IP Library Granted Patent US 10,245,248
Granted Patent B2
US 10,245,248 · App. 15/318,627 · Granted Apr 2, 2019

FAP-activated therapeutic agents, and uses related thereto

Inventors: William W. Bachovchin (Cambridge, MA); Hung-sen Lai (Andover, MA); David G. Sanford (Reading, MA); Sarah E. Poplawski (Belmont, MA); Wengen Wu (Winchester, MA)
Assignee: BACH BIOSCIENCES, LLC
A61K31/337A61K31/4155A61K31/4375A61K31/4545A61K31/517A61K31/519A61K31/69A61K31/704A61K31/7068A61K47/54A61K47/64
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Quick Facts
Patent No.
US 10,245,248
App. No.
15/318,627
Granted
Apr 2, 2019
Kind
B2
Abstract

Disclosed are prodrugs of therapeutic or imaging agents, which prodrugs are selectively cleaved by fibroblast activating protein (FAP) to release the agents. Upon cleavage by FAP of the FAP substrate, the prodrug releases the agent in its active form or in a form that is readily metabolized to its active form. Pharmaceutical compositions comprising the prodrugs, as well as methods of using the prodrugs to treat a disorder characterized by FAP upregulation are also disclosed.

Claims (41)

1. A prodrug represented by the general formula

or a pharmaceutically acceptable salt thereof, wherein:

R 1 represents (C 1 -C 10 )alkyl, (C 1 -C 10 )alkoxy, (C 1 -C 10 )alkyl-C(O)—(C 1 -C 10 )alkyl, (C 3 -C 8 )cycloalkyl, (C 3 -C 8 )cycloalkyl(C 1 -C 10 )alkyl, aryl, aryl(C 1 -C 10 )alkyl, heteroaryl, or heteroaryl(C 1 -C 10 )alkyl, wherein any R 1 is optionally substituted with one or more substituents independently selected from the group consisting of halo, hydroxy, carboxylate, cyano, amino, nitro, and thio (—SH); or —C(═X)R 1 represents an N-terminally blocked alpha amino acid residue and X is O;

R 2 represents H or a (C 1 -C 6 )alkyl;

R 3 represents a (C 1 -C 6 )alkyl;

R 4 is absent or represents one, two or three substituents, each independently selected from a (C 1 -C 6 )alkyl, —OH, —NH 2 , or halogen;

X represents O or S;

Cyt′, or Cyt′L-NH, represents a cytotoxic compound or cytostatic compound, less a hydrogen atom; and

L represents a 4- to 8-membered ring which is part of the cytotoxic compound or cytostatic compound and is recognized by FAP as a P′ 1 residue; or L is a self-immolative linker which is metabolized after FAP cleavage to release Cyt′,

wherein the prodrug is selectively converted to the cytotoxic compound or cytostatic compound by FAP + stromal cells.

2. A prodrug represented by the general formula

or a pharmaceutically acceptable salt thereof, wherein:

R 1 represents a heteroaryl polycyclic moiety;

R 2 represents H or a (C 1 -C 6 )alkyl;

Cyt′ or Cyt′L-NH, represents a cytotoxic compound or cytostatic compound, less a hydrogen atom; and

L represents a 4- to 8-membered ring which is part of the cytotoxic compound or cytostatic compound and is recognized by FAP as a P′ 1 residue; or L is a self-immolative linker which is metabolized after FAP cleavage to release Cyt′,

wherein the prodrug is selectively converted to the cytotoxic compound or cytostatic compound by FAP + stromal cells.

3. A prodrug represented by the general formula

or a pharmaceutically acceptable salt thereof, wherein:

R 1 represents a heteroaryl moiety;

R 2 represents H or a (C 1 -C 6 )alkyl;

Cyt′ or Cyt′-L-NH, represents a cytotoxic compound or cytostatic compound, less a hydrogen atom; and

L represents a 4- to 8-membered ring which is part of the cytotoxic compound or cytostatic compound and is recognized by FAP as a P′ 1 residue; or L is a self-immolative linker which is metabolized after FAP cleavage to release Cyt′,

wherein the prodrug is selectively converted to the cytotoxic compound or cytostatic compound by FAP + stromal cells.

4. The prodrug of claim 1 , wherein Lisa self-immolative linker comprising a heterocycle.

5. The prodrug of claim 4 , wherein the self-immolative linker is selected from the group consisting of His-Ala, p-aminobenzyloxycarbonyl (PABC), and 2,4-bis(hydroxymethyl)aniline.

6. A pharmaceutical composition, comprising a prodrug of claim 1 , or a pharmaceutically acceptable salt thereof; and a pharmaceutically acceptable carrier.

7. A method of treating a disorder characterized by fibroblast activation protein (FAP) upregulation, comprising administering to a subject in need thereof a therapeutically effective amount of a prodrug of claim 1 , or a pharmaceutically acceptable salt thereof.

8. A prodrug represented by the general formula

or a pharmaceutically acceptable salt thereof, wherein:

R 1 represents (C 1 -C 10 )alkyl, (C 1 -C 10 )alkoxy, (C 1 -C 10 )alkyl-C(O)—(C 1 -C 10 )alkyl, (C 3 -C 8 )cycloalkyl, (C 3 -C 8 )cycloalkyl(C 1 -C 10 )alkyl, aryl, aryl(C 1 -C 10 )alkyl, heteroaryl, or heteroaryl(C 1 -C 10 )alkyl, wherein any R 1 is optionally substituted with one or more substituents independently selected from the group consisting of halo, hydroxy, carboxylate, cyano, amino, nitro, and thio (—SH); or —C(═X)R 1 represents an N-terminally blocked alpha amino acid residue and X is O;

R 2 represents H or a (C 1 -C 6 )alkyl;

R 3 represents H or a (C 1 -C 6 )alkyl;

R 4 is absent or represents one, two or three substituents, each independently selected from a (C 1 -C 6 )alkyl, —OH, —NH 2 , or halogen;

X represents O or S;

Cyt′ represents a cytotoxic compound or cytostatic compound, less a hydrogen atom; and

L is a self-immolative linker comprising a heterocycle,

wherein the prodrug is selectively converted to the cytotoxic compound or cytostatic compound by FAP + stromal cells.

9. The prodrug of claim 8 , wherein the self-immolative linker is selected from the group consisting of His-Ala, p-aminobenzyloxycarbonyl (PABC), and 2,4-bis(hydroxymethyl)aniline.

10. A pharmaceutical composition, comprising a prodrug of claim 8 , or a pharmaceutically acceptable salt thereof; and a pharmaceutically acceptable carrier.

11. A method of treating a disorder characterized by fibroblast activation protein (FAP) upregulation, comprising administering to a subject in need thereof a therapeutically effective amount of a prodrug of claim 8 , or a pharmaceutically acceptable salt thereof.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 4, 2018
From: TRUSTEES OF TUFTS COLLEGE
To: BACH BIOSCIENCES, LLC
Reel/Frame 046098/0709 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 10, 2017
From: BACHOVCHIN, WILLIAM W.; LAI, HUNG-SEN; SANFORD, DAVID G.; POPLAWSKI, SARAH E.; WU, WENGEN
To: TRUSTEES OF TUFTS COLLEGE
Reel/Frame 041938/0723 →
Continuity (3)
Provisional Application 62051033 · Sep 16, 2014
Provisional Application 62011989 · Jun 13, 2014
Related Publication 20170119901A1 · May 4, 2017