Age-hardening process featuring anomalous aging time
View Patent ↗This document describes a process/strategy for age hardening nickel based alloys to create desirable properties with reduced energy expenditure. The inventive process introduces isolated atom nucleation sites to accelerate the nucleation rate by approximately 36 times, thereby permitting age hardening to occur in significantly less time and with significantly less energy expenditure.
1. A method for achieving accelerated age hardening in a metal alloy while minimizing the risk of over-aging, comprising:
a. providing a metal alloy containing nickel, molybdenum, chromium, and rhenium;
b. wherein said rhenium comprises 3% to 10% of the total weight of said metal alloy;
c. wherein nickel comprises the majority of said metal alloy by weight;
d. wherein said molybdenum comprises between 20% and 30% of the total weight of said metal alloy;
e. wherein said chromium comprises 5% to 10% of the total weight of said metal alloy; and
f. subjecting said metal alloy to an age hardening process conducted at a temperature in excess of 800K and for a time under 5 minutes that forms long-range-ordered precipitates of the form Ni 2 Re.
2. A method for achieving accelerated age hardening in a metal alloy as recited in claim 1 , further comprising annealing said metal alloy before subjecting said metal alloy to said age hardening process.
3. A method for achieving accelerated age hardening in a metal alloy as recited in claim 2 , further comprising cold working said metal alloy before subjecting said metal alloy to said age hardening process.
4. A method for achieving accelerated age hardening in a metal alloy as recited in claim 1 , further comprising cold working said metal alloy before subjecting said metal alloy to said age hardening process.
5. A method for achieving accelerated age hardening in a metal alloy as recited in claim 1 , wherein said nickel comprises 60% to 70% by weight.
6. A method for achieving accelerated age hardening in a metal alloy as recited in claim 1 , wherein said age hardening is conducted at a temperature of about 873 K.