IP Library › Granted Patent US 10,322,962
Granted Patent B2
US 10,322,962 · App. 15/197,245 · Granted Jun 18, 2019

Method for producing a substrate tube of quartz glass

Inventors: Oliver Ganz (Bruchkoebel, DE); Harald Hain (Kahl, DE)
Assignee: Heraeus Quarzglas GmbH & Co. KG
C03B37/01242C03B23/047C03B37/01245C03B2205/40
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,322,962
App. No.
15/197,245
Granted
Jun 18, 2019
Kind
B2
Abstract

A method for producing substrate tubes of quartz glass includes continuously supplying a hollow cylinder of quartz glass to a heating zone, softening the hollow cylinder zonewise in the heating zone, and drawing off a tubular strand from the softened portion. The hollow cylinder has an outer diameter C a , an inner diameter C i and an inner bore. The tubular strand has an outer diameter T a and an inner diameter T i . The following parameters are applicable to the hollow cylinder and the tubular strand: C a >180 mm, C r >3 with C r =C a /C i , T r <1.6 with T r =T a /T i and C i /T i <2.5. The blow pressure in an inner bore is adjusted to a value in the range of 4 to 10 mbar. Substrate tubes, obtained by cutting the tubular strand to the desired length, serve as semi-finished products for the manufacture of preforms for optical fibers.

Claims (29)

1. A method for producing a substrate tube of quartz glass, comprising:

continuously supplying a hollow cylinder of quartz glass to a heating zone ( 3 ), the hollow cylinder having an outer diameter C a , an inner diameter C i , an inner bore and a wall thickness of at least 62.5 mm;

zonewise softening the hollow cylinder in the heating zone ( 3 ); and

drawing off a tubular strand ( 12 ) from a softened portion of the hollow cylinder, the tubular strand ( 12 ) having an outer diameter T a and an inner diameter T i ,

wherein a blow pressure is produced in an inner bore ( 13 ) is in the range of 4 to 10 mbar, and

wherein the following parameters are applicable to the hollow cylinder ( 4 ) and the tubular strand ( 12 ):

C a >180 mm,

C r >3 with C r =C a /C i ,

T r <1.6 with T r =T a /T i ,

C i /T i <2.5, and

C r /T r >1.88.

2. The method according to claim 1 , wherein the blow pressure is in the range of 6 to 8 mbar, and wherein the following parameters are applicable to the hollow cylinder:

Ca< 300 mm, and

C i /T i <2.

3. The method according to claim 1 , wherein the following parameters are applicable to the tubular strand:

28 mm< Ta< 50 mm, and

T r <1.3.

4. The method according to claim 1 , wherein the following parameters are applicable to the hollow cylinder and the tubular strand:

3.5< Cr< 4.5, and

C r >T r +2.4.

5. The method according to claim 1 , wherein the inner bore of the hollow cylinder has an inner wall that has a surface roughness defined by a roughness value R z >1 μm.

6. The method according to claim 1 , wherein the hollow cylinder has an outer wall that has a surface roughness defined by a roughness value R z >4 μm.

7. The method according to claim 1 , wherein a heating tube ( 1 ) is used that comprises a circular heating space ( 3 ) which is bounded by an inner wall and which defines a heating space volume V Heiz within which the hollow cylinder ( 4 ), a drawing bulb ( 11 ) and the tubular strand ( 12 ) occupy a cylinder space volume V c , where V Heiz >2.5×V c .

8. The method according to claim 7 , wherein an annular gap with a mean gap width in the range of 15 mm and 25 mm remains between the inner wall of the heating zone and the hollow cylinder ( 4 ).

9. The method according to claim 7 , wherein the heating tube ( 1 ) has a length L between 150 mm and 200 mm.

10. The method according to claim 1 , wherein the outer diameter T a of the tubular strand is in the range of 28 mm to not more than 35 mm and a throughput volume is in the range of 10 to 20 kg/h.

11. The method according to claim 1 , wherein the outer diameter T a of the tubular strand is in the range of 35 mm to 50 mm and a throughput volume is in the range of 20 to 30 kg/h.

12. The method according to claim 1 , wherein the tubular strand is drawn off at an elongation ratio of less than 150.

13. The method according to claim 1 , wherein the tubular strand is drawn off at an elongation ratio in the range between 50 and 130.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 25, 2016
From: GANZ, OLIVER; HAIN, HARALD
To: HERAEUS QUARZGLAS GMBH & CO. KG
Reel/Frame 039240/0094 →
Priority Claims (1)
EP 15175343 · Jul 3, 2015 · regional
Continuity (1)
Related Publication 20170001901A1 · Jan 5, 2017