IP Library Granted Patent US 10,000,454
Granted Patent B2
US 10,000,454 · App. 15/310,488 · Granted Jun 19, 2018

Antidiabetic tricyclic compounds

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Quick Facts
Patent No.
US 10,000,454
App. No.
15/310,488
Granted
Jun 19, 2018
Kind
B2
Abstract

Novel compounds of the structural formula (I), and the pharmaceutically acceptable salts thereof, are agonists of G-protein coupled receptor 40 (GPR40) and may be useful in the treatment, prevention and suppression of diseases mediated by the G-protein-coupled receptor 40. The compounds of the present invention may be useful in the treatment of Type 2 diabetes mellitus, and of conditions that are often associated with this disease, including obesity and lipid disorders, such as mixed or diabetic dyslipidemia, hyperlipidemia, hypercholesterolemia, and hypertriglyceridemia.

Claims (703)

1. A compound of structural formula A:

or a pharmaceutically acceptable salt thereof; wherein

X is selected from the group consisting of:

(1) oxygen, and

(2) NR 7 ;

T is CH;

U is CH;

V is N;

W is CH;

A is selected from the group consisting of:

wherein A is unsubstituted or substituted with one to six substituents selected from R a , and wherein two R a substituents together with the carbon atom to which they are attached may form a 3-6 membered cycloalkyl ring or a 3-6 membered cycloheteroalkyl ring containing 0 to 3 heteroatoms independently selected from oxygen, sulfur, and NR 8 , and wherein each 3-6 membered cycloalkyl and each 3-6 membered cycloheteroalkyl ring is unsubstituted or substituted with 1 to 4 substituents selected from: —C 1-6 alkyl, —O—C 1-6 alkyl, halogen and OH;

B is selected from the group consisting of:

(1) C 1-6 alkyl,

(2) aryl,

(3) aryl-O—,

(4) C 3-6 cycloalkyl-,

(5) C 3-6 cycloalkyl-C 1-10 alkyl-,

(6) C 3-6 cycloalkyl-C 1-10 alkyl-O—,

(7) C 2-5 cycloheteroalkyl-,

(8) C 3-6 cycloheteroalkyl-C 1-10 alkyl-,

(9) C 3-6 cycloheteroalkyl-C 1-10 alkyl-O—,

(10) heteroaryl,

(11) heteroaryl-O—,

(12) aryl-C 1-10 alkyl-, and

(13) heteroaryl-C 1-10 alkyl-;

wherein B is unsubstituted or substituted with one to six substituents selected from R b ;

each R 1 is independently selected from the group consisting of:

(1) hydrogen,

(2) halogen,

(3) —OR e ,

(4) —CN,

(5) —C 1-6 alkyl, and

(6) —C 3-6 cycloalkyl,

wherein each alkyl and cycloalkyl is unsubstituted or substituted with one to three substituents selected from R i ;

R 2 is selected from the group consisting of:

(1) hydrogen,

(2) —C 1-6 alkyl, and

(3) —C 3-6 cycloalkyl,

wherein each alkyl and cycloalkyl is unsubstituted or substituted with one to three substituents selected from R j ;

each R 3 is independently selected from the group consisting of:

(1) hydrogen,

(2) halogen,

(3) —OR e ,

(4) —C 1-6 alkyl,

(5) —C 2-6 alkenyl,

(6) —C 2-6 alkynyl,

(7) —C 3-6 cycloalkyl, and

(8) —C 2-6 cycloheteroalkyl,

wherein each alkyl, alkenyl, alkynyl, cycloalkyl and cycloheteroalkyl is unsubstituted or substituted with one to three substituents selected from R L ;

each R 4 is independently selected from the group consisting of:

(1) hydrogen,

(2) halogen,

(3) —OR e ,

(4) —C 1-6 alkyl,

(5) —C 2-6 alkenyl,

(6) —C 2-6 alkynyl,

(7) —C 3-6 cycloalkyl, and

(8) —C 2-6 cycloheteroalkyl,

wherein each alkyl, alkenyl, alkynyl, and cycloalkyl is unsubstituted or substituted with one to three substituents selected from R L ;

R 5 is selected from the group consisting of:

(1) hydrogen,

(2) —C 1-3 alkyl, and

(3) halogen;

R 6 is selected from the group consisting of:

(1) hydrogen,

(2) —C 1-3 alkyl, and

(3) halogen, or

R 5 and R 6 can together form oxo;

R 7 is selected from the group consisting of:

(1) hydrogen,

(2) —C(O)R e , and

(3) —C 1-10 alkyl,

wherein —C 1-10 alkyl is unsubstituted or substituted with one to five fluorines;

each R 8 is selected from the group consisting of:

