IP Library Granted Patent US 10,629,321
Granted Patent B2
US 10,629,321 · App. 15/302,319 · Granted Apr 21, 2020

Misfit p-type transparent conductive oxide (TCO) films, methods and applications

Inventors: Mahmut Aksit (Woodbury, MN); Richard D. Robinson (Ithaca, NY)
Assignee: CORNELL UNIVERSITY
H01B1/08B05D1/005B05D3/0254H01L31/022466H01L31/1884B05D2203/30Y02E10/50
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Quick Facts
Patent No.
US 10,629,321
App. No.
15/302,319
Granted
Apr 21, 2020
Kind
B2
Abstract

A p-type transparent conductive oxide (TCO) mixed metal oxide material layer formed upon a substrate has a formula M1 x M2 y O z generally, Ca x Co y O z more specifically, and Ca 3 C o 4O 9 most specifically. Embodiments provide that the p-type TCO mixed metal oxide material may be formed absent an epitaxial crystalline relationship with respect to the substrate while using a sol-gel synthesis method that uses a chelating polymer material and not a block copolymer material.

Claims (12)

1. A p-type transparent conducting structure generated via solution-based synthesis, the structure comprising:

an optically transparent substrate; and

an at least partially crystalline p-type mixed metal oxide material having a chemical composition Ca x Co y O z and located upon the substrate without an epitaxial crystalline relationship with respect to the substrate, wherein when x is normalized to unity y ranges from about 1.2 to about 1.5, and z is selected consistent with x and y, considering the oxidation states of Ca and Co;

wherein the structure has an optical transparency, and further wherein the structure exhibits p-type conductivity greater than 1 S/cm.

2. The structure of claim 1 , wherein:

the at least partially crystalline p-type mixed metal oxide material has the chemical composition Ca 3 Co 4 O 9 .

3. The structure of claim 1 wherein:

the mixed metal oxide material has an optical transparency in the visible range from about 31 to about 67 percent; and

the mixed metal oxide material comprises a misfit crystal material.

4. The structure of claim 3 wherein the mixed metal oxide material shows no more than five peaks in an x-ray diffraction spectrum from 10 to 40 degrees position of 2⊖.

5. The structure of claim 1 , wherein the mixed metal oxide material has an optical transparency in the near infrared range greater than 85%.

6. The structure of claim 1 , wherein the structure exhibits conductivity greater than 15 S/cm.

Assignments (2)
CONFIRMATORY LICENSE Recorded Dec 14, 2016
From: CORNELL UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 040939/0986 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 6, 2016
From: AKSIT, MAHMUT; ROBINSON, RICHARD D.
To: CORNELL UNIVERSITY
Reel/Frame 039958/0295 →
Continuity (2)
Provisional Application 61977419 · Apr 9, 2014
Related Publication 20170025196A1 · Jan 26, 2017