IP Library Granted Patent US 10,159,722
Granted Patent B2
US 10,159,722 · App. 15/254,629 · Granted Dec 25, 2018

Enzyme-activated collagen and tissue matrices

Inventors: Wenquan Sun (Warrington, PA); Xiaohua Yu (Willimantic, CT)
Assignee: LifeCell Corporation
A61K38/4886A61L27/24A61L27/362A61L27/3604A61L27/3687A61L27/54A61L2300/254
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,159,722
App. No.
15/254,629
Granted
Dec 25, 2018
Kind
B2
Abstract

Devices and methods for treating defects in connective tissue are provided along with methods for making such devices. The devices can include enzyme-activated acellular tissue matrices that facilitate regrowth of the damaged tissue.

Claims (23)

1. A method of treatment comprising:

selecting an anatomical site for treatment;

selecting a collagen-based acellular tissue matrix, wherein the matrix has been contacted with a composition containing at least one protease, wherein the protease consists essentially of at least one of MMP-1, MMP-3, or MMP-9, wherein the protease can cleave one or more matrikines from the tissue matrix, and wherein the composition further contains a deactivating agent comprising one or more chelators for reducing the activity of the at least one protease by binding metal ions needed for activity of the at least one protease; and

implanting the collagen-based acellular tissue matrix into the anatomic site.

2. The method of claim 1 , wherein the acellular tissue matrix comprises an acellular dermal matrix.

3. The method of claim 2 , wherein the acellular tissue matrix comprises an acellular porcine dermal matrix.

4. The method of claim 1 , wherein the protease is a matrix metalloproteinase (MMP).

5. The method of claim 1 , wherein the at least one protease is in a solution.

6. The method of claim 1 , wherein the composition further contains at least one of an elastase or a dispase.

7. The method of claim 1 , wherein the chelating agent comprises ethylenediaminetetraacetic acid (EDTA), ethylene glycol tetraacetic acid (EGTA), or orthophenanthroline.

8. The method of claim 1 , wherein the chelating agent regulates the degradation of the tissue matrix by modulating protease activity.

9. The method of claim 1 , further comprising exposing the acellular tissue matrix to a disinfectant.

10. The method of claim 9 , wherein the disinfectant is isopropyl alcohol.

11. The method of claim 1 , further comprising sterilizing the acellular tissue matrix.

12. The method of claim 11 , wherein sterilizing the acellular tissue matrix comprises application of ethylene oxide, propylene, gamma irradiation, or e-beam irradiation.

13. The method of claim 1 , further comprising lyophilizing the acellular tissue matrix.

14. The method of claim 1 , further comprising storing the acellular tissue matrix in a hydrated state prior to implanting the acellular tissue matrix into the anatomical site.

15. The method of claim 1 , wherein the composition further contains a bioactive substance.

16. The method of claim 15 , wherein the bioactive substance comprises an antibacterial agent, a cytokine, a growth factor, non-collagenous tissue, or cells.

17. The method of claim 1 , wherein the activity of the protease is restored automatically upon implantation into a subject.

18. The method of claim 17 , wherein the restoration of protease activity results in the release of matrikines from the tissue matrix.

19. The method of claim 1 , wherein the matrikines comprise GHK (SEQ ID NO: 1), CNYYSNS (SEQ ID NO: 2), VGPVG (SEQ ID NO: 3), VGVAPG (SEQ ID NO: 4), KKGHK (SEQ ID NO: 5), or DGGRYY (SEQ ID NO: 6).

20. The method of claim 1 , wherein the chelator is present in the composition at a concentration between 4 mM and 20 mM.

Assignments (5)
RELEASE OF SECURITY INTEREST 040098/0268 Recorded Feb 2, 2017
From: WILMINGTON TRUST
To: LIFECELL CORPORATION
Reel/Frame 041608/0554 →
RELEASE OF SECURITY INTEREST 037845/0497 Recorded Feb 2, 2017
From: WILMINGTON TRUST
To: LIFECELL CORPORATION
Reel/Frame 041608/0603 →
RELEASE OF SECURITY INTEREST 040291/0237 Recorded Feb 2, 2017
From: WILMINGTON TRUST
To: LIFECELL CORPORATION
Reel/Frame 041608/0702 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 11, 2016
From: SUN, WENQUAN; YU, XIAOHUA
To: LIFECELL CORPORATION
Reel/Frame 040286/0935 →
LIMITED THIRD LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Oct 7, 2016
From: KCI USA, INC.; LIFECELL CORPORATION; KCI LICENSING, INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 040291/0237 →
Continuity (3)
Continuation 13777153 · Feb 26, 2013
Provisional Application 61608458 · Mar 8, 2012
Related Publication 20170065743A1 · Mar 9, 2017
Cited By (1)
US 12,376,843