IP Library Granted Patent US 10,407,351
Granted Patent B2
US 10,407,351 · App. 15/290,305 · Granted Sep 10, 2019

Method of dispersing anatase titanium dioxide for penetration in concrete structures to reduce pollutants

Inventors: Colin Durante (Mansfield, OH); Craig Higgins (San Diego, CA)
Assignee: Pavement Technology, Inc.
C04B41/5072B01D53/9413B01J21/063B01J35/004B01J35/0013B01J37/0215C04B41/009C04B41/5041C04B41/65B01D2255/20707C04B2111/00827
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Quick Facts
Patent No.
US 10,407,351
App. No.
15/290,305
Granted
Sep 10, 2019
Kind
B2
Abstract

Methods for embedding photocatalytic titanium dioxide in concrete surfaces to reduce pollutants via photocatalytic reactions are provided herein. One method includes mixing a solvent compound with an anatase titanium dioxide (TiO 2 ) photocatalyst, applying an amount of concrete treatment compound to an upper surface of the concrete, the concrete treatment compound comprising a mixture of a liquid carrier compound with the anatase titanium dioxide (TiO 2 ) photocatalyst.

Claims (44)

1. A method for embedding photocatalytic titanium dioxide (TiO 2 ) in a concrete surface of a concrete structure, the method comprising:

determining a desired depth of penetration of the photocatalytic TiO 2 in the concrete surface, the desired depth depending on an expected depth of wear of the concrete structure during a lifespan of the concrete structure;

determining a desired concentration of the photocatalytic TiO 2 in the concrete structure;

selecting a liquid carrier capable of penetrating the concrete structure to the desired depth;

calculating an amount of an anatase TiO 2 photocatalyst based on the desired concentration of the photocatalytic TiO 2 in the concrete structure;

mixing the liquid carrier and the amount of the anatase TiO 2 photocatalyst to produce a photocatalytic compound, the photocatalytic compound sealing and hardening the concrete structure; the photocatalytic compound filling voids in the concrete structure to increase resistance to one or more of the following: water damage, chloride ion penetration, de-icing salt, freeze damage, and thaw damage; and

applying the photocatalytic compound to the concrete surface, the photocatalytic compound being configured to impregnate the concrete structure with the desired concentration of the photocatalytic TiO 2 to the desired depth of penetration, wherein the photocatalytic TiO 2 is to catalyze a reaction of at least one pollutant.

2. The method of claim 1 , wherein the reaction includes chemically altering the at least one pollutant into a non-hazardous material or a less hazardous material.

3. The method of claim 1 , wherein the reaction includes a photocatalytic oxidation (PCO) or a reduction.

4. The method of claim 1 , wherein the concrete structure includes one of the following: a concrete road, a horizontal concrete structure, and a vertical concrete structure.

5. The method of claim 1 , wherein the at least one pollutant includes one or more of a nitrogen oxides (NO x ) and a volatile organic compounds (VOC).

6. The method of claim 1 , wherein the liquid carrier is organic or inorganic.

7. The method of claim 1 , wherein the liquid carrier includes at least one of the following: tetrachloroethylene, toluene, turpentine, acetone, methyl acetate, ethyl acetate, hexane, citrus terpenes, ethanol, methyl ethyl ketone, mineral spirits, and ethyl alcohol.

8. The method of claim 1 , wherein the desired depth of penetration is from at least ⅛ of an inch to ½ of an inch relative to the concrete surface.

9. The method of claim 1 , wherein the concrete structure is in place prior to the application of the photocatalytic compound to the concrete surface or the concrete structure is in a process of curing during the application of the photocatalytic compound to the concrete surface.

10. The method of claim 1 , wherein the desired depth is sufficient for the expected wear of the concrete surface to expose the photocatalytic TiO 2 , a pollution-reducing capability of the photocatalytic TiO 2 being automatically self-regenerated throughout the lifespan of the concrete structure, the expected wear being two tenths inches over the forty years.

11. The method of claim 1 , wherein the anatase TiO 2 photocatalyst includes anatase powder form of TiO 2 at concentrations of 3% to 5% by weight.

12. The method of claim 1 , wherein the application of photocatalytic compound to the concrete surface is at a predetermined rate, the predetermined rate being selected to result in the desired depth of penetration and the desired concentration of the TiO 2 photocatalyst.

