IP Library Granted Patent US 9,834,563
Granted Patent B2
US 9,834,563 · App. 15/039,607 · Granted Dec 5, 2017

Antidiabetic substituted heteroaryl compounds

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Quick Facts
Patent No.
US 9,834,563
App. No.
15/039,607
Granted
Dec 5, 2017
Kind
B2
Abstract

The present invention relates to a compound represented by formula (I): and pharmaceutically acceptable salts thereof. The compounds of formula I are agonists of G-protein coupled receptor 40 (GPR40) and may be useful in the treatment, prevention and suppression of diseases mediated by the G-protein-coupled receptor 40. The compounds of the present invention may be useful in the treatment of Type 2 diabetes mellitus, and of conditions that are often associated with this disease, including obesity and lipid disorders, such as mixed or diabetic dyslipidemia, hyperlipidemia, hypercholesterolemia, and hypertriglyceridemia.

Claims (167)

1. A compound of structural formula I:

or a pharmaceutically acceptable salt thereof, wherein

ring A is a monocyclic heteroaryl containing 1 to 2 N heteroatoms;

X is

(1) bond,

(2) —O—,

(3) NH,

(4) —(C 1-6 )alkyl-O—, wherein the alkyl or oxygen attaches to ring A,

(5) —O—(C 1-6 )alkyl-O—, or

(6) —(C 1-6 )alkyl-N(H)—, wherein the alkyl or nitrogen attaches to ring A;

R 1 is

(1) (C 3-7 )cycloalkyl,

(2) heterocycloalkyl containing 1 to 2 heteroatoms independently selected from the group consisting N, S, and O,

(3) heteroaryl containing 1 to 3 heteroatoms independently selected from the group consisting of N, O, and S,

(4) —S(O) 2 (C 1-3 )alkyl, or

(6) —(CH 2 ) q -aryl,

wherein each heterocycloalkyl, heteroaryl, aryl, or cycloalkyl groups are unsubstituted or substituted with 1 to 2 substitutents each independently R 5 ;

R 2 is

(1) (C 1-6 )alkyl,

(2) halo(C 1-6 )alkyl,

(3) hydroxy(C 1-6 )alkyl, or

(4) halo;

R 3 is

(1) (C 1-6 )alkyl, or

(2) halo;

R 4 is

(1) hydrogen, or

(2) (C 1-3 )alkyl;

R 5 is

(1) oxo,

(2) hydroxy,

(3) (C 1-6 )alkyl,

(4) halo(C 1-6 )alkyl,

(5) hydroxy(C 1-6 )alkyl,

(6) cyano,

(7) phenyl,

(8) —S(O) 2 (C 1-3 )alkyl,

(9) —(C 1-3 )alkyl-S(O) 2 (C 1-3 )alkyl, or

(10) —(C 1-3 )alkyl-N(H)—S(O) 2 (C 1-3 )alkyl;

R 6 is

(1) hydrogen,

(2) (C 1-6 )alkyl, or

(3) (C 3-7 )cycloalkyl;

n is 0, 1, 2, or 3;

m is 0 or 1;

k is 0, 1, 2 or 3; and

q is 0,1,2, or 3.

2. The compound according to claim 1 , or a pharmaceutically acceptable salt thereof, wherein X is a bond, —O—, —N(H)—, —(CH 2 ) 3 —NH—, —(CH 2 ) 2 —NH—, —CH 2 —N(H)—, —(CH 2 ) 4 —O—, —(CH 2 ) 3 —O—, —(CH 2 ) 2 —O—, —CH 2 —O— or —O—(CH 2 ) 3 —O—.

3. The compound of claim 2 , or a pharmaceutically acceptable salt thereof, wherein ring A is pyridinyl or pyrimidinyl.

4. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein R 6 is hydrogen.

