IP Library Granted Patent US 9,765,066
Granted Patent B2
US 9,765,066 · App. 15/214,061 · Granted Sep 19, 2017

Selective HDAC1 and HDAC2 inhibitors

Inventors: John H. van Duzer (Georgetown, MA); Ralph Mazitschek (Belmont, MA)
Assignee: REGENACY PHARMACEUTICALS, LLC
C07D409/12A61K31/4045A61K31/4709A61K31/496A61K31/498A61K31/5377C07D209/08C07D209/34C07D215/48C07D215/54C07D231/56C07D333/20C07D401/12C07D471/04
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Quick Facts
Patent No.
US 9,765,066
App. No.
15/214,061
Granted
Sep 19, 2017
Kind
B2
Abstract

Provided herein are compounds, pharmaceutical compositions comprising such compounds and methods of using such compounds to treat or prevent diseases or disorders associated with HDAC activity, particularly diseases or disorders that involve activity of HDAC1 and/or HDAC2. Such diseases include cancer, sickle-cell anemia, beta-thalassemia, and HIV.

Claims (47)

1. A compound of Formula I:

or a pharmaceutically acceptable salt thereof,

wherein

Y 1 is CR 7 or NR 7 ;

Y 2 , Y 3 , Y 4 , Y 5 , and Y 6 are each independently CH, CH 2 , N, or C(O), wherein at least one of Y 2 , Y 3 , Y 4 , and Y 5 are CH;

R 1 is mono-, bi-, or tri-cyclic aryl or heteroaryl, wherein the mono-, bi-, or tri-cyclic aryl or heteroaryl is optionally substituted;

R 2 and R 3 are each independently selected from C 2-6 -alkenyl, C 2-6 -alkynyl, C 3-6 -cycloalkyl, C 1-6 -alkyl-C 3-6 -cycloalkyl, heterocycloalkyl, C 1-6 -alkyl-heterocycloalkyl, NR 4 R 5 , O—C 1-6 -alkyl-OR 6 , C 1-6 -alkyl-OR 6 , aryl, C(O)N(H)-heteroaryl, C(O)-heteroaryl, C(O)-heterocycloalkyl, C(O)-aryl, C(O)—C 1-6 -alkyl, CO 2 —C 1-6 -alkyl, or C(O)—C 1-6 -alkyl-heterocycloalkyl, wherein the cycloalkyl, heterocycloalkyl, aryl, or heteroaryl is optionally substituted;

R 4 is H, C 1-6 -alkyl, or C 1-6 -alkyl-OR 6 ;

R 5 is CO 2 R 6 , C 1 -C 6 -alkyl-aryl, or C 1-6 -alkyl-OR 6 ;

R 6 is H or C 1-6 -alkyl;

R 7 is null, H, C 1-6 -alkyl, C 3-6 -cycloalkyl, C 1-6 -alkyl-C 3-6 -cycloalkyl, heterocycloalkyl, or C 1-6 -alkyl-heterocycloalkyl;

a line denotes an optionally double bond;

m is 0 or 1; and

n is 0 or 1, provided at least one of m or n is 1.

2. The compound of claim 1 , or a pharmaceutically acceptable salt thereof,

wherein

R 1 is mono-, bi-, or tri-cyclic aryl or heteroaryl, wherein the mono-, bi-, or tri-cyclic aryl or heteroaryl is optionally substituted with halo, C 1-4 -alkyl, CO 2 R 6 , C(O)R 6 , or C 1-6 -alkyl-OR 6 ;

R 2 and R 3 are each independently selected from C 2-6 -alkenyl, C 2-6 -alkynyl, C 3-6 -cycloalkyl, C 1-6 -alkyl-C 3-6 -cycloalkyl, heterocycloalkyl, C 1-6 -alkyl-heterocycloalkyl, NR 4 R 5 , O—C 1-6 -alkyl-OR 6 , C 1-6 -alkyl-OR 6 , aryl, heteroaryl, C(O)N(H)-heteroaryl, C(O)-heteroaryl, C(O)-heterocycloalkyl, C(O)-aryl, C(O)—C 1-6 -alkyl, CO 2 —C 1-6 -alkyl, and C(O)—C 1-6 -alkyl-heterocycloalkyl, wherein the cycloalkyl, heterocycloalkyl, aryl, or heteroaryl is optionally substituted with C 1-4 -alkyl, CO 2 R 6 , C(O)R 6 , or C 1-6 -alkyl-OR 6 .

