IP Library Granted Patent US 10,214,700
Granted Patent B1
US 10,214,700 · App. 15/280,758 · Granted Feb 26, 2019

Methods utilizing durable functional materials for chemical processes that include an oxidation step

Inventors: James E. Miller (Albuquerque, NM); Eric N. Coker (Albuquerque, NM); Andrea Ambrosini (Albuquerque, NM); Ellen B. Stechel (Tempe, AZ)
Assignees: National Technology & Engineering Solutions of Sandia, LLC; Arizona Board of Regents on behalf of Arizona State University
C10J3/725C01B3/32C01B3/36C10J2300/093C10J2300/0983
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Quick Facts
Patent No.
US 10,214,700
App. No.
15/280,758
Granted
Feb 26, 2019
Kind
B1
Abstract

The present disclosure is directed to methods using durable functional materials for processes that include an oxidation step. The durable functional materials are redox active oxygen carrier materials that include a zirconia or yttria-stabilized-zirconia (YSZ) matrix containing a redox-active metal ion(s), such as, but not limited to Fe, Mn, Cu, Co and Cr. In an embodiment, these materials are used in chemical looping processes.

Claims (21)

1. A method, comprising

contacting a redox active oxygen carrier material with a fluid stream to reduce a redox active metal oxide in the redox active oxygen carrier material and oxidize a component in the fluid stream; and

contacting the redox active oxygen carrier material with a second fluid stream to oxidize the reduced redox active metal;

wherein redox active oxygen carrier material comprises a redox active metal ion atomically dispersed in a zirconia or yttria-stabilized zirconia matrix.

2. The method of claim 1 ,

wherein the fluid stream comprises a carbon or hydrocarbon.

3. The method of claim 2 , wherein the hydrocarbon is selected from a group consisting of methane, ethane, propane, butane, kerosene, diesel fuel, coke, biomass and coal.

4. The method of claim 1 , further comprising:

contacting the redox active oxygen carrier material with a second fluid stream to oxidize the reduced redox active metal oxide and form partially reduced products.

5. The method of claim 4 , wherein the partially oxidized products are selected from a group consisting of hydrogen and carbon monoxide.

6. The method of claim 1 , wherein the redox active metal ion is selected from a group consisting of ions of Fe, Mn, Cu, Co and Cr.

7. The method of claim 1 , further comprising:

wherein the second fluid stream comprises air; and

reducing the redox active oxygen carrier material with a hydrocarbon or via thermal means, and

reducing the redox oxygen carrier material to produce oxygen.

8. The method of claim 1 ,

wherein the fluid stream comprises steam and a hydrocarbon.

9. The method of claim 1 ,

wherein the fluid stream comprises carbon dioxide and a hydrocarbon.

10. The method of claim 1 , wherein the fluid stream comprises steam and a hydrocarbon.

11. The method of claim 1 , wherein the fluid stream comprises water and a hydrocarbon.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 18, 2018
From: STECHEL, ELLEN
To: ARIZONA BOARD OF REGENTS FOR AND ON BEHALF OF ARIZONA STATE UNIVERSITY
Reel/Frame 047211/0332 →
CHANGE OF NAME Recorded Oct 16, 2018
From: SANDIA CORPORATION
To: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
Reel/Frame 047240/0724 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 10, 2016
From: MILLER, JAMES E.; COKER, ERIC N.; AMBROSINI, ANDREA
To: SANDIA CORPORATION
Reel/Frame 040276/0433 →
CONFIRMATORY LICENSE Recorded Oct 28, 2016
From: SANDIA CORPORATION
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 040157/0907 →
Continuity (1)
Provisional Application 62234470 · Sep 29, 2015