5. A compound of structural formula I:

or a pharmaceutically acceptable salt thereof, wherein

ring A is a bicyclic heteroaryl containing 1 to 4 heteroatoms independently selected from the group consisting of N, O, and S;

X is

(1) bond,

(2) —O—,

(3) NH,

(4) —(C 1-6 )alkyl-O—, wherein the alkyl or oxygen attaches to ring A,

(5) —O—(C 1-6 )alkyl-O—, or

(6) —(C 1-6 )alkyl-N(H)—, wherein the alkyl or nitrogen attaches to ring A;

R 1 is

(1) (C 3-7 )cycloalkyl,

(2) heterocycloalkyl containing 1 to 2 heteroatoms independently selected from the group consisting N, S, and O,

(3) heteroaryl containing 1 to 3 heteroatoms independently selected from the group consisting of N, O, and S,

(4) —S(O) 2 (C 1-3 )alkyl, or

(6) —(CH 2 ) q -aryl,

wherein each heterocycloalkyl, heteroaryl, aryl, or cycloalkyl groups are unsubstituted or substituted with 1 to 2 substitutents each independently R 5 ;

R 2 is

(1) (C 1-6 )alkyl,

(2) hydroxy(C 1-6 )alkyl, or

(3) halo;

R 3 is

(1) (C 1-6 )alkyl, or

(2) halo;

R 4 is

(1) hydrogen, or

(2) (C 1-3 )alkyl;

R 5 is

(7) oxo,

(8) hydroxy,

(9) (C 1-6 )alkyl,

(10) halo(C 1-6 )alkyl,

(11) hydroxy(C 1-6 )alkyl,

(12) cyano,

(7) phenyl,

(8) —S(O) 2 (C 1-3 )alkyl,

(9) —(C 1-3 )alkyl-S(O) 2 (C 1-3 )alkyl, or

(10) —(C 1-3 )alkyl-N(H)—S(O) 2 (C 1-3 )alkyl;

R 6 is

(1) hydrogen,

(2) (C 1-6 )alkyl, or

(3) (C 3-7 )cycloalkyl;

n is 0, 1, 2, or 3;

m is 0 or 1;

k is 0, 1, 2 or 3; and

q is 0, 1, 2, or 3.

6. The compound according to claim 5 , or a pharmaceutically acceptable salt thereof, wherein X is a bond, —O—, —N(H)—, —(CH 2 ) 3 —NH—, —(CH 2 ) 2 —NH—, —CH 2 —N(H)—, —(CH 2 ) 4 —O—, —(CH 2 ) 3 —O—, —(CH 2 ) 2 —O—, —CH 2 —O— or —O—(CH 2 ) 3 —O—.

7. The compound of claim 6 , or a pharmaceutically acceptable salt thereof, wherein ring A is 1H-pyrazolo[4,3-b]pyridinyl, thiazolo[4,5-b]pyridinyl, or 1H-pyrrolo[2,3-b]pyridinyl.

8. The compound of claim 5 , or a pharmaceutically acceptable salt thereof, wherein R 6 is hydrogen.

9. A compound of structural formula I-A:

or a pharmaceutically acceptable salt thereof, wherein

X is

(1) a bond,

(2) —O—,

(3) —(C 1-6 )alkyl-O—, wherein the alkyl or oxygen attaches to ring A

(4) —O—(C 1-6 )alkyl-O—, or

(5) —(C 1-6 )alkyl-N(H)—, wherein the alkyl or nitrogen attaches to ring A;

R 1 is

(1) (C 3-7 )cycloalkyl,

(2) heterocycloalkyl containing 1 to 2 heteroatoms independently selected from the group consisting of N, S, and O,

(3) heteroaryl containing 1 to 3 heteroatoms independently selected from the group consisting of N, O, and S,

(4) —S(O) 2 (C 1-3 )alkyl, or

(5) —(CH 2 )q-aryl,

wherein each heterocycloalkyl, heteroaryl, aryl, or cycloalkyl groups are unsubstituted or substituted with 1 to 2 substitutents each independently R 5 ;

R 2 is

(1) (C 1-6 )alkyl,

(2) halo(C 1-6 )alkyl, or

(3) hydroxy(C 1-6 )alkyl;