13. The method of claim 12 , wherein the predetermined rate is controlled by using a sprayer applicator with a spray bar of a variable length utilizing one or more nozzles.

14. The method of claim 12 , wherein the predetermined rate is controlled by a computerized flow manager.

15. The method of claim 1 , further comprising texturing the concrete surface prior to the application of the photocatalytic compound.

16. The method of claim 15 , wherein the texturing is performed for safety or adhesion.

17. A method for embedding photocatalytic titanium dioxide (TiO 2 ) in a concrete surface of a concrete structure, the method comprising:

determining a desired depth of penetration of the photocatalytic TiO 2 in the concrete surface, the desired depth depending on an expected depth of wear of the concrete structure during a lifespan of the concrete structure;

determining a desired concentration of the photocatalytic TiO 2 in the concrete structure;

selecting a liquid carrier capable of penetrating the concrete structure to the desired depth;

calculating an amount of an anatase TiO 2 photocatalyst based on the desired concentration of the photocatalytic TiO 2 in the concrete structure;

mixing the liquid carrier and the amount of the anatase TiO 2 photocatalyst to produce a photocatalytic compound, wherein the photocatalytic compound seals and hardens the concrete structure; and fills voids in the concrete structure to increase resistance to one or more of the following: water damage, chloride ion penetration, de-icing salt, freeze damage, and thaw damage; and

applying the photocatalytic compound to the concrete surface, the photocatalytic compound being configured to impregnate the concrete structure with the desired concentration of the photocatalytic TiO 2 to the desired depth of penetration, wherein the photocatalytic TiO 2 is to catalyze a reaction of at least one pollutant,

wherein the application of photocatalytic compound to the concrete surface is at a predetermined rate, the predetermined rate being selected to result in the desired depth of penetration and the desired concentration of the TiO 2 photocatalyst, and

wherein the concrete structure is in place prior to the application of the photocatalytic compound to the concrete surface or the concrete structure is in a process of curing during the application of the photocatalytic compound to the concrete surface.

18. The method of claim 17 , wherein the reaction includes chemically altering the at least one pollutant into a non-hazardous material or a less hazardous material.

19. The method of claim 17 , wherein the reaction includes a photocatalytic oxidation (PCO) or a reduction.

20. The method of claim 17 , wherein the concrete structure includes one of the following: a concrete road, a horizontal concrete structure, and a vertical concrete structure.

21. The method of claim 17 , wherein the at least one pollutant includes one or more of a nitrogen oxides (NO x ) and a volatile organic compounds (VOC).

22. The method of claim 17 , wherein the liquid carrier is organic or inorganic.

23. The method of claim 17 , wherein the liquid carrier includes at least one of the following: tetrachloroethylene, toluene, turpentine, acetone, methyl acetate, ethyl acetate, hexane, citrus terpenes, ethanol, methyl ethyl ketone, mineral spirits, and ethyl alcohol.

24. The method of claim 17 , wherein the desired depth of penetration is from at least ⅛ of an inch to ½ of an inch relative to the concrete surface.

25. The method of claim 17 , wherein the desired depth is sufficient for the expected wear of the concrete surface to expose the photocatalytic TiO 2 , a pollution-reducing capability of the photocatalytic TiO 2 being automatically self-regenerated throughout the lifespan of the concrete structure, the expected wear being two tenths inches over the forty years.

26. The method of claim 17 , wherein the anatase TiO 2 photocatalyst includes anatase powder form of TiO 2 at concentrations of 3% to 5% by weight.

27. The method of claim 17 , wherein the predetermined rate is controlled by using a sprayer applicator with a spray bar of a variable length utilizing one or more nozzles.

28. The method of claim 17 , wherein the predetermined rate is controlled by a computerized flow manager.

29. The method of claim 17 , further comprising texturing the concrete surface prior to the application of the photocatalytic compound.

30. The method of claim 29 , wherein the texturing is performed for safety or adhesion.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 9, 2018
From: DURANTE, COLIN; HIGGINS, CRAIG
To: PAVEMENT TECHNOLOGY, INC.
Reel/Frame 044884/0329 →
Continuity (3)
Continuation In Part 14207341 · Mar 12, 2014
Provisional Application 61780626 · Mar 13, 2013
Related Publication 20170029342A1 · Feb 2, 2017