IP Library Granted Patent US 10,351,498
Granted Patent B2
US 10,351,498 · App. 15/141,553 · Granted Jul 16, 2019

Process for generating hemp oil with a high cannabidiol (CBD) content

Inventors: Michael J. Mona (San Diego, CA); Joshua A. Hartsel (San Diego, CA); Greg Waterbury (San Diego, CA)
Assignee: CV SCIENCES, INC.
C07C37/50B01D3/106B01D3/148C07C37/70C07C37/74C07D311/80C11B3/00C11B3/001C11B3/12B65D73/0092B65D75/367C07C2601/16
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Quick Facts
Patent No.
US 10,351,498
App. No.
15/141,553
Granted
Jul 16, 2019
Kind
B2
Abstract

A method for producing hemp oil, comprising decarboxylation of CBDA in hemp oil; short-path evaporation of CBD from the decarboxylated hemp oil to produce CBD oil; selective THC to CBN conversion performed on the decarboxylated hemp oil.

Claims (15)

1. A method for producing hemp oil, comprising:

decarboxylation of CBDA in hemp oil;

evaporation of CBD from the decarboxylated hemp oil to produce CBD oil; and

a selective THC to CBN conversion performed on the decarboxylated hemp oil.

2. The method of claim 1 , wherein decarboxylation of CBDA in hemp oil comprises:

starting with virgin CO2 extracted hemp oil that has been extracted from the whole plant;

decarboxylating the virgin CO2 extracted hemp oil by heating to 140-160° C. for 10-18 hours to convert the CBDA to CBD.

3. The method of claim 2 , wherein upon reaching about 140-160° C., mixing the resultant solution and then lowering the temperature to between about 75-90° C.

4. The method of claim 1 , wherein the evaporation of CBD from the decarboxylated hemp oil to produce CBD oil comprises isolating the CBD from a crude decarboxylated CO2 extract generated by decarboxylation of CBDA in hemp oil using two sequential evaporation steps, and wherein the first step comprises:

placing decarboxylated hemp oil in a feed tank of a first evaporator;

setting the feed tank heater to between about 90-150° C. and allowing the decarboxylated hemp oil to fully melt;

maintaining a vacuum of at least 0.5 torr to 0.08 torr with primary vacuum pump.

5. The method of claim 1 , wherein the evaporator # 1 is set to 250-275° C. with a feed rate of 2-3.5 Hz from a feed tank pump.

6. The method of claim 5 , wherein the second step comprises using a second evaporator to refine the CBD to maximum purity.

7. The method of claim 6 , wherein the second evaporator is set to 160-175° C. and is equipped with an additional diffusion pump capable of achieving an ultimate vacuum of 0.5-0.005 torr. Evaporator # 2 is fed at a rate consistent with the output of the residue from evaporator # 1 .

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 20, 2019
From: MONA, MICHAEL J., III
To: CV SCIENCES, INC.
Reel/Frame 049234/0964 →
CHANGE OF NAME Recorded Oct 10, 2016
From: CANNAVEST CORP.
To: CV SCIENCES, INC.
Reel/Frame 040300/0425 →
EMPLOYMENT AGREEMENT Recorded Oct 10, 2016
From: HARTSEL, JOSHUA A.
To: CANNAVEST CORP.
Reel/Frame 040482/0789 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 10, 2016
From: MONA, MICHAEL J., III
To: CANNAVEST CORP.
Reel/Frame 039980/0220 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 10, 2016
From: WATERBURY, GREG
To: CANNAVEST CORP.
Reel/Frame 039980/0222 →
Continuity (3)
Continuation 14791184 · Jul 2, 2015
Provisional Application 62020053 · Jul 2, 2014
Related Publication 20170022132A1 · Jan 26, 2017