IP Library Granted Patent US 10,940,217
Granted Patent B2
US 10,940,217 · App. 15/126,103 · Granted Mar 9, 2021

Polyphosphazene delivery system for inorganic nanocrystals

Inventors: David Peter Cormode (Philadelphia, PA); Peter Chhour (Wayne, PA); Andrew Tsourkas (Bryn Mawr, PA); Harry Allcock (State College, PA); Rabe'e Cheheltani (Philadelphia, PA)
Assignees: The Trustees Of The University Of Pennsylvania; The Penn State Research Foundation
A61K49/1809A61B18/04A61B18/18A61K9/1075A61K9/5146A61K38/385A61K41/0023A61K41/0038A61K49/0067A61K49/0082A61K49/0428A61K49/0466A61K49/1857A61N5/10A61B2018/00577A61N2005/1098
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Quick Facts
Patent No.
US 10,940,217
App. No.
15/126,103
Granted
Mar 9, 2021
Kind
B2
Abstract

Nanoclusters comprising inorganic nanocrystals and a biodegradable polymer are disclosed. The inorganic nanocrystals have a mean particle size of 1 to 500 nm. The inorganic nanocrystals are contained within a core of the nanoclusters, on the surface of the nanoclusters, contained within a core of the nanoclusters, dispersed throughout the nanoclusters, or a combination thereof. The biodegradable polymer allows the inorganic nanocrystals to be excreted renally over a period of time. The nanoclusters can be used for medical imaging or other biomedical applications.

Claims (23)

1. A nanocluster comprising:

a plurality of hydrophilic inorganic nanocrystals, each comprising:

a gold nanocrystal having a mean size of about 5 nm or less; and

a first hydrophilic ligand coating selected from the group consisting of: 11-mercaptoundecanoic acid, glutathione and citrate;

a hydrophilic biodegradable polymer encapsulating the plurality of hydrophilic inorganic nanocrystals, wherein:

the hydrophilic biodegradable polymer is adapted to degrade over time by hydrolysis; and

the hydrophilic biodegradable polymer is polyphosphazene; and

a second ligand coating the surface of the hydrophilic biodegradable polymer, wherein the second ligand is PEG;

wherein the nanocluster has a mean size in the range of from about 10 nm to about 300 nm.

2. The nanocluster according to claim 1 , wherein the polyphosphazene is selected from the group consisting of poly(bis(4-carboxyphenoxy)phosphazene) (PCPP) and poly(carboxylatophenoxy)(glycinato) polyphosphazenes (PCGPPs).

3. The nanocluster according to claim 1 , wherein the polymer is crosslinked.

4. The nanocluster according to claim 3 , wherein the polymer is crosslinked with spermine.

5. The nanocluster according to claim 1 , wherein the plurality of hydrophilic inorganic nanocrystals are positioned on a surface of the polymer.

6. The nanocluster according to claim 1 , further comprising a drug contained on the surface of the nanocluster, contained within the core of the nanocluster, dispersed throughout the nanocluster, or a combination thereof.

7. A method comprising:

administering to a patient a plurality of nanoclusters according to claim 1 ; and

imaging the patient with x-ray imaging, computed tomography (CT), magnetic resonance imaging (MRI), photoacoustic imaging, fluorescence, or fluoroscopy.

8. A method for enhancing the effect of radiation therapy, comprising:

administering to a patient a plurality of nanoclusters according to claim 1 ; and

treating the patient with radiation at a targeted site, wherein the plurality of nanoclusters increase the amount of radiation absorbed at the targeted site.

9. A method for ablating tissue, comprising:

administering to a patient a plurality of nanoclusters according to claim 1 ; and

treating the patient with electromagnetic radiation at a targeted site, wherein the plurality of nanoclusters absorb the electromagnetic radiation and convert the electromagnetic radiation to heat to ablate the tissue at the targeted site.

Assignments (4)
CONFIRMATORY LICENSE Recorded Dec 7, 2017
From: UNIVERSITY OF PENNSYLVANIA
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 044752/0989 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 22, 2017
From: THE TRUSTEES OF THE UNIVERSITY OF PENNSYLVANIA
To: PENN STATE RESEARCH FOUNDATION
Reel/Frame 043664/0009 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 14, 2017
From: ALLCOCK, HARRY R.
To: THE PENN STATE RESEARCH FOUNDATION
Reel/Frame 041567/0894 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 26, 2017
From: CORMODE, DAVID PETER; CHHOUR, PETER; TSOURKAS, ANDREW; ALLCOCK, HARRY R.; CHEHELTANI, RABEE
To: THE TRUSTEES OF THE UNIVERSITY OF PENNSYLVANIA
Reel/Frame 041093/0847 →
Continuity (2)
Provisional Application 61954791 · Mar 18, 2014
Related Publication 20170000910A1 · Jan 5, 2017
Cited By (1)
US 12,245,355