IP Library › Granted Patent US 10,471,512
Granted Patent B2
US 10,471,512 · App. 15/314,372 · Granted Nov 12, 2019

Method of producing a powder product

Inventors: Chull Hee Oh (Victoria, AU); Stefan Gulizia (Victoria, AU)
Assignee: Commonwealth Scientific and Industrial Research Organisation
B22F9/04B02C18/062B22F1/0003B33Y70/00C22C14/00B22F2009/042B22F2009/045B22F2301/205C22C1/0458
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Quick Facts
Patent No.
US 10,471,512
App. No.
15/314,372
Granted
Nov 12, 2019
Kind
B2
Abstract

A method of producing a powder suitable for additive manufacturing and/or powder metallurgy applications from a precursor particulate material comprising: subjecting the precursor particulate material to at least one high shear milling process, thereby producing a powder product having a reduced average particle size and a selected particle morphology.

Claims (17)

1. A method of producing an additive manufacturing and/or powder metallurgy powder from a precursor particulate material comprising irregularly shaped Titanium or Titanium alloy particulate material, said method comprising:

subjecting the precursor particulate material to at least one high shear milling process comprising milling the material with at least one high shear mixer which includes a rotor configured to contact and comminute the precursor particulate material and a stator which extends substantially around the rotor,

thereby producing a Ti or Ti alloy powder product having a reduced average particle size and a particle morphology comprising a substantially uniform shaped particle selected from at least one of angular, platelet, spherical, rod or cylindrical shaped particles.

2. A method according to claim 1 , wherein the powder product has a particle size range in which at least 90% of the particles have an average particle size <300 μm.

3. A method according to claim 1 , wherein the morphology of the powder product is controlled by changing the shear milling process conditions including at least one of shear milling rotor speed; shear milling time; or amount of precursor powder.

4. A method according to claim 1 , wherein the flowability of the powder is at most 35 seconds/20 cm 3 .

5. A method according to claim 1 , wherein the apparent/tap density of the powder product is improved at least by 100% after high sheer milling.

6. A method according to claim 1 , wherein the precursor particulate material comprises a coarse particulate material.

7. A method according to claim 1 , wherein the precursor particulate material comprises Ti particulates produced from a Ti manufacturing process.

8. A method according to claim 1 , wherein the precursor particulate material is subjected to at least one pre-processing step comprising at least one comminution processes.

9. A method according to claim 1 , wherein in the high shear milling process, the precursor particulate material is immersed in a liquid.

10. A method according claim 9 , wherein the liquid comprises at least one of water, alcohol or kerosene.

11. A method according to claim 1 , wherein the rotor has a rotor diameter, and wherein the precursor particulate material comprise particles having an average particle size of less than the rotor diameter.

12. A method according to claim 1 , wherein the high shear mixer has a circumferential milling speed of at least 700 m/min.

13. A method according to claim 1 , wherein the precursor particulate material comprise porous Ti/Ti alloy particulates and high shear milling is conducted for a duration of at least 15 minutes.

14. A method according to claim 1 , wherein the stator is configured to have less than 5 mm gap between the rotor and an inner surface of the stator.

15. A method according to claim 1 , wherein the precursor particulate material is subjected to milling with at least two high shear mills.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 21, 2017
From: OH, CHULL HEE; GULIZIA, STEFAN
To: COMMONWEALTH SCIENTIFIC AND INDUSTRIAL RESEARCH ORGANISATION
Reel/Frame 044462/0264 →
Priority Claims (1)
AU 2014902291 · Jun 16, 2014 · national
Continuity (1)
Related Publication 20170197250A1 · Jul 13, 2017