IP Library Granted Patent US 10,056,639
Granted Patent B2
US 10,056,639 · App. 15/162,470 · Granted Aug 21, 2018

Aqueous redox flow batteries featuring improved cell design characteristics

Inventors: Arthur J. Esswein (San Francisco, CA); Steven Y. Reece (Cambridge, MA); Evan R. King (Quincy, MA); John Goeltz (Carmel, CA); Desiree D. Amadeo (Lunenburg, MA)
Assignee: Lockheed Martin Energy, LLC
H01M8/188C07F7/28H01M4/9008H01M8/20Y02E60/528
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Quick Facts
Patent No.
US 10,056,639
App. No.
15/162,470
Granted
Aug 21, 2018
Kind
B2
Abstract

Provided are compositions having the formula M n Ti(L1)(L2)(L3) wherein L1 is a catecholate, and L2 and L3 are each independently selected from catecholates, ascorbate, citrate, glycolates, a polyol, gluconate, glycinate, hydroxyalkanoates, acetate, formate, benzoates, malate, maleate, phthalates, sarcosinate, salicylate, oxalate, a urea, polyamine, aminophenolates, acetylacetone or lactate; each M is independently Na, Li, or K; n is 0 or an integer from 1-6. Also provided are energy storage systems.

Claims (17)

1. A composition comprising:

a titanium complex containing at least one unsubstituted catecholate ligand and at least one substituted catecholate, wherein at least one of the substituted catecholate ligands is a sulfonated catecholate ligand; and

sodium and potassium counterions.

2. The composition of claim 1 , wherein the titanium complex contains a hydroxycatecholate ligand.

3. The composition of claim 1 , wherein the titanium complex contains two unsubstituted catecholate ligands and the one sulfonated catecholate ligand.

4. The composition of claim 1 , wherein the titanium complex contains one unsubstituted catecholate ligand, one sulfonated catecholate ligand, and at least one ligand selected from the group consisting of, ascorbate, citrate, glycolate, a polyol, gluconate, glycinate, a hydroxyalkanoate, acetate, formate, benzoate, malate, maleate, phthalate, sarcosinate, salicylate, oxalate, a urea, a polyamine, an aminophenolate, acetylacetonate, and lactate.

5. The composition of claim 1 , wherein the sodium and potassium counterions are present in substantially equal molar amounts.

6. An aqueous solution comprising the composition of claim 1 .

7. The aqueous solution of claim 6 , wherein the titanium complex has a concentration of at least about 0.5 M in the aqueous solution.

8. The aqueous solution of claim 6 , wherein the titanium complex contains a hydroxycatecholate ligand.

9. The aqueous solution of claim 6 , wherein the titanium complex contains two unsubstituted catecholate ligands and one sulfonated catecholate ligand.

10. The aqueous solution of claim 6 , wherein the titanium complex contains one unsubstituted catecholate ligand, one sulfonated catecholate ligand, and at least-one ligand selected from the group consisting of ascorbate, citrate, glycolate, a polyol, gluconate, glycinate, a hydroxyalkanoate, acetate, formate, benzoate, malate, maleate, phthalate, sarcosinate, salicylate, oxalate, a urea, a polyamine, an aminophenolate, acetylacetonate, and lactate.

11. The aqueous solution of claim 6 , wherein substantially equal molar quantities of the sodium and potassium counterions are present.

12. A flow battery comprising:

a first half-cell containing a first electrolyte solution; and

a second half-cell containing a second electrolyte solution;

wherein at least one of the first electrolyte solution and the second electrolyte solution comprises the aqueous solution of claim 6 .

Assignments (2)
CHANGE OF NAME Recorded Jul 12, 2018
From: LOCKHEED MARTIN ADVANCED ENERGY STORAGE, LLC
To: LOCKHEED MARTIN ENERGY, LLC
Reel/Frame 046570/0942 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 29, 2017
From: ESSWEIN, ARTHUR J.; REECE, STEVEN Y.; KING, EVAN R.; GOELTZ, JOHN; AMADEO, DESIREE D.
To: LOCKHEED MARTIN ADVANCED ENERGY STORAGE, LLC
Reel/Frame 043062/0629 →
Continuity (10)
Continuation 14164839 · Jan 27, 2014
Continuation In Part 13796004 · Mar 12, 2013
Continuation In Part 13795878 · Mar 12, 2013
Provisional Application 61739538 · Dec 19, 2012
Provisional Application 61739140 · Dec 19, 2012
Provisional Application 61738546 · Dec 18, 2012
Provisional Application 61683260 · Aug 15, 2012
Provisional Application 61676473 · Jul 27, 2012
Provisional Application 61739145 · Dec 19, 2012
Related Publication 20160268623A1 · Sep 15, 2016