IP Library › Granted Patent US 10,254,257
Granted Patent B2
US 10,254,257 · App. 15/107,337 · Granted Apr 9, 2019

ESD protected tubing for removing charge from lumen

Inventors: Tony Ziegler (Steinfeld, DE); Stefan Falk-Jordan (Karlsruhe, DE)
Assignee: Agilent Technologies, Inc.
G01N30/6052B01D15/24F16L11/127G01N30/74G01N30/80G01N2030/027
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Quick Facts
Patent No.
US 10,254,257
App. No.
15/107,337
Granted
Apr 9, 2019
Kind
B2
Abstract

An electrostatic discharge protected device for conducting a fluid through at least one lumen includes a tubing having a hollow interior defining the at least one lumen. The tubing includes an electrically conductive section configured for conducting electric charge, generated within the at least one lumen when the fluid flows through the at least one lumen, away from the at least one lumen.

Claims (43)

1. An electrostatic discharge protected device for conducting a fluid through at least one lumen, wherein the device comprises:

a tubing having a hollow interior defining the at least one lumen;

wherein the tubing comprises an outer electrically conductive section configured for conducting electric charge, generated within the at least one lumen when the fluid flows through the at least one lumen, away from the at least one lumen,

wherein the tubing comprises an interior inert section delimiting the entire lumen, the interior inert section forming an intermediate structure separating the at least one lumen from the electrically conductive section, preventing direct contact between the fluid and the electrically conductive section, and configured to conduct electric charge therethrough to the outer electrical section.

2. The device of claim 1 , wherein the outer electrically conductive section extends to an outer surface of the tuning so that the electric charge is conducted away from the at least one lumen through at least one part of a wall of the tubing.

3. The device of claim 1 , wherein the inert section is configured for electrically conducting the generated electric charge from the at least one lumen through the intermediate structure and towards the electrically conductive section.

4. The device of claim 1 , wherein the inert section has, at least at a portion where the chemically inert section is surrounded by the electrically conductive section, a radial thickness (D) in a range between 0.05 mm and 0.4 mm.

5. The device of claim 1 , wherein the tubing has a circular or a polygonal outer circumference.

6. The device of claim 1 , comprising at least one of the following features:

at least the part of the material of the tubing which is in direct contact with the fluid conducted through the at least one lumen is chemically inert against a non-polar solvent to be conducted as at least part of the fluid through the at least one lumen;

the electrically conductive section is integrated or embedded within a wall of the tubing;

the device comprises a ground connector configured to be connected to the electrically conductive section for discharging the electrostatic charge towards ground;

the device comprises an electrically conductive fitting system for mechanically coupling the device to a grounded housing and simultaneously electrically coupling the electrically conductive section to the grounded housing;

an external diameter (L) of the tubing is smaller than 8 mm;

a thickness (d) of a wall of the tubing is in a range between 0.3 mm and 1.5 mm;

the electrically conductive section has a value of the ohmic resistance per length of the tubing of less than 2 MΩ/m.

7. The device of claim 1 , wherein the interior inert section of the tubing comprises a bioinert material which suppresses fluid dissolution of metal components out from a wall of the tubing.

8. The device of claim 1 , wherein the electrically conductive section is configured as an axially extending annular segment of the tubing.

9. The device of claim 8 , wherein the annular segment extends over an annular range (α) of angular degrees ranging between 30° and 180°.

10. A fluid separation apparatus for separating a fluidic sample into a plurality of fractions, the apparatus comprising:

a fluid drive unit configured for driving a fluid comprising a mobile phase and the fluidic sample in the mobile phase along a fluidic path;

a separation unit arranged within the fluidic path and configured for separating the fluidic sample into the plurality of fractions;

a device according to claim 1 for conducting the fluid along at least a portion of the fluidic path.

11. The fluid separation apparatus of claim 10 , further comprising at least one of:

a detector configured to detect separated fractions of the fluidic sample;

a fractioner unit configured to collect separated fractions of the fluidic sample;

a data processing unit configured to process data received from the fluid separation apparatus;

a degassing apparatus for degassing the mobile phase.

12. A method of implementing a device according to claim 1 as a fluidic connection downstream of a flow cell of a liquid chromatography apparatus.

13. The method of claim 12 , wherein the device is implemented as fluidic connection between the flow cell and a fractioner of the liquid chromatography apparatus.

14. The device of claim 1 , wherein the tubing comprises an optically transparent section at least in one or more portions of the tubing, thereby enabling an external inspection of the conducted fluid within the at least one lumen.

15. The device of claim 14 , wherein the entire lumen is delimited by the optically transparent section, and wherein the electrically conductive section is arranged to surround part of the optically transparent section so that the electric charge is at least partially electrically conducted from the at least one lumen via the optically transparent section to the electrically conductive section.

16. The device of claim 14 , further comprising a light source configured for generating primary optical light for propagation through a first part of the optically transparent section, the at least one lumen, and a second part of the optically transparent section, and further comprising a light detector arranged for detecting secondary optical light being transmitted through the fluid upon being irradiated with the primary optical light.

17. The device of claim 14 , wherein at least one of the group consisting of the chemically inert section and the optically transparent section.

18. A method of conducting a fluid, in particular a non-polar fluid, through at least one lumen with electrostatic discharge protection, wherein the method comprises:

conducting the fluid through a hollow interior of a tubing defining the at least one lumen;

conducting electric charge, generated within the at least one lumen when the fluid flows through the at least one lumen, away from the at least one lumen by an outer electrically conductive section of the tubing,

wherein the tubing comprises an interior inert section delimiting the entire lumen, the interior inert section forming an intermediate structure separating the at least one lumen from the electrically conductive section, preventing direct contact between the fluid and the electrically conductive section, and configured to conduct electric charge therethrough to the outer electrical section.

19. The method of claim 18 , comprising at least one of the following features:

the electric charge is conducted away from the at least one lumen through at least a part of a wall of the tubing;

the fluid comprises or consists of a non-polar solvent;

the generated electric charge is conducted from the at least one lumen through the intermediate structure and towards the electrically conductive section.

20. The method of claim 18 , wherein the interior inert section of the tubing comprises a bioinert material which suppresses fluid dissolution of metal components out from a wall of the tubing.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 22, 2016
From: ZIEGLER, TONY; FALK-JORDAN, STEFAN
To: AGILENT TECHNOLOGIES, INC.
Reel/Frame 038987/0455 →
Continuity (1)
Related Publication 20170003256A1 · Jan 5, 2017