IP Library Granted Patent US 11,220,663
Granted Patent B2
US 11,220,663 · App. 15/299,964 · Granted Jan 11, 2022

System and process for clarifying thin stillage

Inventors: Neal Jakel (Cedar Rapids, IA); John Kwik (Bellbrook, OH); Michael Franko (Denver, CO)
Assignee: Fluid Quip Technologies, LLC
C12F3/10B01D1/00B01D3/002B01D21/01B01D21/2488C12P7/06
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Quick Facts
Patent No.
US 11,220,663
App. No.
15/299,964
Granted
Jan 11, 2022
Kind
B2
Abstract

The present invention is directed to improved systems and processes for clarifying a thin stillage stream in a biofuel production process, such as a dry grind alcohol production process, that removes desirable amounts of insoluble solids from at least a portion of the thin stillage stream, thereby realizing any number of process enhancements.

Claims (30)

1. A process for clarifying a thin stillage stream in a biofuel production process, the process comprising:

separating a whole stillage byproduct into an insoluble solids portion, including fiber, and a thin stillage stream, including residual insoluble solids and oil;

directly mechanically separating the thin stillage stream into only a residual insoluble solids stream and a clarified thin stillage stream, which includes additional insoluble solids and the oil, wherein mechanically separating the thin stillage stream into only the residual insoluble solids stream and the clarified thin stillage stream defines a first treatment of the thin stillage stream;

thereafter, directly combining the separated residual insoluble solids stream with the whole stillage byproduct and/or the insoluble solids portion from the whole stillage byproduct;

mechanically separating out additional insoluble solids from the clarified thin stillage stream as underflow that defines backset, which is directly returned to the process at a step prior to separating the whole stillage byproduct; and

thereafter, subjecting the clarified thin stillage stream, which includes the oil, to evaporation via a first evaporator.

2. The process of claim 1 further comprising adding surfactant and/or flocculant to at least one of the whole stillage byproduct or the clarified thin stillage stream.

3. The process of claim 1 further comprising adding surfactant and/or flocculant to the clarified thin stillage stream prior to subjecting the clarified thin stillage stream to evaporation.

4. The process of claim 1 wherein the biofuel production process is a dry grind biofuel production process.

5. The process of claim 1 further comprising adding surfactant to the clarified thin stillage stream prior to subjecting the clarified thin stillage stream to evaporation.

6. The process of claim 1 wherein the clarified thin stillage stream defines feedstock for zein protein processing, fertilizers, pesticides, nutritional supplements, or pharmaceuticals.

7. The process of claim 1 wherein directly combining the separated residual insoluble solids stream with the whole stillage byproduct and/or the insoluble solids portion from the whole stillage byproduct comprises directly combining the separated residual insoluble solids stream with the whole stillage byproduct and/or the insoluble solids portion from the whole stillage byproduct prior to subjecting the whole stillage byproduct and/or the insoluble solids portion to a dryer.

8. The process of claim 1 wherein mechanically separating out additional insoluble solids from the clarified thin stillage stream comprises separating out the additional insoluble solids from the clarified thin stillage stream as underflow that defines backset, which is directly returned to the process by being directly joined with the whole stillage byproduct prior to separating the whole stillage byproduct.

9. The process of claim 1 further comprising recovering the oil from the evaporated clarified thin stillage stream after the first evaporator.

10. The process of claim 1 further comprising adding surfactant and/or flocculant to the clarified thin stillage stream prior to subjecting the clarified thin stillage stream, which includes the oil, to evaporation, and recovering the oil from the evaporated clarified thin stillage stream after the first evaporator.

11. A process for clarifying a thin stillage stream in a biofuel production process, the process comprising:

separating a whole stillage byproduct into an insoluble solids portion, including fiber, and a thin stillage stream, including residual insoluble solids and oil;

mechanically separating the thin stillage stream into only a residual insoluble solids stream and a clarified thin stillage stream, which includes additional insoluble solids and the oil,. wherein mechanically separating the thin stillage stream into only the residual insoluble solids stream and the clarified thin stillage stream defines a first treatment of the thin stillage stream;

thereafter, directly combining the separated residual insoluble solids stream with the whole stillage byproduct and/or the insoluble solids portion from the whole stillage byproduct;

mechanically separating out additional insoluble solids from the clarified thin stillage stream as underflow that defines backset, which is directly returned to the process at a step prior to separating the whole stillage byproduct; and

thereafter, subjecting the clarified thin stillage stream, which includes the oil, to evaporation via a first evaporator.

12. The process of claim 11 further comprising adding surfactant and/or flocculant to at least one of the whole stillage byproduct or the clarified thin stillage stream.

13. The process of claim 11 further comprising adding surfactant and/or flocculant to the clarified thin stillage stream prior to subjecting the clarified thin stillage stream to evaporation.

14. The process of claim 11 wherein the biofuel production process is a dry grind biofuel production process.

15. The process of claim 11 further comprising adding surfactant to the clarified thin stillage stream prior to subjecting the clarified thin stillage stream to evaporation.

16. The process of claim 11 wherein the clarified thin stillage stream defines feedstock for zein protein processing, fertilizers, pesticides, nutritional supplements, or pharmaceuticals.

17. The process of claim 11 wherein directly combining the separated residual insoluble solids stream with the whole stillage byproduct and/or the insoluble solids portion from the whole stillage byproduct comprises directly combining the separated residual insoluble solids stream with the whole stillage byproduct and/or the insoluble solids portion from the whole stillage byproduct prior to subjecting the whole stillage byproduct and/or the insoluble solids portion to a dryer.

18. The process of claim 11 wherein mechanically separating out additional insoluble solids from the clarified thin stillage stream comprises separating out the additional insoluble solids from the clarified thin stillage stream as underflow that defines backset, which is directly returned to the process by being directly joined with the whole stillage byproduct prior to separating the whole stillage byproduct.

19. The process of claim 11 further comprising recovering the oil from the evaporated clarified thin stillage stream after the first evaporator.

20. The process of claim 11 further comprising adding surfactant and/or flocculant to the clarified thin stillage stream prior to subjecting the clarified thin stillage stream, which includes the oil, to evaporation, and recovering the oil from the evaporated clarified thin stillage stream after the first evaporator.

Assignments (2)
CHANGE OF NAME Recorded Jun 14, 2019
From: FLUID QUIP PROCESS TECHNOLOGIES, LLC
To: FLUID QUIP TECHNOLOGIES, LLC
Reel/Frame 049476/0914 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2017
From: JAKEL, NEAL; KWIK, JOHN; FRANKO, MICHAEL
To: FLUID QUIP PROCESS TECHNOLOGIES, LLC
Reel/Frame 041525/0714 →
Continuity (2)
Provisional Application 62245318 · Oct 23, 2015
Related Publication 20170114293A1 · Apr 27, 2017