Nitriding process method of steel member
A first nitriding process step is performed in which a steel member is subjected to a nitriding process in a nitriding gas atmosphere having a nitriding potential with which a nitride compound layer having a γ′ phase or an ε phase is generated, and thereafter a second nitriding process step is performed in which the steel member is subjected to a nitriding process in a nitriding gas atmosphere having a nitriding potential lower than the nitriding potential in the first nitriding process step, to thereby precipitate the γ′ phase in the nitride compound layer. It is possible to generate the nitride compound layer having a desired phase mode uniformly all over a component to be treated and to manufacture a nitrided steel member high in pitting resistance and bending fatigue strength.
1. A nitriding process method of a steel member,
wherein a first nitriding process step is performed in which the steel member is subjected to a nitriding process in a nitriding gas atmosphere having a nitriding potential with which a nitride compound layer having a γ′ phase or an ϵ phase is generated, and thereafter a second nitriding process step is performed in which the steel member is subjected to a nitriding process in a nitriding gas atmosphere having a nitriding potential lower than the nitriding potential in the first nitriding process step, to thereby further precipitate γ′ phase in the nitride compound layer, and
wherein the first nitriding step is performed in a nitriding gas atmosphere having a 0.6 to 1.51 nitriding potential, and the second nitriding process step is performed in a nitriding gas atmosphere having a 0.16 to 0.25 nitriding potential.
2. The nitriding process method of the steel member according to claim 1 , wherein, in the first nitriding process step, the nitriding potential is controlled to 0.6 to 1.51 by introducing NH 3 gas to a heating chamber where the nitriding process is performed and adjusting a flow rate of H 2 gas, and
wherein, in the second nitriding process step, the nitriding potential is controlled to 0.16 to 0.25 by introducing the NH 3 gas at a flow rate lower than the flow rate in the first nitriding process step to the heating chamber where the nitriding process is performed and adjusting a flow rate of the H 2 gas.
3. The nitriding process method of the steel member according to claim 2 , wherein temperatures in the heating chamber in the first nitriding step and the second nitriding step are kept at 520 to 610° C.
4. The nitriding process method of the steel member according to claim 3 , wherein a difference between the temperatures in the first nitriding step and the second nitriding step is within 50° C.
5. The nitriding process step of the steel member according to claim 4 , wherein the temperatures in the first nitriding step and the second nitriding step are equal to each other.