IP Library Granted Patent US 11,149,324
Granted Patent B2
US 11,149,324 · App. 15/078,562 · Granted Oct 19, 2021

High strength austenitic stainless steel having excellent resistance to hydrogen embrittlement, method for manufacturing the same, and hydrogen equipment used for high-pressure hydrogen gas and liquid hydrogen environment

Inventors: Kazuhisa Matsumoto (Hikari, JP); Masaharu Hatano (Hikari, JP)
Assignee: NIPPON STEEL STAINLESS STEEL CORPORATION
C21D9/0068C21D8/005C22C38/001C22C38/002C22C38/005C22C38/02C22C38/04C22C38/06C22C38/42C22C38/44C22C38/46C22C38/48C22C38/50C22C38/54F17C1/10F17C1/14F17C2203/0643F17C2203/0648F17C2221/012F17C2223/0123F17C2223/036F17C2260/011F17C2260/053
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Quick Facts
Patent No.
US 11,149,324
App. No.
15/078,562
Granted
Oct 19, 2021
Kind
B2
Abstract

This high strength austenitic stainless steel having excellent resistance to hydrogen embrittlement includes, in terms of mass %, C: 0.2% or less, Si: 0.2% to 1.5%, Mn: 0.5% to 2.5%, P: 0.06% or less, S: 0.008% or less, Ni: 10.0% to 20.0%, Cr: 16.0% to 25.0%, Mo: 3.5% or less, Cu: 3.5% or less, N: 0.01% to 0.50%; and O: 0.015% or less, with the balance being Fe and unavoidable impurities, in which an average size of precipitates is 100 nm or less and an amount of the precipitates is 0.001% to 1.0% in terms of mass %.

Claims (92)

1. An austenitic stainless steel having resistance to hydrogen embrittlement comprising, in terms of mass %:

C: 0.2% or less;

Si: 0.2% to 1.5%;

Mn: 0.5% to 2.5%;

P: 0.042% or less;

S: 0.008% or less;

Ni: 10.0% to 20.0%;

Cr: 16.0% to 19.1%;

Mo: 3.5% or less;

Cu: 1.52% or less;

N: 0.01% to 0.50%; and

O: 0.015% or less,

with a balance being Fe and unavoidable impurities,

wherein an average size of precipitates is 100 nm or less and an amount of the precipitates is 0.001% to 1.0% in terms of mass %.

2. The austenitic stainless steel having resistance to hydrogen embrittlement according to claim 1 , further comprising one or more selected from the group consisting of, in terms of mass %,

Al: 0.3% or less,

Mg: 0.01% or less,

Ca: 0.01% or less,

REM: 0.10% or less, and

B: 0.008% or less.

3. The austenitic stainless steel having resistance to hydrogen embrittlement according to claim 1 , further comprising one or more selected from the group consisting of, in terms of mass %,

Ti: 0.5% or less,

Nb: 0.5% or less, and

V: 0.5% or less.

4. The austenitic stainless steel having resistance to hydrogen embrittlement according to claim 1 , which is used for a high-pressure hydrogen gas and liquid hydrogen environment.

5. A method for manufacturing the austenitic stainless steel having resistance to hydrogen embrittlement according to claim 1 , the method comprising:

subjecting a semi-finished product having a component composition comprising, in terms of mass %:

C: 0.2% or less;

Si: 0.2% to 1.5%;

Mn: 0.5% to 2.5%;

P: 0.042% or less;

S: 0.008% or less;

Ni: 10.0% to 20.0%;

Cr: 16.0% to 19.1%;

Mo: 3.5% or less;

Cu: 1.52% or less;

N: 0.01% to 0.50%; and

O: 0.015% or less,

with a balance being Fe and unavoidable impurities, to hot working;

performing a final heat treatment at a temperature of 1000° C. to 1200° C.; and

performing cooling after the final heat treatment,

wherein, in the cooling, an average cooling rate until a temperature reaches 750° C. is controlled to be less than 2.0° C./s.

6. The austenitic stainless steel having resistance to hydrogen embrittlement according to claim 2 , further comprising one or more selected from the group consisting of, in terms of mass %,

Ti: 0.5% or less,

Nb: 0.5% or less, and

V: 0.5% or less.

7. The austenitic stainless steel having resistance to hydrogen embrittlement according to claim 2 , which is used for a high-pressure hydrogen gas and liquid hydrogen environment.

8. The austenitic stainless steel having resistance to hydrogen embrittlement according to claim 3 , which is used for a high-pressure hydrogen gas and liquid hydrogen environment.

9. A method for manufacturing the austenitic stainless steel having resistance to hydrogen embrittlement according to claim 2 , the method comprising:

subjecting a semi-finished product having a component composition comprising, in terms of mass %:

C: 0.2% or less;

Si: 0.2% to 1.5%;

Mn: 0.5% to 2.5%;

P: 0.042% or less;

S: 0.008% or less;

Ni: 10.0% to 20.0%;

Cr: 16.0% to 19.1%;

Mo: 3.5% or less;

Cu: 1.52% or less;

N: 0.01% to 0.50%;

O: 0.015% or less; and

one or more selected from the group consisting of, in terms of mass %,

Al: 0.3% or less,

Mg: 0.01% or less,

Ca: 0.01% or less,

REM: 0.10% or less, and

B: 0.008% or less;

with a balance being Fe and unavoidable impurities, to hot working;

performing a final heat treatment at a temperature of 1000° C. to 1200° C.; and

performing cooling after the final heat treatment,

wherein, in the cooling, an average cooling rate until a temperature reaches 750° C. is controlled to be less than 2.0° C./s.

10. A method for manufacturing the austenitic stainless steel having resistance to hydrogen embrittlement according to claim 3 , the method comprising:

subjecting a semi-finished product having a component composition comprising, in terms of mass %:

C: 0.2% or less;

Si: 0.2% to 1.5%;

Mn: 0.5% to 2.5%;

P: 0.042% or less;

S: 0.008% or less;

Ni: 10.0% to 20.0%;

Cr: 16.0% to 19.1%;

Mo: 3.5% or less;

Cu: 1.52% or less;

N: 0.01% to 0.50%;

O: 0.015% or less; and

one or more selected from the group consisting of, in terms of mass %,

Ti: 0.5% or less,

Nb: 0.5% or less, and

V: 0.5% or less;

with a balance being Fe and unavoidable impurities, to hot working;

performing a final heat treatment at a temperature of 1000° C. to 1200° C.; and

performing cooling after the final heat treatment,

wherein, in the cooling, an average cooling rate until a temperature reaches 750° C. is controlled to be less than 2.0° C./s.

Assignments (2)
CHANGE OF NAME Recorded Jul 8, 2021
From: NIPPON STEEL & SUMIKIN STAINLESS STEEL CORPORATION
To: NIPPON STEEL STAINLESS STEEL CORPORATION
Reel/Frame 056805/0030 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 5, 2016
From: MATSUMOTO, KAZUHISA; HATANO, MASAHARU
To: NIPPON STEEL & SUMIKIN STAINLESS STEEL CORPORATION
Reel/Frame 038191/0385 →
Priority Claims (2)
JP JP2015-064951 · Mar 26, 2015 · national
JP JP2016-057076 · Mar 22, 2016 · national
Continuity (1)
Related Publication 20160281187A1 · Sep 29, 2016