(1) hydrogen,

(2) —C(O)R e , and

(3) —C 1-10 alkyl,

wherein —C 1-10 alkyl is unsubstituted or substituted with one to five fluorines;

each R 9 is selected from the group consisting of:

(1) hydrogen, and

(2) —C 1-6 alkyl,

wherein —C 1-6 alkyl is unsubstituted or substituted with one to five fluorines;

each R a is independently selected from the group consisting of:

(1) —C 1-6 alkyl,

(2) —O—C 1-6 alkyl,

(3) halogen,

(4) oxo,

(5) —OR e ,

(6) —N(R c )S(O) m R e ,

(7) —S(O) m R e ,

(8) —S(O) m NR c R d ,

(9) —NR c R d ,

(10) —C(O)R e ,

(11) —OC(O)R e ,

(12) —CO 2 R e ,

(13) —CN,

(14) —C(O)NR c R d ,

(15) —N(R c )C(O)R e ,

(16) —N(R c )C(O)OR e ,

(17) —N(R c )C(O)NR c R d ,

(18) —CF 3 ,

(19) —OCF 3 ,

(20) —OCHF 2 ,

(21) —(CH 2 ) p —C 3-6 cycloalkyl,

(22) —(CH 2 ) p —C 2-10 cycloheteroalkyl,

(23) —(CH 2 ) p -aryl, and

(24) —(CH 2 ) p -heteroaryl,

wherein R a is unsubstituted or substituted with one to three substituents selected from R m ;

each R b is independently selected from the group consisting of:

(1) —C 1-10 alkyl,

(2) —O—C 1-10 alkyl,

(3) —C 2-10 alkenyl,

(4) halogen,

(5) —OH,

(6) —OC 2-10 alkenyl,

(7) —O(CH 2 )pOC 1-10 alkyl,

(8) —O(CH 2 )pC 3-6 cycloalkyl,

(9) —O(CH 2 )pC 2-10 cycloheteroalkyl,

(10) —O(CH 2 )p-aryl,

(11) —O(CH 2 )p-heteroaryl,

(12) —N(R c )S(O) m R e ,

(13) —S(O) m R e ,

(14) —O(CH 2 )p-S(O) m R e ,

(15) —S(O) m NR c R d ,

(16) —NR c R d ,

(17) —C(O)R e ,

(18) —OC(O)R e ,

(19) —CO 2 R e ,

(20) —CN,

(21) —C(O)NR c R d ,

(22) —N(R c )C(O)R e ,

(23) —N(R c )C(O)OR e ,

(24) —N(R c )C(O)NR c R d ,

(25) —O(CH 2 )pO-C 3-6 cycloalkyl,

(26) —O(CH 2 )pO-C 2-10 cycloheteroalkyl,

(27) —CF 3 ,

(28) —OCF 3 ,

(29) —OCHF 2 ,

(30) —(CH 2 )p-C 3-6 cycloalkyl,

(31) —(CH 2 )p-C 2-10 cycloheteroalkyl,

(32) —(CH 2 )p-aryl, and

(33) —(CH 2 )p-heteroaryl,

wherein each R b is unsubstituted or substituted with one to five substituents selected from R k ;

each R c and R d is independently selected from the group consisting of:

(1) hydrogen,

(2) —C 1-10 alkyl,

(3) —C 2-10 alkenyl,

(4) —C 3-6 cycloalkyl,

(5) C 3-6 cycloalkyl-C 1-10 alkyl-,

(6) —C 2-6 cycloheteroalkyl,

(7) C 2-6 cycloheteroalkyl-C 1-10 alkyl-,

(8) aryl,

(9) heteroaryl,

(10) aryl-C 1-10 alkyl-, and

(11) heteroaryl-C 1-10 alkyl-, or

R c and R d together with the atom(s) to which they are attached form a cycloheteroalkyl ring of 4 to 7 members containing 0-2 additional heteroatoms independently selected from oxygen, sulfur and N—R g , and wherein each R c and R d is unsubstituted or substituted with one to three substituents independently selected from R f ;

each R e is independently selected from the group consisting of:

(1) hydrogen,

(2) —C 1-10 alkyl,

(3) —C 2-10 alkenyl,

(4) —C 3-6 cycloalkyl,

(5) —C 3-6 cycloalkyl-C 1-10 alkyl-,

(6) —C 2-5 cycloheteroalkyl,

(7) —C 2-5 cycloheteroalkyl-C 1-10 alkyl-,

(8) aryl,

(9) heteroaryl,

(10) aryl-C 1-10 alkyl-, and

(11) heteroaryl-C 1-10 alkyl-,

wherein each R e is unsubstituted or substituted with one to three substituents selected from R h ;

each R f is selected from the group consisting of:

