IP Library Granted Patent US 9,916,927
Granted Patent B1
US 9,916,927 · App. 15/081,377 · Granted Mar 13, 2018

Thin insulation coatings by sol-gel method

Inventors: Hom Kandel (Tallahassee, FL); Jun Lu (Tallahassee, FL); Youri Viouchkov (Tallahassee, FL); Scott Gundlach (Tallahassee, FL); Adam Voran (Tallahassee, FL); William D. Markiewicz (Monticello, FL)
Assignee: The Florida State University Research Foundation, Inc.
H01F41/127C04B28/24H01F6/06H01F41/048
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Quick Facts
Patent No.
US 9,916,927
App. No.
15/081,377
Granted
Mar 13, 2018
Kind
B1
Abstract

Electrically insulating Al 2 O 3 —SiO 2 thin coatings have been deposited on long-length 316 stainless steel (SS) tape using a reel-to-reel continuous sol-gel dip coating process for co-winding insulation into YBCO pancake coils, a high temperature superconductor magnet technology. Coatings with a thickness of ˜2 μm are achieved after just one dip with a tape withdrawal speed of ˜16 mm/s (1 m/min) and a calcination at 700° C. The coatings were measured to have a room-temperature breakdown voltage of about 100 V, corresponding to a dc dielectric strength of about 50 MV/m. Consequently, this process has low cost and high throughput and produces a thin electrical insulation with excellent thermal, dielectric, and mechanical properties. A new technique has been developed in the coating process to mitigate coating buildup near the edges of the tape.

Claims (11)

1. A coating for a metallic tape or wire, comprising:

a material having a uniform thickness surrounding the metallic tape or wire,

wherein the material comprises:

one part by weight alkyl silicate binding material;

two parts by weight anhydrous ethyl alcohol; and

3/10 part by weight aluminum oxide powder.

2. The coating of claim 1 , wherein the alkyl silicate binding material contains at least 19 percent by weight silicon dioxide.

3. The coating of claim 1 , wherein the aluminum oxide powder has a particle size of about 0.3 μm.

4. The coating of claim 1 , wherein the coating is a silica polymer formed from a sol-gel solution.

5. The coating of claim 1 , wherein the uniform thickness is between 2 μm and 8 μm.

6. The coating of claim 1 , wherein the coating is disposed on a high temperature superconducting material.

Assignments (2)
CONFIRMATORY LICENSE Recorded Nov 8, 2017
From: FLORIDA STATE UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 044412/0901 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 28, 2016
From: KANDEL, HOM; LU, JUN; VIOUCHKOV, YOURI; GUNDLACH, SCOTT; VORAN, ADAM; MARKIEWICZ, WILLIAM D.
To: THE FLORIDA STATE UNIVERSITY RESEARCH FOUNDATION, INC.
Reel/Frame 038109/0174 →
Continuity (2)
Division 14134665 · Dec 19, 2013
Provisional Application 61739304 · Dec 19, 2012