IP Library Granted Patent US 9,822,107
Granted Patent B2
US 9,822,107 · App. 15/105,713 · Granted Nov 21, 2017

Thiazole-substituted aminoheteroaryls as spleen tyrosine kinase inhibitors

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 9,822,107
App. No.
15/105,713
Granted
Nov 21, 2017
Kind
B2
Abstract

The invention provides certain thiazole-substituted aminoheteroaryl compounds of the Formula (I) or pharmaceutically acceptable salts thereof, wherein ring R 1 , R 2 , R 3 , R 4 , ring B, and the subscript r are as defined herein. The invention also provides pharmaceutical compositions comprising such compounds, and methods of using the compounds for treating diseases or conditions mediated by Spleen Tyrosine Kinase (Syk).

Claims (71)

1. A compound of the Formula (I)

or a pharmaceutically acceptable salt thereof, wherein

ring B is selected from the group consisting of indole, quinoline, indazole, and benzimidazole,

R 1 is selected from the group consisting of:

(a) H;

(b) C 1 -C 3 alkyl;

(c) C 1 -C 3 fluoroalkyl;

(d) C 1 -C 3 alkoxy; and

(e) C 3 -C 6 cycloalkyl;

R 2 is selected from the group consisting of H and halo;

R 3 is selected from the group consisting of

(a) H;

(b) C 1 -C 3 alkyl;

(c) C 1 -C 3 alkoxy; and

(d) halo; or

two R 3 when substituted on a common carbon atom together with the carbon atom form a carbonyl;

R 4 is selected from the group consisting of:

ring C y is a mono- or bicyclic carbocyclic ring system containing 4 to 12 carbon atoms;

ring C A is phenyl or C 3 -C 6 cycloalkyl;

R 5 is —C(O)OH;

R 6 is C 1 -C 3 alkyl or halo;

R 7 is H or C 1 -C 3 alkyl;

R 8 is H or F;

the subscript r is 0, 1, 2, 3, or 4;

the subscripts is 0 or 1; and

the subscript t is 0, 1, 2, 3, 4, or 5.

2. The compound of any one of claim 1 or a pharmaceutically acceptable salt thereof, wherein R 1 is selected from the group consisting of H, methyl, —CF 3 , and —CF 2 .

3. The compound of any one of claim 2 or a pharmaceutically acceptable salt thereof, wherein R 1 is —CF 3 or —CF 2 .

4. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein R 2 is H.

5. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein R 3 is H or methyl.

6. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein the moiety in Formula (I)

is selected from the group consisting of:

7. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein R 4 is

8. The compound of claim 7 or a pharmaceutically acceptable salt thereof wherein C y is cyclobutyl or cyclohexyl.

9. The compound of claim 7 or a pharmaceutically acceptable salt thereof, wherein

C y is cyclohexyl;

R 5 is —C(O)OH;

R 6 is methyl;

the subscripts is 1; and

the subscript t is 0, 1, or 2.

10. The compound of claim 8 or a pharmaceutically acceptable salt thereof, wherein

C y is cyclobutyl; and

the subscripts s and t are both 0.

11. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein R 4 is

12. The compound of claim 11 or a pharmaceutically acceptable salt thereof, wherein

C A is cyclohexyl;

R 5 is —C(O)OH;

R 7 is H or methyl;

the subscripts is 1; and

the subscript t is 0, 1, or 2.

13. The compound of claim 1 or a pharmaceutically acceptably salt thereof, wherein the compound is selected from the group consisting of:

(trans)-4-(1-hydroxy-1-(5-(6-((4-(trifluoromethyl)pyrimidin-2-yl)amino)-1H-indol-4-yl)thiazol-2-yl)ethyl)cyclohexanecarboxylic acid;

1-[5-(6-{[4-(trifluoromethyl)pyrimidin-2-yl]amino}-1H-indol-4-yl)-1,3-thiazol-2-yl]cyclobutanol;

4-hydroxy-2,2-dimethyl-4-[5-(6-{[4-(trifluoromethyl)pyrimidin-2-yl]amino}-1H-indol-4-yl)-1,3-thiazol-2-yl]cyclohexanecarboxylic acid;

4-hydroxy-2,2-dimethyl-4-[5-(1-methyl-6-{[4-(trifluoromethyl)pyrimidin-2-yl]amino}-1H-indol-4-yl)-1,3-thiazol-2-yl]cyclohexanecarboxylic acid;