(1) halogen,

(2) —C 1-10 alkyl,

(3) —OH,

(4) —OC 1-6 alkyl,

(5) —S(O) m —C 1-4 alkyl,

(6) —CN,

(7) —CF 3 ,

(8) —OCHF 2 , and

(9) —OCF 3 ,

wherein each alkyl is unsubstituted or substituted with one to three substituents independently selected from: —OH, halogen, cyano, and —S(O) 2 CH 3 ;

each R g is selected from the group consisting of:

(1) hydrogen,

(2) —C(O)R e , and

(3) —C 1-10 alkyl,

wherein alkyl is unsubstituted or substituted with one to five fluorines;

each R h is selected from the group consisting of:

(1) halogen,

(2) —C 1-10 alkyl,

(3) —OH,

(4) —O—C 1-4 alkyl,

(5) —S(O) m —C 1-4 alkyl,

(6) —CN,

(7) —CF 3 ,

(8) —OCHF 2 , and

(9) —OCF 3 ,

wherein each alkyl is unsubstituted or substituted with one to three substituents independently selected from: —OH, halogen, cyano, and —S(O) 2 CH 3 ;

R i is independently selected from the group consisting of:

(1) —C 1-6 alkyl,

(2) —OR e ,

(3) —N(R c )S(O) m R e ,

(4) halogen,

(5) —S(O) m R e ,

(6) —S(O) m NR c R d ,

(7) —NR c R d ,

(8) —C(O)R e ,

(9) —OC(O)R e ,

(10) —CO 2 R e ,

(11) —CN,

(12) —C(O)NR c R d ,

(13) —N(R c )C(O)R e ,

(14) —N(R c )C(O)OR e ,

(15) —N(R c )C(O)NR c R d ,

(16) —CF 3 ,

(17) —OCF 3 ,

(18) —OCHF 2 ,

(19) —C 3-6 cycloalkyl, and

(20) —C 2-5 cycloheteroalkyl;

R j is independently selected from the group consisting of:

(1) —C 1-6 alkyl,

(2) —OR e ,

(3) —N(R c )S(O) m R e ,

(4) halogen,

(5) —S(O) m R e ,

(6) —S(O) m NR c R d ,

(7) —NR c R d ,

(8) —C(O)R e ,

(9) —OC(O)R e ,

(10) —CO 2 R e ,

(11) —CN,

(12) —C(O)NR c R d ,

(13) —N(R c )C(O)R e ,

(14) —N(R c )C(O)OR e ,

(15) —N(R c )C(O)NR c R d ,

(16) —CF 3 ,

(17) —OCF 3 ,

(18) —OCHF 2 ,

(19) —C 3-6 cycloalkyl, and

(20) —C 2-5 cycloheteroalkyl;

each R k is independently selected from the group consisting of:

(1) halogen,

(2) —C 1-6 alkyl,

(3) —OH,

(4) oxo,

(5) —OC 1-6 alkyl,

(6) —SO 2 —C 1-6 alkyl,

(7) —C 1-6 alkyl-SO 2 C 1-6 alkyl,

(8) —CN,

(9) —CF 3 ,

(10) —OCHF 2 ,

(11) —OCF 3 ,

(12) —NH 2 ,

(13) —NHSO 2 C 1-6 alkyl,

(14) —NHC(O)C 1-6 alkyl,

(15) ═N(OCH 3 ),

(16) —P(O)(OH) 2 , and

(17) —P(O)(OC 1-6 alkyl) 2 ,

wherein each alkyl is unsubstituted or substituted with one to three substituents independently selected from: —OH, —OC 1-6 alkyl, halogen, cyano, and —S(O) 2 C 1-6 alkyl;

R L is selected from the group consisting of:

(1) —C 1-6 alkyl,

(2) halogen,

(3) —OR e ,

(4) —N(R c )S(O) m R e ,

(5) —S(O) m R e ,

(6) —S(O) m NR c R d ,

(7) —NR c R d ,

(8) —C(O)R e ,

(9) —OC(O)R e ,

(10) —CO 2 R e ,

(11) —CN,

(12) —C(O)NR c R d ,

(13) —N(R c )C(O)R e ,

(14) —N(R c )C(O)OR e ,

(15) —N(R c )C(O)NR c R d ,

(16) —CF 3 ,

(17) —OCF 3 ,

(18) —OCHF 2 ,

(19) —C 3-6 cycloalkyl, and

(20) —C 2-5 cycloheteroalkyl;

each R m is independently selected from the group consisting of:

