IP Library Granted Patent US 9,893,354
Granted Patent B2
US 9,893,354 · App. 15/049,489 · Granted Feb 13, 2018

Hyper-dendritic nanoporous zinc foam anodes, methods of producing the same, and methods for their use

Inventors: Daniel A. Steingart (Princeton, NJ); Mylad Chamoun (Princeton, NJ); Benjamin Hertzberg (Princeton, NJ); Greg Davies (Princeton, NJ); Andrew G. Hsieh (Princeton, NJ)
Assignee: THE TRUSTEES OF PRINCETON UNIVERSITY
H01M4/42C25D5/00C25D5/16H01M4/0452H01M4/244H01M4/29H01M4/38H01M4/661C25D3/22H01M2004/021H01M2004/027
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Quick Facts
Patent No.
US 9,893,354
App. No.
15/049,489
Granted
Feb 13, 2018
Kind
B2
Abstract

Disclosed are hyper-dendritic nanoporous zinc foam electrodes, viz., anodes, methods of producing the same, and methods for their use in electrochemical cells, especially in rechargeable electrical batteries.

Claims (10)

1. An electrode comprising hyper-dendritic nanoporous zinc foam.

2. An electrode according to claim 1 , electrodeposited hyper-dendritic nanoporous zinc foam upon a substrate or structure.

3. An electrode according to claim 1 , wherein the hyper-dendritic nanoporous zinc foam comprises nanoparticles formed on secondary dendrites in a three-dimensional network.

4. An electrode according to claim 3 , wherein the nanoparticles formed on secondary dendrites in a three-dimensional network with a particle size distribution of 54.1-96.0 nm.

5. A method of forming an electrode according to claim 1 , which method comprises the step of:

depositing zinc from an aqueous composition which includes zinc via electrodeposition onto a substrate or structure using an electrical overpotential to thereby form hyper-dendritic nanoporous zinc foam having primary and secondary dendrites in a three-dimensional network.

6. A method according to claim 5 , wherein the zinc foam provides an electrical current pathway therethrough and to the substrate or structure.

7. A method according to claim 5 , wherein the substrate or structure contains nickel.

8. A method according to claim 5 , wherein said zinc foam is formed in potentiostatic charging conditions at −2.0 volt versus mercury/mercury oxide and higher, in a three-electrode setup consisting of a platinum or nickel working electrode, a mercury/mercury oxide reference electrode and a platinum or nickel counter electrode.

9. A primary or secondary battery which comprises an electrode according to claim 1 .

Assignments (2)
CONFIRMATORY LICENSE Recorded Nov 17, 2023
From: PRINCETON UNIVERSITY
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 065617/0015 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 12, 2017
From: STEINGART, DANIEL A.; CHAMOUN, MYLAD; HERTZBERG, BENJAMIN; DAVIES, GREG; HSIEH, ANDREW G.
To: THE TRUSTEES OF PRINCETON UNIVERSITY
Reel/Frame 043854/0243 →
Continuity (2)
Provisional Application 62121699 · Feb 27, 2015
Related Publication 20170025677A1 · Jan 26, 2017