IP Library Granted Patent US 10,385,251
Granted Patent B2
US 10,385,251 · App. 15/026,233 · Granted Aug 20, 2019

Compounds, complexes, compositions, methods and systems for heating and cooling

Inventors: William F. Schneider (Notre Dame, IN); Joan F. Brennecke (Notre Dame, IN); George Mozurkewich (Albuquerque, NM); Mark J. McCready (Notre Dame, IN); Edward J. Maginn (Notre Dame, IN); Brandon L. Ashfeld (Notre Dame, IN); Mark Stadtherr (Notre Dame, IN)
Assignee: UNIVERSITY OF NOTRE DAME DU LAC
C09K5/16C09K5/041F25B13/00F25B9/008F25B2309/06
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Quick Facts
Patent No.
US 10,385,251
App. No.
15/026,233
Granted
Aug 20, 2019
Kind
B2
Abstract

Disclosed herein are ionic liquid compounds, complexes and compositions suitable for use as refrigerants. Methods and systems for heating and/or cooling, including vapor compression heating or cooling systems, including such refrigerants are also disclosed. Preferred ionic liquids include those having anions selected from pyrrolide, pyrazolide, triazolide, imidazolide, benzimidazolide, and indolide, and cations selected from phosphonium, ammonium, pyrrolidinium, imidazolium, and pyridinium.

Claims (31)

1. A composition comprising:

an ionic liquid; and

carbon dioxide;

wherein the ionic liquid has a CO 2 binding enthalpy of from about (−)20 kJ/mol to about (−)40 kJ/mol;

wherein the composition is suitable for use in a vapor compression cooling or heating system; and

wherein the ionic liquid comprises an anion selected from the group consisting of 2-nitropyrrole, 3-nitropyrazole, 4-nitropyrazole, 2-nitro imidazole, 2-cyano imidazole, 2-chloro imidazole, 2-bromo imidazole, imidazole-2-carbaldehyde, 2-trifluoromethyl imidazole, 2-nitro indolide, 3-nitro indolide, 7-nitro indolide, 2-cyano indolide, 7-cyano indolide, 2-fluoro indolide, 2-chloro indolide, 7-chloro indolide, 2-bromo indolide, 7-bromo indolide, indolide-2-carbaldehyde, indolide-7-carbaldehyde, 2-trifluromethyl indolide, 7-trifluromethyl indolide, o-fluorophenoxide, m-fluorophenoxide, o-cyanophenoxide, m-cyanophenoxide, p-cyanophenoxide, m-hydroxyphenoxide, m-nitrophenoxide, 2,6-difluorophenoxide, 2,6-difluoro-4-methylphenoxide.

2. The composition of claim 1 , further comprising an additive that improves the flowability of the composition.

3. The composition of claim 2 , wherein the additive comprises tetraglyme.

4. A method of cooling or heating an enclosed space comprising:

compressing a composition comprising an ionic liquid and carbon dioxide;

cooling said composition;

reducing the pressure of said composition; and

contacting the enclosed space with said composition;

wherein the ionic liquid has a CO 2 binding enthalpy of from about (−)20 kJ/mol to about (−)40 kJ/mol; and

wherein the ionic liquid comprises an anion selected from the group consisting of 2-nitropyrrole, 3-nitropyrazole, 4-nitropyrazole, 2-nitro imidazole, 2-cyano imidazole, 2-chloro imidazole, 2-bromo imidazole, imidazole-2-carbaldehyde, 2-trifluoromethyl imidazole, 2-nitro indolide, 3-nitro indolide, 7-nitro indolide, 2-cyano indolide, 7-cyano indolide, 2-fluoro indolide, 2-chloro indolide, 7-chloro indolide, 2-bromo indolide, 7-bromo indolide, indolide-2-carbaldehyde, indolide-7-carbaldehyde, 2-trifluromethyl indolide, 7-trifluromethyl indolide, o-fluorophenoxide, m-fluorophenoxide, o-cyanophenoxide, m-cyanophenoxide, p-cyanophenoxide, m-hydroxyphenoxide, m-nitrophenoxide, 2,6-difluorophenoxide, 2,6-difluoro-4-methylphenoxide.

5. The method of claim 4 , wherein the composition further comprises an additive that improves the flowability of the composition.

6. The method of claim 5 , wherein the additive comprises tetraglyme.

7. A system for cooling or heating an enclosed space comprising:

a composition comprising an ionic liquid and carbon dioxide;

a compression device;

a means for cooling said composition;

an expansion device; and

a heat exchanger;

wherein the ionic liquid has a CO 2 binding enthalpy of from about (−)20 kJ/mol to about (−)40 kJ/mol; and

wherein the ionic liquid comprises an anion selected from the group consisting of 2-nitropyrrole, 3-nitropyrazole, 4-nitropyrazole, 2-nitro imidazole, 2-cyano imidazole, 2-chloro imidazole, 2-bromo imidazole, imidazole-2-carbaldehyde, 2-trifluoromethyl imidazole, 2-nitro indolide, 3-nitro indolide, 7-nitro indolide, 2-cyano indolide, 7-cyano indolide, 2-fluoro indolide, 2-chloro indolide, 7-chloro indolide, 2-bromo indolide, 7-bromo indolide, indolide-2-carbaldehyde, indolide-7-carbaldehyde, 2-trifluromethyl indolide, 7-trifluromethyl indolide, o-fluorophenoxide, m-fluorophenoxide, o-cyanophenoxide, m-cyanophenoxide, p-cyanophenoxide, m-hydroxyphenoxide, m-nitrophenoxide, 2,6-difluorophenoxide, 2,6-difluoro-4-methylphenoxide.

8. The system of claim 7 , wherein the composition further comprises an additive that improves the flowability of the composition.

9. The system of claim 8 , wherein the additive comprises tetraglyme.

10. The method of claim 4 , wherein the ionic liquid further comprises a cation selected from the group consisting of phosphonium, ammonium, pyrrolidinium, imidazolium, and pyridinium.

11. The system of claim 7 , wherein the ionic liquid further comprises a cation selected from the group consisting of phosphonium, ammonium, pyrrolidinium, imidazolium, and pyridinium.

12. The system of claim 7 , further comprising a system to provide an optimized ratio of carbon dioxide to ionic liquid.

13. The composition of claim 1 , wherein the ionic liquid further comprises a cation selected from the group consisting of phosphonium, ammonium, pyrrolidinium, imidazolium, and pyridinium.

Assignments (2)
CONFIRMATORY LICENSE Recorded Dec 14, 2023
From: UNIVERSITY OF NOTRE DAME
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 066012/0575 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 2, 2018
From: SCHNEIDER, WILLIAM F.; BRENNECKE, JOAN F.; MOZURKEWICH, GEORGE; MCCREADY, MARK J.; MAGINN, EDWARD J.; ASHFELD, BRANDON L.; STADHERR, MARK
To: UNIVERSITY OF NOTRE DAME DU LAC
Reel/Frame 046254/0341 →
Continuity (2)
Provisional Application 61884334 · Sep 30, 2013
Related Publication 20160237333A1 · Aug 18, 2016