(1) halogen,

(2) —C 1-6 alkyl,

(3) —OH,

(4) oxo,

(5) —OC 1-6 alkyl,

(6) —SO 2 —C 1-6 alkyl,

(7) —C 1-6 alkyl-SO 2 C 1-6 alkyl,

(8) —CN,

(9) —CF 3 ,

(10) —OCHF 2 ,

(11) —OCF 3 ,

(12) —NH 2 ,

(13) —NHSO 2 C 1-6 alkyl,

(14) —NHC(O)C 1-6 alkyl,

(15) ═N(OCH 3 ),

(16) —P(O)(OH) 2 , and

(17) —P(O)(OC 1-6 alkyl) 2 ,

wherein each C 1-10 alkyl is unsubstituted or substituted with one to three substituents independently selected from: —OH, —OC 1-6 alkyl, halogen, cyano, and —S(O) 2 C 1-6 alkyl;

n is 1;

each m is independently 0, 1 or 2;

each p is independently selected from: 0, 1, 2, 3, 4, 5, 6, 7, 8, 9 or 10; and

q is independently selected from: 1, 2 or 3;

or a pharmaceutically acceptable salt thereof.

2. A compound of structural formula I:

wherein

X is selected from the group consisting of:

(1) oxygen, and

(2) NR 7 ;

T is CH;

U is CH;

V is N;

W is CH;

A is selected from the group consisting of:

wherein A is unsubstituted or substituted with one to six substituents selected from R a , and wherein two R a substituents together with the carbon atom to which they are attached may form a 3-6 membered cycloalkyl ring or a 3-6 membered cycloheteroalkyl ring containing 0 to 3 heteroatoms independently selected from oxygen, sulfur, and NR 8 , and wherein each 3-6 membered cycloalkyl and each 3-6 membered cycloheteroalkyl ring is unsubstituted or substituted with 1 to 4 substituents selected from: —C 1-6 alkyl, —O—C 1-6 alkyl, halogen and OH

B is selected from the group consisting of:

(1) aryl,

(2) aryl-O—,

(3) C 3-6 cycloalkyl-,

(4) C 3-6 cycloalkyl-C 1-10 alkyl-,

(5) C 3-6 cycloalkyl-C 1-10 alkyl-O—,

(6) C 2-5 cycloheteroalkyl-,

(7) C 3-6 cycloheteroalkyl-C 1-10 alkyl-,

(8) C 3-6 cycloheteroalkyl-C 1-10 alkyl-O—,

(9) heteroaryl,

(10) heteroaryl-O—,

(11) aryl-C 1-10 alkyl-, and

(12) heteroaryl-C 1-10 alkyl-;

wherein B is unsubstituted or substituted with one to six substituents selected from R b ;

each R 1 is independently selected from the group consisting of:

(1) hydrogen,

(2) halogen,

(3) —OR e ,

(4) —CN,

(5) —C 1-6 alkyl, and

(6) —C 3-6 cycloalkyl,

wherein each alkyl and cycloalkyl is unsubstituted or substituted with one to three substituents selected from R 1 ;

R 2 is selected from the group consisting of:

(1) hydrogen,

(2) —C 1-6 alkyl, and

(3) —C 3-6 cycloalkyl,

wherein each alkyl and cycloalkyl is unsubstituted or substituted with one to three substituents selected from R j ;

each R 3 is independently selected from the group consisting of:

(1) hydrogen,

(2) halogen,

(3) —OR e ,

(4) —C 1-6 alkyl,

(5) —C 2-6 alkenyl,

(6) —C 2-6 alkynyl,

(7) —C 3-6 cycloalkyl, and

(8) —C 2-6 cycloheteroalkyl,

wherein each alkyl, alkenyl, alkynyl, cycloalkyl and cycloheteroalkyl is unsubstituted or substituted with one to three substituents selected from R L ;

each R 4 is independently selected from the group consisting of:

(1) hydrogen,

(2) halogen,

(3) —OR e ,

(4) —C 1-6 alkyl,

(5) —C 2-6 alkenyl,

(6) —C 2-6 alkynyl,

(7) —C 3-6 cycloalkyl, and

(8) —C 2-6 cycloheteroalkyl,

wherein each alkyl, alkenyl, alkynyl, and cycloalkyl is unsubstituted or substituted with one to three substituents selected from R L ;

R 5 is selected from the group consisting of:

(1) hydrogen,

(2) —C 1-3 alkyl, and

(3) halogen;

R 6 is selected from the group consisting of:

(1) hydrogen,

(2) —C 1-3 alkyl, and

(3) halogen, or

R 5 and R 6 can together form oxo;

