IP Library Granted Patent US 10,096,734
Granted Patent B2
US 10,096,734 · App. 15/150,824 · Granted Oct 9, 2018

Methods of forming colloidal nanocrystal-based thin film devices

Inventors: Cherie R. Kagan (Bala-Cynwyd, PA); Aaron T. Fafarman (Philadelphia, PA); Ji-Hyuk Choi (Philadelphia, PA); Weon-Kyu Koh (Los Alamos, NM); David K. Kim (Lincoln, MA); Soong Ju Oh (Philadelphia, PA); Yuming Lai (Philadelphia, PA); Sung-Hoon Hong (Daejeon, KR); Sangameshwar Rao Saudari (Fishkill, NY); Christopher B. Murray (Bala Cynwyd, PA)
Assignee: The Trustees of the University of Pennsylvania
H01L31/07B82Y10/00B82Y40/00H01B1/06H01L29/0665H01L29/22H01L29/2203H01L29/24H01L29/413H01L29/45H01L29/4908H01L29/66969H01L29/78603H01L29/78681H01L31/0324H01L31/18B82Y20/00H01L29/127H01L29/18Y02E10/50Y10S977/891Y10S977/938Y10S977/954
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Quick Facts
Patent No.
US 10,096,734
App. No.
15/150,824
Granted
Oct 9, 2018
Kind
B2
Abstract

Methods of forming colloidal nanocrystal (NC)-based thin film devicesare disclosed. The methods include the steps of depositing a dispersion of NCs on a substrate to form a NC thin-film, wherein at least a portion of the NCs is capped with chalcogenocyanate (xCN)-based ligands; and doping the NC thin-film with a metal.

Claims (27)

1. A method of forming colloidal nanocrystal (NC)-based thin film devices, the method comprising the steps of:

depositing a dispersion of NCs on a substrate to form a NC thin-film, wherein at least a portion of the NCs is capped with chalcogenocyanate (xCN)-based ligands; and

doping the NC thin-film with a metal.

2. The method of claim 1 , wherein the doping step comprises evaporation and thermal diffusion.

3. The method of claim 1 , wherein the metal is at least one of indium-based, lead-based, tin-based, gallium-based or selenium-based.

4. The method of claim 1 , wherein the doping step occurs at about room temperature.

5. The method of claim 1 , wherein the doping step is initiated by annealing.

6. The method of claim 1 , wherein the doping step comprises blanket deposition.

7. The method of claim 1 , wherein the NCs are at least one of cadmium-based, lead-based, zinc-based, or bismuth-based.

8. The method of claim 1 , wherein the substrate is flexible.

9. The method of claim 1 , wherein the metal is patterned on the NC thin film device.

10. The method of claim 1 , further comprising depositing one or more additional layer of NCs on the previously deposited layer of NCs.

11. A method of forming colloidal nanocrystal (NC)-based thin film devices, the method comprising the step of:

depositing a dispersion of NCs on a substrate to form a NC thin-film, wherein at least a portion of the NCs is capped with chalcogenocyanate (xCN)-based ligands.

12. The method of claim 11 , wherein the NCs are at least one of cadmium-based, lead-based, zinc-based, or bismuth-based.

13. The method of claim 11 , wherein the substrate is flexible.

14. A method of forming colloidal nanocrystal (NC)-based thin film devices, the method comprising the steps of:

depositing a dispersion of NCs on a substrate; and

doping the NC thin film with a metal by evaporation and thermal diffusion to form a NC-based thin film device.

15. The method of claim 14 , wherein at least a portion of the NCs is capped with chalcogenocyanate (xCN)-based ligands.

16. The method of claim 14 , wherein the doping step comprises annealing the NC thin film with a metal, thereby diffusing a portion of the metal into the NC thin film.

17. The method of claim 14 , wherein the metal is at least one of indium-based, lead-based, or selenium-based.

18. The method of claim 14 , wherein the deposited NC thin-film is doped at about room temperature.

19. The method of claim 14 , wherein the deposited NC thin film is doped by annealing.

20. The method of claim 14 , wherein the NCs are at least one of cadmium-based, lead-based, zinc-based, or bismuth-based.

21. The method of claim 14 , wherein the substrate is flexible.

22. The method of claim 14 , wherein the metal is patterned on the NC thin film device.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 14, 2018
From: KAGAN, CHERIE R.; FAFARMAN, AARON T.; CHOI, JI-HYUK; KOH, WEON-KYU; KIM, DAVID K.; OH, SOONG JU; LAI, YUMING; HONG, SUNG-HOON; SAUDARI, SANGAMESHWAR RAO; MURRAY, CHRISTOPHER B.
To: THE TRUSTEES OF THE UNIVERSITY OF PENNSYLVANIA
Reel/Frame 047501/0972 →
CONFIRMATORY LICENSE Recorded Oct 15, 2018
From: PENNSYLVANIA, UNIVERSITY OF
To: NAVY, SECRETARY OF THE UNITED STATES OF AMERICA
Reel/Frame 047261/0748 →
CONFIRMATORY LICENSE Recorded Apr 14, 2017
From: UNIVERSITY OF PENNSYLVANIA
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 042257/0641 →
Continuity (4)
Division 13969863 · Aug 19, 2013
Provisional Application 61754248 · Jan 18, 2013
Provisional Application 61684425 · Aug 17, 2012
Related Publication 20160336474A1 · Nov 17, 2016