IP Library Granted Patent US 9,972,776
Granted Patent B2
US 9,972,776 · App. 15/260,351 · Granted May 15, 2018

Plasma processing method

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Quick Facts
Patent No.
US 9,972,776
App. No.
15/260,351
Granted
May 15, 2018
Kind
B2
Abstract

According to one embodiment of the present invention, there is provided a plasma processing method for forming a pattern of a mask on a laminated film of a magnetic film and a metal oxide film, and the plasma processing method includes: plasma etching the magnetic film in a chamber; and after the plasma etching, plasma cleaning the chamber, wherein the plasma cleaning performs first plasma cleaning of plasma cleaning using a gas mixture of chlorine element-containing gas and boron trichloride gas, and after the first plasma cleaning, second plasma cleaning of removing boron remaining in the chamber.

Claims (59)

1. A plasma processing method for transcribing a pattern of a mask onto a laminated film in which a first magnetic film, a metal oxide film arranged over the first magnetic film, and a second magnetic film arranged over the metal oxide film are deposited, the plasma processing method comprising:

etching to plasma-etch the second magnetic film using the mask in a chamber; and

cleaning to plasma-clean the chamber, in which the second magnetic film is plasma-etched, after the etching,

wherein the cleaning includes:

a first plasma cleaning to plasma-clean using a gas mixture of a chlorine gas and boron trichloride gas, and

after the first plasma-cleaning and before another etching in the chamber, a second plasma-cleaning to plasma-clean using a gas mixture of carbon tetrafluoride gas and oxygen gas.

2. The plasma processing method according to claim 1 ,

wherein the first and second magnetic films contain at least one of iron, cobalt, and nickel elements, respectively.

3. The plasma processing method according to claim 1 ,

wherein the etching reaches the first magnetic film.

4. The plasma processing method according to claim 1 ,

wherein the etching does not reach the first magnetic film.

5. The plasma processing method according to claim 1 ,

wherein the metal oxide film is a magnesium oxide film.

6. The plasma processing method according to claim 1 ,

wherein the mask includes a tantalum film, and

wherein in the etching, the second magnetic film is etched using chlorine gas.

7. The plasma processing method according to claim 6 ,

wherein the laminated film functions as a magnetic tunnel junction (MTJ) device having a structure in which the metal oxide film is interposed between the first and second magnetic films.

8. The plasma processing method according to claim 1 ,

wherein, in the etching, the second magnetic film is etched using an inductively-coupled plasma etching apparatus having a Faraday shield, and

wherein a radio frequency voltage applied to the Faraday shield during the second plasma-cleaning is lower than a radio frequency voltage applied to the Faraday shield during the first plasma-cleaning.

9. A plasma processing method for transcribing a pattern of a mask onto a laminated film in which a first magnetic film, a metal oxide film arranged over the first magnetic film, and a second magnetic film arranged over the metal oxide film are deposited, the plasma processing method comprising:

etching to plasma-etch the second magnetic film using the mask in a chamber, the etching producing deposits containing one or more etched materials in the chamber; and

cleaning to plasma-clean the chamber to remove the deposits, in which the second magnetic film is plasma-etched, after the etching,

wherein the cleaning includes:

first plasma cleaning to plasma-clean the chamber to remove the deposits using a gas mixture of a chlorine element-containing gas and boron trichloride gas, the first plasma cleaning producing residual boron in the chamber from the boron trichloride gas, and

after the first plasma-cleaning and before another etching in the chamber, a second plasma-cleaning to remove the residual boron remaining in the chamber, and

wherein the second plasma cleaning uses a gas mixture of carbon tetrafluoride gas and oxygen element-containing gas.

10. The plasma processing method according to claim 9 ,

wherein the first and second magnetic films each contain at least one of iron, cobalt, or nickel elements.

11. The plasma processing method according to claim 9 ,

wherein the etching reaches the first magnetic film.

12. The plasma processing method according to claim 9 ,

wherein the etching does not reach the first magnetic film.

13. The plasma processing method according to claim 9 ,

wherein the metal oxide film is a magnesium oxide film, and

wherein the oxygen element-containing gas is oxygen gas.

14. The plasma processing method according to claim 13 ,

wherein the chlorine element-containing gas is chlorine gas.

15. The plasma processing method according to claim 14 ,

wherein the mask includes a tantalum film, and

wherein in the etching, the second magnetic film is etched using chlorine gas.

16. The plasma processing method according to claim 15 ,

wherein the laminated film functions as a magnetic tunnel junction (MTJ) device having a structure in which the metal oxide film is interposed between the first and second magnetic films.

17. A plasma processing method for transcribing a pattern of a mask onto a laminated film in which a first magnetic film, a metal oxide film arranged over the first magnetic film, and a second magnetic film arranged over the metal oxide film are deposited, the plasma processing method comprising:

etching to plasma-etch the second magnetic film using the mask in a chamber, the etching producing deposits containing one or more etched materials in the chamber; and

cleaning to plasma-clean the chamber to remove the deposits, in which the second magnetic film is plasma-etched, after the etching,

wherein the cleaning includes:

first plasma cleaning to plasma-clean the chamber to remove the deposits using a gas mixture of a chlorine element-containing gas and boron trichloride gas, the first plasma cleaning producing residual boron in the chamber from the boron trichloride gas, and

after the first plasma-cleaning and before another etching in the chamber, a second plasma-cleaning to remove the residual boron remaining in the chamber,

wherein the second plasma cleaning uses a gas mixture of carbon tetrafluoride gas and oxygen element-containing gas,

wherein, in the etching, the second magnetic film is etched using an inductively-coupled plasma etching apparatus having a Faraday shield, and

wherein a radio frequency voltage applied to the Faraday shield during the second plasma-cleaning using the gas mixture of carbon tetrafluoride gas and oxygen element-containing gas is lower than a radio frequency voltage applied to the Faraday shield during the first plasma-cleaning using the gas mixture of the chlorine element-containing gas and boron trichloride gas.

18. The plasma processing method according to claim 17 ,

wherein the metal oxide film is a magnesium oxide film, and

wherein the oxygen element-containing gas is oxygen gas.

19. The plasma processing method according to claim 18 ,

wherein the chlorine element-containing gas is chlorine gas.

Assignments (2)
CHANGE OF NAME AND ADDRESS Recorded Mar 30, 2020
From: HITACHI HIGH-TECHNOLOGIES CORPORATION
To: HITACHI HIGH-TECH CORPORATION
Reel/Frame 052259/0227 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 9, 2016
From: SUYAMA, MAKOTO; YAMAMOTO, NAOHIRO; ISHIMARU, MASATO; TOYOOKA, HIDENORI; HOSAKA, NORIHIRO
To: HITACHI HIGH-TECHNOLOGIES CORPORATION
Reel/Frame 039680/0934 →