IP Library Granted Patent US 10,343,141
Granted Patent B1
US 10,343,141 · App. 15/269,745 · Granted Jul 9, 2019

Compositions, systems and methods using selective porous materials for oxygen separation

Inventors: Tina M. Nenoff (Albuquerque, NM); Dorina Florentina Sava Gallis (Albuquerque, NM); Marie Vernell Parkes (Albuquerque, NM); Jeffery A. Greathouse (Albuquerque, NM)
Assignee: National Technology & Engineering Solutions of Sandia, LLC
B01J20/226B01D53/04B01D2253/204B01D2257/104
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Quick Facts
Patent No.
US 10,343,141
App. No.
15/269,745
Granted
Jul 9, 2019
Kind
B1
Abstract

MOFs are disclosed that can efficiently adsorb oxygen from a gas stream, such as air. Systems and methods are also disclosed that utilize MOFs to separate oxygen from a gas stream. The separated oxygen may be used in a commercial process such as a combustion process.

Claims (10)

1. A composition, comprising:

a metal-organic framework material capable of oxygen capture, the metal organic framework material consisting essentially of m/Cu-BTC, where BTC=benzene-1,3,5-tricarboxylic acid and m/Cu represents partial substitution of Cu with a metal ion (m) selected from a group consisting Sc, Ti, V, Mn, Fe and Co.

2. The composition of claim 1 , wherein m is Sc.

3. A process, comprising:

contacting a gas stream containing oxygen at a first concentration with a metal-organic framework material having the formula m/Cu-BTC, where BTC=benzene-1,3,5-tricarboxylic acid and m/Cu represents partial substitution of Cu with a metal ion (m) selected from a group consisting Sc, Ti, V, Mn, Fe and Co at a first temperature and first pressure to adsorb oxygen from the gas stream into the metal-organic framework; and

desorbing oxygen from the metal-organic framework material at a second temperature and a second pressure.

4. The process of claim 3 , wherein the first and second temperatures are equal.

5. The process of claim 3 , wherein the second pressure is less than the first pressure.

6. The process of claim 3 , wherein the second temperature is greater than the first temperature.

7. The process of claim 3 , wherein the first temperature is ambient temperature.

Assignments (3)
CHANGE OF NAME Recorded Mar 7, 2018
From: SANDIA CORPORATION
To: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
Reel/Frame 045516/0311 →
CONFIRMATORY LICENSE Recorded Dec 28, 2016
From: SANDIA CORPORATION
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 041208/0799 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 19, 2016
From: NENOFF, TINA M.; SAVA GALLIS, DORINA FLORENTINA; PARKES, MARIE VERNELL; GREATHOUSE, JEFFREY
To: SANDIA CORPORATION
Reel/Frame 040670/0766 →
Continuity (2)
Provisional Application 62220549 · Sep 18, 2015
Provisional Application 62325833 · Apr 21, 2016