US 20050238804A1 · Garbar · 2005 [cited by examiner]
US 20050247760A1 · Palm · 2005 [cited by examiner]
US 20060197222A1 · Auerbach · 2006 [cited by examiner]
US 20080202380A1 · Bao · 2008 [cited by examiner]
US 20090025967A1 · Boureghda et al. · 2009 [cited by applicant]
US 20090162557A1 · Lu et al. · 2009 [cited by applicant]
US 20090206456A1 · Guth · 2009 [cited by examiner]
US 20090294963A1 · Guth · 2009 [cited by examiner]
US 20120103515A1 · Endoh · 2012 [cited by examiner]
CN 101803016A · 2010 [cited by applicant]
EP 1586604A1 · 2005 [cited by applicant]
JP 07073740A · 1995 [cited by examiner]
JP 2000183530A · 2000 [cited by examiner]
JP 2002245873A · 2002 [cited by applicant]
JP 2004055402A · 2004 [cited by examiner]
JP 2005104149A · 2005 [cited by examiner]
JP 2006041008A · 2006 [cited by examiner]
JP 3756283B2 · 2006 [cited by applicant]
JP 2008235198A · 2008 [cited by examiner]
JP 2009123607A · 2009 [cited by applicant]
JP 2010131669A · 2010 [cited by examiner]
KR 1020070033329 · 2007 [cited by applicant]
KR 20080112624A · 2008 [cited by applicant]
KR 1020080114202A · 2008 [cited by applicant]
KR 1020100089814 · 2010 [cited by applicant]
WO WO9920689A1 · 1999 [cited by examiner]
WO 2005079353A2 · 2005 [cited by applicant]
WO 2008017062A1 · 2008 [cited by applicant]
WO 2008065728A1 · 2008 [cited by applicant]
WO 2009016388A1 · 2009 [cited by applicant]
WO WO2011007402A1 · 2011 [cited by examiner]
JP 2010-131669 machine translation (Year: 2010). [cited by examiner]
PVA Safety Data Sheet (Year: 2015). [cited by examiner]
PVB Safety Data Sheet (Year: 2015). [cited by examiner]
JP 2006-041008 machine translation (Year: 2006). [cited by examiner]
Jin et al. Introduction to Microsystem Packaging Technology. Chapter 4. 2011. p. 65-85. (Year: 2011). [cited by examiner]
Ethyl Cellulose. PubChem. NIH. National Library of Medicine. Compound Summary. Created Jul. 9, 2008. Modified Aug. 28, 2021. (Year: 2008). [cited by examiner]
Zhang et al. Pressure-assisted low-temperature sintering of silver paste as an alternative die-attach solution to solder reflow. IEEE Transactions on Electronics Packaging Manufacturing, vol. 25, No. 4, Oct. 2002, 279-2… [cited by examiner]
JP 2004-055402 machine translation (Year: 2004). [cited by examiner]
JP 2008-235198 machine translation (Year: 2008). [cited by examiner]
C1075S (LPA409-021). Heraeus Electronics GmbH & Co. Accessed Mar. 11, 2024. (Year: 2024). [cited by examiner]
“Review: Epoxy Resin Basic I”, The Japan Society of Epoxy Resin Technology, Nov. 19, 2003, First Edition, p. 32. [cited by applicant]
Machine Translation of KR 10-2008-0114202 A, Mar. 10, 2015. [cited by applicant]
Choi Y S et al.: “Conductive paste composition for forming electrode used in plasma display panel, comprises solvent and conductive nano particles, dispersing agent, binder and reactive monomer in amounts of specific ra… [cited by applicant]
Kyoeisha Chemical Co., Ltd. Catalog, Sep. 26, 2008. [cited by applicant]
8000 Series Film Release Liners Brochure, Saint-Gobain, Aug. 17, 2003, pp. 1-2, PDF available at norton-films.com/uploadedFiles/SGNortonFilms-NA/Documents/Coated/Coated-8000-Liners-AFF1017.pdf. [cited by applicant]
Armeen Products: Description of Product Families and Application Areas, Akzo Nobel Surface Chemistry LLC, Mar. 14, 2008, pp. 1-7, sc.akzonobel.com/en/fa/Documents/AkzoNobel_tb_ArmeenProducts.pdf. [cited by applicant]
Endres, Hans-Josef Siebert-Raths, Andrea. (2011). Engineering Biopolymers-Markets, Manufacturing, Properties and Applications—4.2.8 Polyvinyl Pyrrolidones (PVP). Hanser Publishers. app.knovel.com/hotlink/pdf/id:kt00924O… [cited by applicant]
“Flexible Electronics”, Wikipedia, Aug. 13, 2009, pp. 1-2, web.archive.org/web/20090813131534/http://en.wikipedia.org/wiki/Flexible_electronics. [cited by applicant]
“Glass Transition Temperatures,” Polymer Properties Database, https://polymerdatbase.com/polymer physics/Polymer Tg C.html, downloaded Jul. 20, 2021, 6 pages. [cited by applicant]
“Glass Transition,” Polymer Properties Database, https://polymerdatbase.com/polymer physics/Glass Transition.html, downloaded Jul. 20, 2021, 2 pages. [cited by applicant]