R 7 is selected from the group consisting of:

(1) hydrogen,

(2) —C(O)R e , and

(3) —C 1-10 alkyl,

wherein —C 1-10 alkyl is unsubstituted or substituted with one to five fluorines;

each R 8 is selected from the group consisting of:

(1) hydrogen,

(2) —C(O)R e , and

(3) —C 1-10 alkyl,

wherein —C 1-10 alkyl is unsubstituted or substituted with one to five fluorines;

each R a is independently selected from the group consisting of:

(1) —C 1-6 alkyl,

(2) —O—C 1-6 alkyl,

(3) halogen,

(4) oxo,

(5) —OR e ,

(6) —N(R c )S(O) m R e ,

(7) —S(O) m R e ,

(8) —S(O) m NR c R d ,

(9) —NR c R d ,

(10) —C(O)R e ,

(11) —OC(O)R e ,

(12) —CO 2 R e ,

(13) —CN,

(14) —C(O)NR c R d ,

(15) —N(R c )C(O)R e ,

(16) —N(R c )C(O)OR e ,

(17) —N(R c )C(O)NR c R d ,

(18) —CF 3 ,

(19) —OCF 3 ,

(20) —OCHF 2 ,

(21) —(CH 2 ) p —C 3-6 cycloalkyl,

(22) —(CH 2 ) p —C 2-10 cycloheteroalkyl,

(23) —(CH 2 ) p -aryl, and

(24) —(CH 2 ) p -heteroaryl,

wherein R a is unsubstituted or substituted with one to three substituents selected from R m ;

each R b is independently selected from the group consisting of:

(1) —C 1-10 alkyl,

(2) —O—C 1-10 alkyl,

(3) —C 2-10 alkenyl,

(4) halogen,

(5) —OH,

(6) —OC 2-10 alkenyl,

(7) —O(CH 2 )pOC 1-10 alkyl,

(8) —O(CH 2 )pC 3-6 cycloalkyl,

(9) —O(CH 2 )pC 2-10 cycloheteroalkyl,

(10) —O(CH 2 )p-aryl,

(11) —O(CH 2 )p-heteroaryl,

(12) —N(R c )S(O) m R e ,

(13) —S(O) m R e ,

(14) —O(CH 2 )p-S(O) m R e ,

(15) —S(O) m NR c R d ,

(16) —NR c R d ,

(17) —C(O)R e ,

(18) —OC(O)R e ,

(19) —CO 2 R e ,

(20) —CN,

(21) —C(O)NR c R d ,

(22) —N(R c )C(O)R e ,

(23) —N(R c )C(O)OR e ,

(24) —N(R c )C(O)NR c R d ,

(25) —O(CH 2 )pO-C 3-6 cycloalkyl,

(26) —O(CH 2 )pO-C 2-10 cycloheteroalkyl,

(27) —CF 3 ,

(28) —OCF 3 ,

(29) —OCHF 2 ,

(30) —(CH 2 )p-C 3-6 cycloalkyl,

(31) —(CH 2 )p-C 2-10 cycloheteroalkyl,

(32) —(CH 2 )p-aryl, and

(33) —(CH 2 )p-heteroaryl,

wherein each R b is unsubstituted or substituted with one to five substituents selected from R k ;

each R c and R d is independently selected from the group consisting of:

(1) hydrogen,

(2) —C 1-10 alkyl,

(3) —C 2-10 alkenyl,

(4) —C 3-6 cycloalkyl,

(5) C 3-6 cycloalkyl-C 1-10 alkyl-,

(6) —C 2-6 cycloheteroalkyl,

(7) C 2-6 cycloheteroalkyl-C 1-10 alkyl-,

(8) aryl,

(9) heteroaryl,

(10) aryl-C 1-10 alkyl-, and

(11) heteroaryl-C 1-10 alkyl-, or

R c and R d together with the atom(s) to which they are attached form a cycloheteroalkyl ring of 4 to 7 members containing 0-2 additional heteroatoms independently selected from oxygen, sulfur and N—R g , and wherein each R c and R d is unsubstituted or substituted with one to three substituents independently selected from R f ;

each R e is independently selected from the group consisting of:

(1) hydrogen,

(2) —C 1-10 alkyl,

(3) —C 2-10 alkenyl,

(4) —C 3-6 cycloalkyl,

(5) —C 3-6 cycloalkyl-C 1-10 alkyl-,

(6) —C 2-5 cycloheteroalkyl,

(7) —C 2-5 cycloheteroalkyl-C 1-10 alkyl-,

(8) aryl,

(9) heteroaryl,

(10) aryl-C 1-10 alkyl-, and

(11) heteroaryl-C 1-10 alkyl-,

wherein each R e is unsubstituted or substituted with one to three substituents selected from R h ;

each R f is selected from the group consisting of:

