IP Library Granted Patent US 11,014,121
Granted Patent B2
US 11,014,121 · App. 15/301,528 · Granted May 25, 2021

Surface functionalisation method

Inventors: Pascal Viel (Meudon, FR); Thomas Berthelot (Les Ulis, FR); Xavier Lefevre (Lausanne, CH); Jérôme Polesel Maris (Vallieres, FR)
Assignee: Commissariat A L'Energie Atomique Et Aux Energies Alternatives
B05D7/24B05D1/18B05D3/0254B05D3/064B05D3/108B05D3/12B05D7/02C23C18/1889C23C18/1893C23C18/208C23C18/2086B05D3/067B05D3/101B05D2201/00B05D2203/00C23C18/1658C23C18/1831C23C18/2066C23C18/30C23C18/36C23C18/38C23C18/40
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Quick Facts
Patent No.
US 11,014,121
App. No.
15/301,528
Granted
May 25, 2021
Kind
B2
Abstract

The invention relates to a method for functionalising a surface of a solid substrate with at least one acrylic acid polymer layer, said method including the steps of: i) placing the surface in contact with a solution having of at least one acrylic acid homopolymer, a solvent and, optionally, metal salts; ii) removing the solvent from the solution in contact with the surface; and iii) binding the polymer to the surface by thermal treatment.

Claims (17)

1. A process for functionalizing a surface of a solid support with at least one layer of polymer of acrylic acid, said process comprising the stages of:

i) bringing said surface into contact with a solution consisting of:

at least one acrylic acid homopolymer; and

a solvent;

ii) removing the solvent from the solution in contact with said surface; and

iii) fixing the polymer to said surface by heat treatment at a temperature of between 150° C. and 300° C.;

the solid support being selected from the group consisting of metal oxides, papers, and carbon fibers.

2. The process as claimed in claim 1 , in which the polymer is applied to the surface of the solid support by dipping, centrifuging, sprinkling, projection or transfer.

3. The process as claimed in claim 1 , in which the process additionally comprises stages ii 1 ) and ii 2 ), subsequent to stage ii) of:

ii 1 ) rinsing the surface of the solid support obtained in stage ii) with water; and

ii 2 ) drying said surface.

4. The process as claimed in claim 1 , comprising a stage, subsequent to stage iii), of covalent grafting of at least one molecule to the polymer layer obtained.

5. The process as claimed in claim 4 , in which the at least one molecule is a biological molecule or a resin.

6. The process as claimed in claim 4 , in which the at least one molecule consists of two molecules as a two-component resin.

7. The process as claimed in claim 1 , wherein the support comprises metal oxides.

8. The process as claimed in claim 1 , wherein the support is selected from the group consisting of papers and carbon fibers.

9. The process as claimed in claim 1 , wherein the support comprises papers.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 21, 2017
From: VIEL, PASCAL; BERTHELOT, THOMAS; LEFEVRE, XAVIER; POLESEL MARIS, JÉRÔME
To: COMMISSARIAT A L'ENERGIE ATOMIQUE ET AUX ENERGIES ALTERNATIVES
Reel/Frame 042091/0672 →
Priority Claims (1)
FR 1452978 · Apr 3, 2014 · national
Continuity (1)
Related Publication 20170113249A1 · Apr 27, 2017