IP Library Granted Patent US 9,663,527
Granted Patent B2
US 9,663,527 · App. 15/116,659 · Granted May 30, 2017

Factor XIa inhibitors

Inventors: Santhosh F. Neelamkavil (Edison, NJ); Scott D. Edmondson (Clark, NJ); Zhuyan Guo (Scotch Plains, NJ); Alan W. Hruza (Hackettstown, NJ); Zahid Hussain (Dayton, NJ); Charles A. Lesburg (Newton, MA); Remond Moningka (Jersey City, NJ); Anthony K. Ogawa (New Providence, NJ); Rudrajit Mal (Piscataway, NJ)
Assignee: MERCK SHARP & DOHME CORP.
C07D487/08C07D471/08
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Quick Facts
Patent No.
US 9,663,527
App. No.
15/116,659
Granted
May 30, 2017
Kind
B2
Abstract

The present invention provides a compound of Formula (I) and pharmaceutical compositions comprising one or more said compounds, and methods for using said compounds for treating or preventing thromboses, embolisms, hypercoagulability or fibrotic changes. The compounds are selective Factor XIa inhibitors or dual inhibitors of Factor XIa and plasma kallikrein.

Claims (31)

1. A compound of the formula:

wherein

is heteroaryl, which is optionally substituted with one to three groups independently selected from the group consisting of halo, methyl and cyano;

Z is CH 2 , C═O or CHC(O)OH;

R 1 is hydrogen, C 1-6 alkyl, C 3-6 cycloalkyl, halo, cyano or hydroxy, wherein said alkyl and cycloalkyl groups are optionally substituted with one to three groups independently selected from the group consisting of halo and hydroxy;

each R 2 is independently selected from the group consisting of halo, cyano, hydroxy, OR 3 , C 1-6 alkyl, CO 2 H, CO 2 R 3 , (R 3 )CO 2 H, (R 3 )CO 2 R 4 , NR 5 R 6 , (R 3 )NR 5 R 6 , NHCOR 3 , NHC(O)OR 3 , NHCO 2 (R 3 )OR 4 , NHCO 2 (R 3 )CO 2 H, (R 3 )NHCO 2 R 4 , NHCONR 5 R 6 , NHSO 2 R 3 , CONR 5 R 6 , CH 2 CONR 5 R 6 and NHCONH(R 3 )heterocyclyl;

R 3 is hydrogen or C 1-6 alkyl, wherein said alkyl is optionally substituted with hydroxy or one to three halo;

R 4 is hydrogen or C 1-6 alkyl, wherein said alkyl is optionally substituted with one to three halo;

R 5 is hydrogen or C 1-6 alkyl,

R 6 is hydrogen or C 1-6 alkyl,

R 7 is hydrogen or C 1-6 alkyl, CO 2 H, COR 3 , CONR 5 R 6 , wherein said alkyl is optionally substituted with one to three halo;

x is an integer between zero and three;

y is an integer between zero and three;

z is an integer between zero and three;

or a pharmaceutically acceptable salt thereof.

2. The compound of claim 1 wherein

is a nitrogen-containing heteroaryl, which is optionally substituted with one to three groups independently selected from the group consisting of halo, methyl and cyano; or a pharmaceutically acceptable salt thereof.

3. The compound of claim 1 wherein

is a selected from the group consisting of pyrrolyl, pyrazolyl, imidazolyl, triazolyl, pyridinyl, pyridazinyl, pyrimidinyl, pyrazinyl and triazinyl, wherein said groups are optionally substituted with one to three groups independently selected from the group consisting of halo, methyl and cyano; or a pharmaceutically acceptable salt thereof.

4. The compound of claim 1 wherein R 1 is hydrogen; or a pharmaceutically acceptable salt thereof.

5. The compound of claim 1 wherein R 2 is NHC(O)OR 3 ; or a pharmaceutically acceptable salt thereof.

6. The compound of claim 1 wherein x is 1; or a pharmaceutically acceptable salt thereof.

7. The compound of claim 1 selected from:

8. A pharmaceutical composition comprising a compound of claim 1 and a pharmaceutically acceptable carrier.

9. A method for inhibiting thrombus formation in blood or treating thrombus formation in blood comprising administering a composition of claim 8 to a mammal in need of thereof.

10. A method for preventing thrombus formation in blood comprising administering a composition of claim 8 to a mammal in need thereof.

11. A method of treating venous thromboembolism and pulmonary embolism in a mammal comprising administering a composition of claim 8 to a mammal in need thereof.

12. A method of treating deep vein thrombosis in a mammal comprising administering a composition of claim 8 to a mammal in need thereof.

13. A method of treating thromboembolic stroke in a human comprising administering a composition of claim 8 to a human in need thereof.

14. The compound of claim 1 which is

or a pharmaceutically acceptable salt thereof.

Assignments (2)
MERGER Recorded Aug 8, 2022
From: MERCK SHARP & DOHME CORP.
To: MERCK SHARP & DOHME LLC
Reel/Frame 061102/0145 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 4, 2016
From: NEELAMKAVIL, SANTHOSH F.; EDMONDSON, SCOTT D.; GUO, ZHUYAN; HRUZA, ALAN W.; HUSSAIN, ZAHID; LESBURG, CHARLES A.; MONINGKA, REMOND; OGAWA, ANTHONY K.; MAL, RUDRAJIT
To: MERCK SHARP & DOHME CORP.
Reel/Frame 039344/0694 →
Continuity (2)
Provisional Application 61938230 · Feb 11, 2014
Related Publication 20160347757A1 · Dec 1, 2016