(1) halogen,

(2) —C 1-10 alkyl,

(3) —OH,

(4) —OC 1-6 alkyl,

(5) —S(O) m —C 1-4 alkyl,

(6) —CN,

(7) —CF 3 ,

(8) —OCHF 2 , and

(9) —OCF 3 ,

wherein each alkyl is unsubstituted or substituted with one to three substituents independently selected from: —OH, halogen, cyano, and —S(O) 2 CH 3 ;

each R g is selected from the group consisting of:

(1) hydrogen,

(2) —C(O)R e , and

(3) —C 1-10 alkyl,

wherein alkyl is unsubstituted or substituted with one to five fluorines;

each R h is selected from the group consisting of:

(1) halogen,

(2) —C 1-10 alkyl,

(3) —OH,

(4) —O—C 1-4 alkyl,

(5) —S(O) m —C 1-4 alkyl,

(6) —CN,

(7) —CF 3 ,

(8) —OCHF 2 , and

(9) —OCF 3 ,

wherein each alkyl is unsubstituted or substituted with one to three substituents independently selected from: —OH, halogen, cyano, and —S(O) 2 CH 3 ;

R i is independently selected from the group consisting of:

(1) —C 1-6 alkyl,

(2) —OR e ,

(3) —N(R c )S(O) m R e ,

(4) halogen,

(5) —S(O) m R e ,

(6) —S(O) m NR c R d ,

(7) —NR c R d ,

(8) —C(O)R e ,

(9) —OC(O)R e ,

(10) —CO 2 R e ,

(11) —CN,

(12) —C(O)NR c R d ,

(13) —N(R c )C(O)R e ,

(14) —N(R c )C(O)OR e ,

(15) —N(R c )C(O)NR c R d ,

(16) —CF 3 ,

(17) —OCF 3 ,

(18) —OCHF 2 ,

(19) —C 3-6 cycloalkyl, and

(20) —C 2-5 cycloheteroalkyl;

R j is independently selected from the group consisting of:

(1) —C 1-6 alkyl,

(2) —OR e ,

(3) —N(R c )S(O) m R e ,

(4) halogen,

(5) —S(O) m R e ,

(6) —S(O) m NR c R d ,

(7) —NR c R d ,

(8) —C(O)R e ,

(9) —OC(O)R e ,

(10) —CO 2 R e ,

(11) —CN,

(12) —C(O)NR c R d ,

(13) —N(R c )C(O)R e ,

(14) —N(R c )C(O)OR e ,

(15) —N(R c )C(O)NR c R d ,

(16) —CF 3 ,

(17) —OCF 3 ,

(18) —OCHF 2 ,

(19) —C 3-6 cycloalkyl, and

(20) —C 2-5 cycloheteroalkyl;

each R k is independently selected from the group consisting of:

(1) halogen,

(2) —C 1-6 alkyl,

(3) —OH,

(4) oxo,

(5) —OC 1-6 alkyl,

(6) —SO 2 —C 1-6 alkyl,

(7) —C 1-6 alkyl-SO 2 C 1-6 alkyl,

(8) —CN,

(9) —CF 3 ,

(10) —OCHF 2 ,

(11) —OCF 3 ,

(12) —NH 2 ,

(13) —NHSO 2 C 1-6 alkyl,

(14) —NHC(O)C 1-6 alkyl,

(15) ═N(OCH 3 ),

(16) —P(O)(OH) 2 , and

(17) —P(O)(OC 1-6 alkyl) 2 ,

wherein each alkyl is unsubstituted or substituted with one to three substituents independently selected from: —OH, —OC 1-6 alkyl, halogen, cyano, and —S(O) 2 C 1-6 alkyl;

R L is selected from the group consisting of:

(1) —C 1-6 alkyl,

(2) halogen,

(3) —OR e ,

(4) —N(R c )S(O) m R e ,

(5) —S(O) m R e ,

(6) —S(O) m NR c R d ,

(7) —NR c R d ,

(8) —C(O)R e ,

(9) —OC(O)R e ,

(10) —CO 2 R e ,

(11) —CN,

(12) —C(O)NR c R d ,

(13) —N(R c )C(O)R e ,

(14) —N(R c )C(O)OR e ,

(15) —N(R c )C(O)NR c R d ,

(16) —CF 3 ,

(17) —OCF 3 ,

(18) —OCHF 2 ,

(19) —C 3-6 cycloalkyl, and

(20) —C 2-5 cycloheteroalkyl;

each R m is independently selected from the group consisting of:

