IP Library Granted Patent US 10,259,158
Granted Patent B2
US 10,259,158 · App. 15/130,261 · Granted Apr 16, 2019

Method and apparatus for fabricating ceramic and metal components via additive manufacturing with uniform layered radiation drying

Inventors: Ming C Leu (Rolla, MO); Amir Ghazanfari (Rolla, MO); Wenbin Li (Rolla, MO); Gregory E. Hilmas (Rolla, MO); Robert G Landers (Rolla, MO)
Assignee: The Curators of the University of Missouri
B29C64/106B28B1/001B29C64/124B29C64/188B33Y10/00B33Y30/00B33Y50/02
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Quick Facts
Patent No.
US 10,259,158
App. No.
15/130,261
Granted
Apr 16, 2019
Kind
B2
Abstract

A freeform extrusion fabrication process for producing three-dimensional ceramic, metal and functionally gradient composite objects, including the steps of filling a plurality of paste sources with a respective plurality of aqueous paste compositions, operationally connecting respective syringes containing respective aqueous paste compositions to a mixing chamber, moving a first aqueous paste composition from a first respective paste source into the mixing chamber, moving a second aqueous paste composition from a second respective paste source into the mixing chamber, mixing the first and second aqueous paste compositions to define a first admixture having a first admixture composition, extruding the first admixture onto a surface to define an extruded layer having a first admixture composition, surrounding the sides of the extruded layer with an oil bath, radiatively drying the extruded layer.

Claims (20)

1. A multilayered extrusion fabrication process for producing three-dimensional ceramic and metal objects, comprising:

a) preparing an aqueous paste;

b) extruding the aqueous paste onto a target surface in an oil tank to define an extruded layer having a top surface and at least one side surface;

c) filling the oil tank with sufficient oil to submerge the at least one side surface of the extruded layer in oil;

d) uniformly drying the extruded layer with an application of thermal energy through the top surface remove moisture contained therein; and

e) repeating steps b) through d) to define a green body made of a plurality of stacked, dried layers.

2. A multilayered extrusion fabrication process for producing three-dimensional compositionally gradient ceramic and metal objects, comprising:

a) preparing an aqueous paste, wherein the aqueous paste has a first composition;

b) extruding the aqueous paste onto a target surface in a liquid tank to define an extruded layer having a top surface and at least one side surface;

c) filling the liquid tank with sufficient oil to cover the at least one side surface of the extruded layer in liquid while leaving the top surface liquid-free;

d) heating the extruded layer to remove moisture through the top surface to yield a dried layer;

e) changing the composition of the aqueous paste to a second composition; and

f) repeating steps b) through e) to define a green body made of a plurality of stacked dried layers.

3. The process of claim 2 , wherein steps b) and e) occur simultaneously.

4. The process of claim 2 and further comprising:

g) draining liquid from the liquid tank; and

h) drying the green body to remove residual moisture.

5. The process of claim 2 wherein the second composition is different from the first composition.

6. The process of claim 2 wherein the green body is less than four volume percent binder.

7. The process of claim 2 wherein the green body is less than one volume percent binder.

Assignments (2)
CONFIRMATORY LICENSE Recorded Jan 28, 2019
From: MISSOURI UNIVERSITY/SCIENCE & TECHNOLOGY
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 048150/0260 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 20, 2018
From: LEU, MING C.; GHAZANFARI, AMIR; LI, WENBIN; HILMAS, GREGORY E.; LANDERS, ROBERT G.
To: THE CURATORS OF THE UNIVERSITY OF MISSOURI
Reel/Frame 044973/0960 →
Continuity (1)
Related Publication 20170297221A1 · Oct 19, 2017
Cited By (1)
US 12,429,848