IP Library Granted Patent US 10,060,865
Granted Patent B2
US 10,060,865 · App. 15/065,637 · Granted Aug 28, 2018

Measurement of critical dimensions of nanostructures using X-ray grazing incidence in-plane diffraction

Inventors: Ronald D. Ruth (Stanford, CA); Roderick J. Loewen (Redwood City, CA); Martin A. Gifford (Palo Alto, CA)
Assignee: Lyncean Technologies, Inc.
G01N23/207G01B15/00G01B2210/56G01N2223/6116
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Quick Facts
Patent No.
US 10,060,865
App. No.
15/065,637
Granted
Aug 28, 2018
Kind
B2
Abstract

The manufactured structure is illuminated with an x-ray beam. The manufactured structure is positioned at a selected grazing angle and a selected rotation angle with respect to the x-ray beam. The selected rotation angle has been selected to enhance in-plane diffraction of reflections of the x-ray beam by the manufactured structure. A grazing in-plane diffraction beam produced by interference with the periodic feature is detected. A property of the grazing in-plane diffraction beam is determined by the critical dimension.

Claims (63)

1. A system for analyzing a manufactured structure having a periodic feature characterized by a critical dimension including:

a x-ray beam source configured to illuminate the manufactured structure with an x-ray beam, wherein the manufactured structure is positioned at a selected grazing angle and a selected rotation angle with respect to the x-ray beam and the selected rotation angle has been selected to enhance in-plane diffraction of reflections of the x-ray beam by the manufactured structure;

a detector configured to detect a grazing in-plane diffraction beam produced by interference with the periodic feature, wherein a property of the grazing in-plane diffraction beam is determined by the critical dimension; and

a processor configured to characterize the critical dimension based on the property of the grazing in-plane diffraction beam.

2. The system of claim 1 , wherein the system is utilized inline in a semiconductor manufacturing process to detect deviation of the manufactured structure from a reference.

3. The system of claim 1 , wherein the manufactured structure is at least a portion of a semiconductor device.

4. The system of claim 1 , wherein the x-ray beam illuminating the manufactured structure has been collimated.

5. The system of claim 1 , wherein the x-ray beam illuminating the manufactured structure has not been collimated.

6. The system of claim 1 , wherein divergent rays of the x-ray beam illuminating the manufactured structure have been focused on the manufactured structure.

7. The system of claim 1 , wherein the x-ray beam illuminating the manufactured structure has a divergence greater than 3 milliradians.

8. The system of claim 1 , wherein characterizing the critical dimension includes determining a measurement value of structure parameters of the critical dimension.

9. The system of claim 1 , wherein characterizing the critical dimension includes comparing the property of the grazing in-plane diffraction beam with a model generated property of an expected grazing in-plane diffraction beam.

10. The system of claim 9 , wherein the model generated property of the expected grazing in-plane diffraction beam was generated using a Parratt analytical model.

11. The system of claim 1 , wherein the selected rotation angle includes an in-plane rotation angle in a plane of the manufactured structure and the in-plane rotation angle has been selected to enhance a diffraction pattern produced by the grazing in-plane diffraction beam when in-plane reflected x-ray paths are superposed.

12. The system of claim 1 , wherein the detector is a two-dimensional detector including scintillator-coupled CCDs.

13. The system of claim 1 , wherein detecting the grazing in-plane diffraction beam includes detecting a diffraction pattern caused at least in part by multiple reflections of a single ray on multiple surfaces of the periodic feature.

14. The system of claim 1 , wherein detecting the grazing in-plane diffraction beam includes detecting a Laue-Bragg diffraction.

15. The system of claim 1 , wherein the property of the grazing in-plane diffraction beam includes one or more of the following: an intensity, an angle, and a position.

16. The system of claim 1 , wherein the critical dimension includes one or more of the following: a sidewall angle, a line height, a linewidth, a pitch, and a roughness.

17. The system of claim 1 , wherein characterizing the critical dimension includes aggregating properties of grazing in-plane diffraction beams detected at different measurement instances corresponding to different rotation angles.

18. The system of claim 1 , wherein characterizing the critical dimension includes detecting one or more peaks of a plot of the property of the grazing in-plane diffraction beam.

19. A method for analyzing a manufactured structure having a periodic feature characterized by a critical dimension including:

illuminating the manufactured structure with an x-ray beam, wherein the manufactured structure is positioned at a selected grazing angle and a selected rotation angle with respect to the x-ray beam and the selected rotation angle has been selected to enhance in-plane diffraction of reflections of the x-ray beam by the manufactured structure;

detecting a grazing in-plane diffraction beam produced by interference with the periodic feature, wherein a property of the grazing in-plane diffraction beam is determined by the critical dimension; and

characterizing the critical dimension based on the property of the grazing in-plane diffraction beam.

20. The method of claim 19 , wherein characterizing the critical dimension includes detecting a deviation of the manufactured structure from a reference as a part of a semiconductor manufacturing process.

21. The method of claim 19 , wherein the manufactured structure is at least a portion of a semiconductor device.

22. The method of claim 19 , wherein the x-ray beam illuminating the manufactured structure has been collimated.

23. The method of claim 19 , wherein the x-ray beam illuminating the manufactured structure has not been collimated.

24. The method of claim 19 , wherein divergent rays of the x-ray beam illuminating the manufactured structure have been focused on the manufactured structure.

25. The method of claim 19 , wherein the x-ray beam illuminating the manufactured structure has a divergence greater than 3 milliradians.

26. The method of claim 19 , wherein characterizing the critical dimension includes determining a measurement value of structure parameters of the critical dimension.

27. The method of claim 19 , wherein characterizing the critical dimension includes comparing the property of the grazing in-plane diffraction beam with a model generated property of an expected grazing in-plane diffraction beam.