(1) halogen,

(2) —C 1-6 alkyl,

(3) —OH,

(4) oxo,

(5) —OC 1-6 alkyl,

(6) —SO 2 —C 1-6 alkyl,

(7) —C 1-6 alkyl-SO 2 C 1-6 alkyl,

(8) —CN,

(9) —CF 3 ,

(10) —OCHF 2 ,

(11) —OCF 3 ,

(12) —NH 2 ,

(13) —NHSO 2 C 1-6 alkyl,

(14) —NHC(O)C 1-6 alkyl,

(15) ═N(OCH 3 ),

(16) —P(O)(OH) 2 , and

(17) —P(O)(OC 1-6 alkyl) 2 ,

wherein each C 1-10 alkyl is unsubstituted or substituted with one to three substituents independently selected from: —OH, —OC 1-6 alkyl, halogen, cyano, and —S(O) 2 C 1-6 alkyl;

n is 1;

each m is independently 0, 1 or 2;

each p is independently selected from: 0, 1, 2, 3, 4, 5, 6, 7, 8, 9 or 10; and

q is independently selected from: 1, 2 or 3;

or a pharmaceutically acceptable salt thereof.

3. The compound according to claim 1 of structural formula Ia

or a pharmaceutically acceptable salt thereof.

4. The compound according to claim 1 wherein R 1 is hydrogen; or a pharmaceutically acceptable salt thereof.

5. The compound according to claim 1 wherein X is oxygen; or a pharmaceutically acceptable salt thereof.

6. The compound according to claim 1 wherein A is selected from the group consisting of:

wherein A is unsubstituted or substituted with one to six substituents selected from R a , and wherein two R a substituents together with the carbon atom to which they are attached may form a 3-6 membered cycloalkyl ring or a 3-6 membered cycloheteroalkyl ring containing 0 to 3 heteroatoms independently selected from oxygen, sulfur, and NR 8 , and wherein each 3-6 membered cycloalkyl ring and each 3-6 membered cycloheteroalkyl ring is unsubstituted or substituted with 1 to 4 substituents selected from: —C 1-6 alkyl, —O—C 1-6 alkyl, halogen and OH;

or a pharmaceutically acceptable salt thereof.

7. The compound according to claim 1 wherein A is selected from the group consisting of:

wherein A is unsubstituted or substituted with one to six substituents selected from R a ;

or a pharmaceutically acceptable salt thereof.

8. The compound according to claim 1 wherein B is selected from the group consisting of:

(1) aryl, and

(2) heteroaryl,

wherein each aryl and heteroaryl is unsubstituted or substituted with one to six substituents selected from R b ;

or a pharmaceutically acceptable salt thereof.

9. The compound according to claim 1 wherein B is selected from the group consisting of:

(1) phenyl,

(2) pyridine and

(3) benzimidazole,

wherein each phenyl, pyridine and benzimidazole is unsubstituted or substituted with one to six substituents selected from R b ;

or a pharmaceutically acceptable salt thereof.

10. The compound according to claim 1 wherein R 3 and R 4 are independently selected from the group consisting of:

(1) hydrogen,

(2) halogen, and

(3) —C 1-6 alkyl,

wherein each alkyl is unsubstituted or substituted with one to three substituents selected from R L ; or a pharmaceutically acceptable salt thereof.

11. The compound according to claim 1 wherein R 3 and R 4 are hydrogen; or a pharmaceutically acceptable salt thereof.

12. The compound according to claim 1 wherein R 2 is hydrogen; or a pharmaceutically acceptable salt thereof.

13. The compound according to claim 1 wherein R 5 and R 6 are selected from the group consisting of:

(1) hydrogen, and

(2) halogen;

or a pharmaceutically acceptable salt thereof.

14. The compound according to claim 1 wherein R 5 and R 6 are hydrogen; or a pharmaceutically acceptable salt thereof.

15. The compound according to claim 1 wherein the absolute stereochemistry at the two stereogenic carbon centers is indicated below:

or a pharmaceutically acceptable salt thereof.