3. The compound of claim 1 , or a pharmaceutically acceptable salt thereof,

wherein

R 1 is monocyclic aryl or heteroaryl, wherein the aryl or heteroaryl is optionally substituted with halo;

R 2 and R 3 are each independently selected from C 2-6 -alkenyl, C 3-6 -cycloalkyl, C 1-6 -alkyl-C 3-6 -cycloalkyl, heterocycloalkyl, C 1-6 -alkyl-heterocycloalkyl, NR 4 R 5 , O—C 1-6 -alkyl-OR 6 , or C 1-6 -alkyl-OR 6 ;

R 4 is H or C 1-6 -alkyl;

R 5 is CO 2 R 6 or C 1-6 -alkyl-OR 6 ; and

R 6 is C 1-6 -alkyl.

4. The compound of claim 1 , or a pharmaceutically acceptable salt thereof,

wherein

m is 1; n is 1; Y 1 is N; and Y 2 , Y 3 , Y 4 , Y 5 , and Y 6 are each CH;

m is 0; n is 1; Y 2 is N; Y 1 is CR 7 ; and Y 3 , Y 4 , and Y 6 are each CH;

m is 0; n is 1; Y 1 is CR 7 ; Y 2 is N; Y 3 is C(O); Y 4 is CH 2 ; and Y 6 is CH;

m is 1; n is 1; Y 1 is CR 7 ; Y 2 is N, and Y 3 , Y 4 , Y 5 , and Y 6 are each CH;

m is 0; n is 1; Y 1 is CR 7 ; Y 2 and Y 3 are each N; and Y 4 and Y 6 are each CH;

m is 0; n is 1; Y 1 and Y 2 are N; Y 3 , Y 4 , and Y 6 are each CH; or

m is 1; n is 1; and Y1, Y 2 , Y 3 , Y 4 , Y 5 , and Y 6 are each CH.

5. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein R 1 is phenyl, thienyl, or pyridinyl.

6. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein R 1 is para to NH 2 in the compound of Formula I.

7. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein R 2 is cyclopropyl, cyclopentyl, CH 2 -cyclopropyl, CH 2 CH═CH 2 .

8. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein R 3 is heterocycloalkyl, C 1-6 -alkyl-heterocycloalkyl, O—C 1-6 -alkyl-OR 6 , or C 1-6 -alkyl-OR 6 , or NR 4 R 5 .

9. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein R 3 is morpholinyl, piperazinyl, CH 2 CH 2 -morpholinyl, CH 2 -morpholinyl, CH 2 CH 2 -piperazinyl, CH 2 -piperazinyl, OCH 2 CH 2 OCH 3 , OCH 2 OCH 3 , CH 2 CH 2 OCH 3 , or NHCO 2 CH 2 CH 3 .

10. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein R 7 is H or C 3-6 -cycloalkyl.

11. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein R 7 is cyclopropyl.

12. The compound claim 1 , having the structure of Formula III:

or a pharmaceutically acceptable salt thereof.

13. A compound selected from the group consisting of:

or pharmaceutically acceptable salts thereof.

14. A compound selected from the group consisting of:

or pharmaceutically acceptable salts thereof.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 2, 2017
From: ACETYLON PHARMACEUTICALS, INC.
To: REGENACY PHARMACEUTICALS, LLC
Reel/Frame 043175/0534 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 22, 2016
From: VAN DUZER, JOHN H.; MAZITSCHEK, RALPH
To: ACETYLON PHARMACEUTICALS, INC.
Reel/Frame 039837/0302 →
Continuity (6)
Division 14824831 · Aug 12, 2015
Division 14069741 · Nov 1, 2013
Provisional Application 61889276 · Oct 10, 2013
Provisional Application 61778231 · Mar 12, 2013
Provisional Application 61721881 · Nov 2, 2012
Related Publication 20170044144A1 · Feb 16, 2017