R 3 is

(1) (C 1-6 )alkyl, or

(2) halo;

R 4 is

(1) hydrogen, or

(2) (C 1-3 )alkyl;

R 5 is

(1) oxo,

(2) hydroxy,

(3) (C 1-6 )alkyl,

(4) halo(C 1-6 )alkyl,

(5) hydroxy(C 1-6 )alkyl,

(6) cyano,

(7) phenyl,

(8) —S(O) 2 (C 1-3 )alkyl,

(9) —(C 1-3 )alkyl-S(O) 2 (C 1-3 )alkyl, or

(10) —(C 1-3 )alkyl-N(H)—S(O) 2 (C 1-3 )alkyl;

n is 0, 1, 2, or 3;

m is 0 or 1;

k is 0, 1, 2 or 3, and

q is 0, 1, 2, or 3.

10. A compound selected from

or a pharmaceutically acceptable salt, thereof.

11. A pharmaceutical composition comprising a compound of claim 1 , or a pharmaceutically acceptable salt thereof, and a pharmaceutically acceptable carrier.

12. A method of treating type 2 diabetes mellitus in a patient in need of treatment comprising the administration to the patient of a therapeutically effective amount of a compound of claim 1 , or a pharmaceutically acceptable salt thereof.

13. A pharmaceutical composition comprising

(1) a compound of claim 1 or a pharmaceutically acceptable salt thereof;

(2) one or more compounds selected from the group consisting of:

(a) PPAR gamma agonists and partial agonists;

(b) biguanides;

(c) protein tyrosine phosphatase-1B (PTP-1B) inhibitors;

(d) dipeptidyl peptidase IV (DP-IV) inhibitors;

(e) insulin or an insulin mimetic;

(f) sulfonylureas;

(g) α-glucosidase inhibitors;

(h) agents which improve a patient's lipid profile, said agents being selected from the group consisting of (i) HMG-CoA reductase inhibitors, (ii) bile acid sequestrants, (iii) nicotinyl alcohol, nicotinic acid or a salt thereof, (iv) PPARα agonists, (v) cholesterol absorption inhibitors, (vi) acyl CoA:cholesterol acyltransferase (ACAT) inhibitors, (vii) CETP inhibitors, and (viii) phenolic anti-oxidants;

(i) PPARα/γ dual agonists,

(j) PPARδ agonists,

(k) antiobesity compounds,

(l) ileal bile acid transporter inhibitors;

(m) anti-inflammatory agents;

(n) glucagon receptor antagonists;

(o) GLP-1;

(p) GIP-1;

(q) GLP-1 analogs;

(r) HSD-1 inhibitors;

(s) SGLT 1 inhibitors; and

(t) SGLT 2 inhibitors; and

(3) a pharmaceutically acceptable carrier.

Assignments (4)
MERGER Recorded Aug 8, 2022
From: MERCK SHARP & DOHME CORP.
To: MERCK SHARP & DOHME LLC
Reel/Frame 061102/0145 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 26, 2016
From: HU, BIN; CUI, MINGXIANG; CHEN, ZHENGXIA; DAI, MEIBI; ZHANG, ZAIHONG; LV, YING; TIAN, LILI
To: WUXI APPTEC (SHANGHAI) CO., LTD.
Reel/Frame 038729/0193 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 26, 2016
From: WUXI APPTEC (SHANGHAI) CO., LTD.
To: MERCK SHARP & DOHME CORP.
Reel/Frame 038729/0392 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 26, 2016
From: HAGMANN, WILLIAM K.; LI, BING; SZEWCZYK, JASON W.; WANG, BOWEI; PARKER, DANN; BLIZZARD, TIMOTHY; JOSIEN, HUBERT; BIJU, PURAKKATTLE; CHOBANIAN, HARRY; GUDE, CANDIDO; NARGUND, RAVI P.; PIO, BARBARA; DANG, QUN; LIN, LINUS S.
To: MERCK SHARP & DOHME CORP.
Reel/Frame 038824/0001 →