IP Library Granted Patent US 10,392,312
Granted Patent B2
US 10,392,312 · App. 15/110,523 · Granted Aug 27, 2019

Silicon oxycarbide environmental barrier coating

Inventors: Xia Tang (West Hartford, CT); Paul Sheedy (Bolton, CT); Tania Bhatia Kashyap (West Hartford, CT); Wayde R. Schmidt (Pomfret Center, CT); Daniel G. Goberman (East Granby, CT)
Assignee: United Technologies Corporation
C04B41/87B32B9/005C04B35/14C04B35/195C04B35/5603B32B2255/20B32B2264/102B32B2307/308B32B2307/7265
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Quick Facts
Patent No.
US 10,392,312
App. No.
15/110,523
Granted
Aug 27, 2019
Kind
B2
Abstract

An article includes a ceramic-based substrate and a barrier layer on the ceramic-based substrate. The barrier layer includes a matrix of barium-magnesium alumino-silicate or SiO 2 , a dispersion of silicon oxycarbide particles in the matrix, and a dispersion of particles, of the other of barium-magnesium alumino-silicate or SiO 2 , in the matrix.

Claims (23)

1. An article comprising:

a ceramic-based substrate;

a barrier layer on the ceramic-based substrate, the barrier layer including a matrix of barium-magnesium alumino-silicate or SiO 2 , a dispersion of silicon oxycarbide particles in the matrix, the silicon oxycarbide particles having Si, O, and C in a covalently bonded network, and a dispersion of particles, of the other of barium-magnesium alumino-silicate or SiO 2 , in the matrix; and

a distinct intermediate layer between the barrier layer and the ceramic-based substrate, the distinct intermediate layer including an intermediate layer matrix of SiO 2 and a dispersion of intermediate layer silicon oxycarbide particles in the intermediate layer matrix.

2. The article as recited in claim 1 , wherein the barrier layer includes, by volume, 1-30% of the barium-magnesium alumino-silicate particles.

3. The article as recited in claim 1 , wherein the barrier layer includes, by volume, 30-94% of the silicon oxycarbide particles.

4. The article as recited in claim 1 , wherein the barrier layer includes, by volume, 5-40% of the matrix of SiO 2 .

5. The article as recited in claim 1 , wherein the barrier layer includes, by volume, 1-30% of the barium-magnesium alumino-silicate particles, 5-40% of the matrix of SiO 2 , and a balance of the silicon oxycarbide particles.

6. The article as recited in claim 5 , wherein the barrier layer includes, by volume, 1-5% of the barium-magnesium alumino-silicate particles.

7. The article as recited in claim 1 , wherein the silicon oxycarbide particles in the barrier layer have an average maximum dimension D 1 and the intermediate layer silicon oxycarbide particles in the distinct intermediate layer have an average maximum dimension D 2 , and D 2 is less than D 1 .

8. The article as recited in claim 1 , wherein the distinct intermediate layer includes, by volume, 5-40% of the intermediate layer matrix of SiO 2 and a balance of the dispersion of the intermediate layer silicon oxycarbide particles.

9. The article as recited in claim 1 , wherein the matrix of SiO 2 is continuous.

10. The article as recited in claim 1 , wherein the silicon oxycarbide particles have a composition SiO x M z C y , where M is at least one metal, x<2, y>0 and z<1 and x and z are non-zero.

11. The article as recited in claim 1 , wherein the silicon oxycarbide particles have an average maximum dimension of 1-75 micrometers.

12. The article as recited in claim 1 , further comprising a ceramic-based top coat on the barrier layer.

13. The article as recited in claim 1 , wherein the barrier layer consists of the matrix of SiO 2 , the dispersion of the silicon oxycarbide particles in the matrix, and the dispersion of the barium-magnesium alumino-silicate particles in the matrix.

14. A composite material comprising:

a matrix of barium-magnesium alumino-silicate or SiO 2 ;

a dispersion of silicon oxycarbide particles in the matrix, the silicon oxycarbide particles having Si, O, and C in a covalently bonded network; and

a dispersion of particles, of the other of barium-magnesium alumino-silicate or SiO 2 , in the matrix.

15. The composite material as recited in claim 14 , including, by volume, 1-30% of the barium-magnesium alumino-silicate particles, 5-40% of the matrix of SiO 2 , and a balance of the silicon oxycarbide particles.

16. The composite material as recited in claim 15 , including, by volume, 1-5% of the barium-magnesium alumino-silicate particles.

17. The composite material as recited in claim 14 , wherein the matrix of SiO 2 is continuous.

Assignments (4)
CHANGE OF NAME Recorded Jul 27, 2023
From: RAYTHEON TECHNOLOGIES CORPORATION
To: RTX CORPORATION
Reel/Frame 064714/0001 →
CORRECTIVE ASSIGNMENT TO CORRECT THE AND REMOVE PATENT APPLICATION NUMBER 11886281 AND ADD PATENT APPLICATION NUMBER 14846874. TO CORRECT THE RECEIVING PARTY ADDRESS PREVIOUSLY RECORDED AT REEL: 054062 FRAME: 0001. ASSIGNOR(S) HEREBY CONFIRMS THE CHANGE OF ADDRESS. Recorded Mar 4, 2021
From: UNITED TECHNOLOGIES CORPORATION
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 055659/0001 →
CHANGE OF NAME Recorded Sep 4, 2020
From: UNITED TECHNOLOGIES CORPORATION
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 054062/0001 →
CONFIRMATORY LICENSE Recorded Aug 13, 2018
From: UNITED TECHNOLOGIES CORPORATION
To: NAVY, SECRETARY OF THE UNITED STATES OF AMERICA
Reel/Frame 046785/0846 →
Continuity (2)
Provisional Application 61927101 · Jan 14, 2014
Related Publication 20160332922A1 · Nov 17, 2016
Cited By (3)
US 12,234,194 US 12,311,574 US 12,428,348