16. The compound according to claim 1 of structural formula Ia

wherein:

X is oxygen;

T is CH;

U is CH;

V is N;

W is CH;

A is selected from the group consisting of:

wherein A is unsubstituted or substituted with one to six substituents selected from R a , and wherein two R a substituents together with the carbon atom to which they are attached may form a 3-6 membered cycloalkyl ring or a 3-6 membered cycloheteroalkyl ring containing 0 to 3 heteroatoms independently selected from oxygen, sulfur, and NR 8 , and wherein each 3-6 membered cycloalkyl ring and each 3-6 membered cycloheteroalkyl ring is unsubstituted or substituted with 1 to 4 substituents selected from: —C 1-6 alkyl, —O—C 1-6 alkyl, halogen and OH;

B is selected from the group consisting of:

(1) aryl, and

(2) heteroaryl,

wherein each aryl and heteroaryl is unsubstituted or substituted with one to six substituents selected from R b ;

R 1 and R 2 are hydrogen;

R 3 and R 4 are independently selected from the group consisting of:

(1) hydrogen,

(2) halogen, and

(3) —C 1-6 alkyl,

wherein each alkyl is unsubstituted or substituted with one to three substituents selected from R L ;

R 5 and R 6 are selected from the group consisting of:

(1) hydrogen, and

(2) halogen; and

n is 1;

or a pharmaceutically acceptable salt thereof.

17. The compound according to claim 1 of structural formula Ia

wherein:

X is oxygen;

T is CH;

V is N;

W is CH;

A is selected from the group consisting of:

wherein A is unsubstituted or substituted with one to six substituents selected from R a ;

B is selected from the group consisting of:

(1) phenyl,

(2) pyridine, and

(3) benzimidazole,

wherein each phenyl, pyridine and benzimidazole is unsubstituted or substituted with one to six substituents selected from R b ;

R 1 , R 2 , R 3 , R 4 , R 5 and R 6 are hydrogen; and

n is 1;

or a pharmaceutically acceptable salt thereof.

18. A compound selected from:

or a pharmaceutically acceptable salt thereof.

19. A pharmaceutical composition comprising a compound of claim 1 , or a pharmaceutically acceptable salt thereof, and a pharmaceutically acceptable carrier.

20. A method of treating type 2 diabetes mellitus in a patient in need of treatment comprising the administration to the patient of a therapeutically effective amount of a compound of claim 1 , or a pharmaceutically acceptable salt thereof.

21. A pharmaceutical composition comprising

(1) a compound of claim 1 or a pharmaceutically acceptable salt thereof,

(2) one or more compounds selected from the group consisting of:

(a) PPAR gamma agonists and partial agonists;

(b) biguanides;

(c) protein tyrosine phosphatase-1B (PTP-1B) inhibitors;

(d) dipeptidyl peptidase IV (DP-IV) inhibitors;

(e) insulin or an insulin mimetic;

(f) sulfonylureas;

(g) α-glucosidase inhibitors;

(h) agents which improve a patient's lipid profile, said agents being selected from the group consisting of (i) HMG-CoA reductase inhibitors, (ii) bile acid sequestrants, (iii) nicotinyl alcohol, nicotinic acid or a salt thereof, (iv) PPARα agonists, (v) cholesterol absorption inhibitors, (vi) acyl CoA: cholesterol acyltransferase (ACAT) inhibitors, (vii) CETP inhibitors, and (viii) phenolic anti-oxidants;

(i) PPARα/γ dual agonists,

(j) PPARδ agonists,

(k) antiobesity compounds,

(l) ileal bile acid transporter inhibitors;

(m) anti-inflammatory agents;

(n) glucagon receptor antagonists;

(o) GLP-1;

(p) GIP-1;

(q) GLP-1 analogs;

(r) HSD-1 inhibitors;

(s) SGLT 1 inhibitors; and

(t) SGLT 2 inhibitors; and

(3) a pharmaceutically acceptable carrier.

22. A pharmaceutical composition comprising a compound according to claim 1 , or a pharmaceutically acceptable salt thereof, and a compound selected from simvastatin, ezetimibe and sitagliptin; and a pharmaceutically acceptable carrier.

Assignments (4)
MERGER Recorded Aug 8, 2022
From: MERCK SHARP & DOHME CORP.
To: MERCK SHARP & DOHME LLC
Reel/Frame 061102/0145 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 11, 2016
From: CHEN, ZHENGXIA; CUI, MINGXIANG; HU, BIN
To: WUXI APPTEC (SHANGHAI) CO., LTD.
Reel/Frame 040284/0082 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 11, 2016
From: WUXI APPTEC (SHANGHAI) CO., LTD.
To: MERCK SHARP & DOHME CORP.
Reel/Frame 040284/0311 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 11, 2016
From: BIFTU, TESFAYE; BIJU, PURAKKATTLE; BLIZZARD, TIMOTHY A.; CLEMENTS, MATTHEW J.; FRIE, JESSICA L.; HAGMANN, WILLIAM K.; JOSIEN, HUBERT; NAIR, ANILKUMAR G.; PLUMMER, CHRISTOPHER W.; ZHU, CHENG
To: MERCK SHARP & DOHME CORP.
Reel/Frame 040591/0385 →