28. The method of claim 27 , wherein the model generated property of the expected grazing in-plane diffraction beam was generated using a Parratt analytical model.

29. The method of claim 19 , wherein the selected rotation angle includes an in-plane rotation angle in a plane of the manufactured structure and the in-plane rotation angle has been selected to enhance a diffraction pattern produced by the grazing in-plane diffraction beam when in-plane reflected x-ray paths are superposed.

30. The method of claim 19 , wherein the grazing in-plane diffraction beam is detected using a two-dimensional detector including scintillator-coupled CCDs.

31. The method of claim 19 , wherein detecting the grazing in-plane diffraction beam includes detecting a diffraction pattern caused at least in part by multiple reflections of a single ray on multiple surfaces of the periodic feature.

32. The method of claim 19 , wherein detecting the grazing in-plane diffraction beam includes detecting a Laue-Bragg diffraction.

33. The method of claim 19 , wherein the property of the grazing in-plane diffraction beam includes one or more of the following: an intensity, an angle, and a position.

34. The method of claim 19 , wherein the critical dimension includes one or more of the following: a sidewall angle, a line height, a linewidth, a pitch, and a roughness.

35. The method of claim 19 , wherein characterizing the critical dimension includes aggregating properties of grazing in-plane diffraction beams detected at different measurement instances corresponding to different rotation angles.

36. The method of claim 19 , wherein characterizing the critical dimension includes detecting one or more peaks of a plot of the property of the grazing in-plane diffraction beam.

37. A computer program product for analyzing a manufactured structure having a periodic feature characterized by a critical dimension, the computer program product being embodied in a tangible computer readable storage medium and comprising computer instructions for:

illuminating the manufactured structure with an x-ray beam, wherein the manufactured structure is positioned at a selected grazing angle and a selected rotation angle with respect to the x-ray beam and the selected rotation angle has been selected to enhance in-plane diffraction of reflections of the x-ray beam by the manufactured structure;

detecting a grazing in-plane diffraction beam produced by interference with the periodic feature, wherein a property of the grazing in-plane diffraction beam is determined by the critical dimension; and

characterizing the critical dimension based on the property of the grazing in-plane diffraction beam.

38. The computer program product of claim 37 , wherein characterizing the critical dimension includes detecting a deviation of the manufactured structure from a reference as a part of a semiconductor manufacturing process.

39. The computer program product of claim 37 , wherein the manufactured structure is at least a portion of a semiconductor device.

40. computer program product of claim 37 , wherein the x-ray beam illuminating the manufactured structure has been collimated.

41. The computer program product of claim 37 , wherein the x-ray beam illuminating the manufactured structure has not been collimated.

42. The computer program product of claim 37 , wherein divergent rays of the x-ray beam illuminating the manufactured structure have been focused on the manufactured structure.

43. The computer program product of claim 37 , wherein the x-ray beam illuminating the manufactured structure has a divergence greater than 3 milliradians.

44. The computer program product of claim 37 , wherein characterizing the critical dimension includes determining a measurement value of structure parameters of the critical dimension.

45. The computer program product of claim 37 , wherein characterizing the critical dimension includes comparing the property of the grazing in-plane diffraction beam with a model generated property of an expected grazing in-plane diffraction beam.

46. The computer program product of claim 45 , wherein the model generated property of the expected grazing in-plane diffraction beam was generated using a Parratt analytical model.

47. The computer program product of claim 37 , wherein the selected rotation angle includes an in-plane rotation angle in a plane of the manufactured structure and the in-plane rotation angle has been selected to enhance a diffraction pattern produced by the grazing in-plane diffraction beam when in-plane reflected x-ray paths are superposed.

48. The computer program product of claim 37 , wherein the grazing in-plane diffraction beam is detected using a two-dimensional detector including scintillator-coupled CCDs.

49. The computer program product of claim 37 , wherein detecting the grazing in-plane diffraction beam includes detecting a diffraction pattern caused at least in part by multiple reflections of a single ray on multiple surfaces of the periodic feature.

50. The computer program product of claim 37 , wherein detecting the grazing in-plane diffraction beam includes detecting a Laue-Bragg diffraction.

51. The computer program product of claim 37 , wherein the property of the grazing in-plane diffraction beam includes one or more of the following: an intensity, an angle, and a position.

52. The computer program product of claim 37 , wherein the critical dimension includes one or more of the following: a sidewall angle, a line height, a linewidth, a pitch, and a roughness.

53. The computer program product of claim 37 , wherein characterizing the critical dimension includes aggregating properties of grazing in-plane diffraction beams detected at different measurement instances corresponding to different rotation angles.

54. The computer program product of claim 37 , wherein characterizing the critical dimension includes detecting one or more peaks of a plot of the property of the grazing in-plane diffraction beam.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 8, 2023
From: LYNCEAN TECHNOLOGIES, INC.
To: LYNCEAN (ASSIGNMENT FOR THE BENEFIT OF CREDITORS), LLC
Reel/Frame 062621/0823 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 8, 2023
From: LYNCEAN (ASSIGNMENT FOR THE BENEFIT OF CREDITORS), LLC
To: LYRA ACQUISITION HOLDINGS LLC
Reel/Frame 062621/0834 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 13, 2016
From: RUTH, RONALD D.; LOEWEN, RODERICK J.; GIFFORD, MARTIN A.
To: LYNCEAN TECHNOLOGIES, INC.
Reel/Frame 038594/0321 →
Continuity (2)
Provisional Application 62131082 · Mar 10, 2015
Related Publication 20160266056A1 · Sep 15, 2016
Cited By (1)
US 12,710,403