4-hydroxy-2,2-dimethyl-4-(5-(7-((4-(trifluoromethyl)pyrimidin-2-yl)amino)quinolin-4-yl)thiazol-2-yl)cyclohexanecarboxylic acid;

(trans)-1-hydroxy-1-(5-(7-((4-(trifluoromethyl)pyrimidin-2-yl)amino)quinolin-4-yl)thiazol-2-yl)ethyl)cyclohexanecarboxylic acid;

4-hydroxy-2,2-dimethyl-4-(5-(6-((4-(trifluoromethyl)pyrimidin-2-yl)amino)-1H-indol-3-yl)thiazol-2-yl)cyclohexanecarboxylic acid;

(cis)-4-hydroxy-2,2-dimethyl-4-(5-(5-((4-(trifluoromethyl)pyrimidin-2-yl)amino)-1H-indol-3-yl)thiazol-2-yl)cyclohexanecarboxylic acid;

(trans)-4-(1-hydroxy-1-(5-(6-((4-(trifluoromethyl)pyrimidin-2-yl)amino)-1H-indol-3-yl)thiazol-2-yl)ethyl)cyclohexanecarboxylic acid;

(cis) 4-hydroxy-4-(5-(5-((4-(trifluoromethyl)pyrimidin-2-yl)amino)-1H-indol-3-yl)thiazol-2-yl)cyclohexanecarboxylic acid;

(cis)-4-(5-(5-((4-(difluoromethyl)pyrimidin-2-yl)amino)-1H-indol-3-yl)thiazol-2-yl)-4-hydroxycyclohexanecarboxylic acid;

4-[2-(1-hydroxycyclobutyl)-1,3-thiazol-5-yl]-6-{[4-(trifluoromethyl)pyrimidin-2-yl]amino}-1,3-dihydro-2H-benzimidazol-2-one;

4-hydroxy-2,2-dimethyl-4-[5-(5-{[4-(trifluoromethyl)pyrimidin-2-yl]amino}-1H-indazol-7-yl)-1,3-thiazol-2-yl]cyclohexanecarboxylic acid;

(trans)-4-(1-hydroxy-1-[5-(5-{[4-(trifluoromethyl)pyrimidin-2-yl]amino-1H-indazol-7-yl)-1,3-thiazol-2-yl]ethyl}-2,2-dimethylcyclohexanecarboxylic acid;

(trans)-4-(1-hydroxy-1-[5-(5-{[4-(trifluoromethyl)pyrimidin-2-yl]amino}-1H-indazol-7-yl)-1,3-thiazol-2-yl]ethyl}cyclohexanecarboxylic acid;

(trans)-4-(1-hydroxy-1-(5-(6-((4-(trifluoromethyl)pyrimidin-2-yl)amino)-1H-indazol-4-yl)thiazol-2-yl)ethyl)cyclohexanecarboxylic acid; and

(trans)-4-(1-hydroxy-1-(5-(6-((4-(trifluoromethyl)pyrimidin-2-yl)amino)-1H-benzo[d]imidazol-4-yl)thiazol-2-yl)ethyl)cyclohexanecarboxylic acid;

or a pharmaceutically acceptable salt thereof.

14. A pharmaceutical composition comprising the compound of claim 1 or a pharmaceutically acceptable salt thereof and a pharmaceutically acceptable carrier.

15. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein the compound is 4-hydroxy-2,2-dimethyl-4-(5-(7-((4-(trifluoromethyl)pyrimidin-2-yl)amino)quinolin-4-yl)thiazol-2-yl)cyclohexanecarboxylic acid.

Assignments (3)
MERGER Recorded Aug 8, 2022
From: MERCK SHARP & DOHME CORP.
To: MERCK SHARP & DOHME LLC
Reel/Frame 061102/0145 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 17, 2017
From: ROBICHAUD, JOEL S.; GAUTHIER, JACQUES YVES; FOURNIER, JEAN-FRANCOIS
To: MERCK CANADA INC.
Reel/Frame 043320/0406 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 22, 2017
From: ANDRESEN, BRIAN M.; ARRINGTON, KENNETH L.; OTTE, RYAN D.; ELLIS, JOHN MICHAEL; BUTCHER, JOHN W.; NORTHRUP, ALAN B.
To: MERCK SHARP & DOHME CORP.
Reel/Frame 041331/0289 →