IP Library Granted Patent US 10,640,435
Granted Patent B2
US 10,640,435 · App. 15/157,109 · Granted May 5, 2020

Multimetallic catalysts

Inventors: Peter C. Stair (Northbrook, IL); Jeffrey Camacho Bunquin (Westmont, IL); Christopher L. Marshall (Naperville, IL); Adam S. Hock (Chicago, IL)
Assignee: UChicago Argonne, LLC
C07C5/3337B01J23/60B01J23/8926B01J37/0244C07C2521/08C07C2523/06C07C2523/34C07C2523/42C07C2523/60C07C2523/656Y02P20/52
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Quick Facts
Patent No.
US 10,640,435
App. No.
15/157,109
Granted
May 5, 2020
Kind
B2
Abstract

A multimetallic catalyst having a substrate, intermediate layer and catalyst layer. The catalyst exhibits selectivity greater than 90% and a conversion rate of greater than 30%.

Claims (17)

1. A catalyst comprising:

a substrate;

an intermediate layer having a partial monoatomic thickness or a monoatomic thickness and comprising MO x wherein MO x is selected from the transition metal oxides consisting of TiO 2 , ZrO 2 , CoO x (x=1-1.5), ZnO, and MnOx (x=1 to 4), the intermediate layer deposited on the substrate; and

a catalyst layer comprising a platinum group metal, the catalyst layer deposited on the metal oxide intermediate layer;

wherein the catalyst exhibits at least 95% selectivity for propene and further wherein the catalyst exhibits at least a 70% propane conversion.

2. The catalyst of claim 1 , wherein the substrate comprises silica.

3. The catalyst of claim 1 , wherein the catalyst layer consists essentially of a platinum material.

4. The catalyst of claim 1 further comprising an overcoat layer deposited on the catalyst.

5. The catalyst of claim 1 , wherein the overcoat layer comprises multiple layers of alumina.

6. A catalyst for alkane dehydrogenation comprising:

a substrate consisting essentially of silica;

an intermediate layer consisting essentially of ZnO, the intermediate layer deposited on the substrate; and

a catalyst layer consisting essentially of a platinum group metal, the catalyst layer deposited on the intermediate layer;

wherein the catalyst exhibits at least 95% selectivity for propene and further wherein the catalyst exhibits at least a 70% propane conversion.

7. The catalyst of claim 6 , wherein the catalyst exhibits a turnover frequency of at least 100,000 per hour after 50 hours.

8. The catalyst of claim 6 , wherein the intermediate layer has a mono atomic layer thickness.

9. The catalyst of claim 6 , wherein the intermediate layer has a partial mono atomic layer thickness.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 20, 2020
From: STAIR, PETER C.
To: NORTHWESTERN UNIVERSITY
Reel/Frame 052441/0791 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 17, 2020
From: MARSHALL, CHRISTOPHER L.; BUNQUIN, JEFFREY CAMACHO
To: UCHICAGO ARGONNE, LLC
Reel/Frame 051545/0951 →
CONFIRMATORY LICENSE Recorded Aug 3, 2016
From: UCHICAGO ARGONNE, LLC
To: ENERGY, UNITED STATES DEPARTMENT OF
Reel/Frame 039626/0607 →
Continuity (1)
Related Publication 20170333878A1 · Nov 23, 2017
Cited By (1)
US 12,435,415