IP Library Granted Patent US 10,857,490
Granted Patent B2
US 10,857,490 · App. 15/322,348 · Granted Dec 8, 2020

Separation process having improved capacity

Inventors: Thomas Bartos (Arden, NC); Anders Bitsch-Larsen (Wheaton, IL); Timothy Keyes (Arden, NC)
Assignee: BP Corporation North America Inc.
B01D33/09B01D33/60B01D33/663B01D2201/202B01D2201/345
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Quick Facts
Patent No.
US 10,857,490
App. No.
15/322,348
Granted
Dec 8, 2020
Kind
B2
Abstract

A process for the separation of the components of a solid/liquid mixture. The process Includes the use of a rotary pressure filter apparatus having improved capacity.

Claims (38)

1. A method for separating a solid/liquid mixture, comprising:

in a rotary pressure filter apparatus comprising one or more filter members, the rotary pressure filter having a cumulative filter area of all filter members thereof, filtering a solid/liquid mixture to form a filter cake comprising the solid on at least one filter member at a rate sufficient to form at least 3000 kg of filter cake per square meter of cumulative filter area per hour, calculated on a dry-weight basis;

washing the filter cake with a wash fluid in the rotary pressure filter apparatus to form a wet filter cake;

transferring the wet filter cake to a dryer, the wet filter cake comprising at least 10 wt % wash fluid; and

drying the wet filter cake in the dryer.

2. The method of claim 1 , wherein the solid/liquid mixture is filtered at a rate sufficient to form at least 5000 kg of filter cake per square meter of cumulative filter area per hour, calculated on a dry-weight basis.

3. The method of claim 1 , wherein the solid/liquid mixture is filtered at a rate sufficient to form at least 8000 kg of filter cake per square meter of cumulative filter area per hour, calculated on a dry-weight basis.

4. The method of claim 3 , wherein the wet filter cake comprises at least 12 wt % wash fluid.

5. The method of claim 3 , wherein the wet filter cake comprises at least 15 wt % wash fluid.

6. The method of claim 1 , wherein a circumference of the rotary pressure apparatus defines a 360° work path, and the at least one dry zone comprises less than 50° of the work path.

7. The method of claim 1 , wherein a circumference of the rotary pressure apparatus defines a 360° work path, and the at least one dry zone comprises less than 40° of the work path.

8. The method of claim 1 , wherein a circumference of the rotary pressure apparatus defines a 360° work path, and the at least one dry zone comprises less than 30° of the work path.

9. The method of claim 1 , wherein the filter cake comprises an aromatic carboxylic acid.

10. The method of claim 1 , wherein the filter cake comprises terephthalic acid.

11. The method of claim 10 , wherein the filter cake comprises at least 99.4 wt % terephthalic acid on a solvent free basis.

12. The method claim 10 , wherein the filter cake comprises at least 99.8 wt % terephthalic acid on a solvent free basis.

13. The method of claim 10 , wherein the wash fluid comprises water.

14. The method of claim 1 , wherein a circumference of the rotary pressure apparatus defines a 360° work path, and the work path comprises a feed zone, a first wash zone, a second wash zone, a dry zone, and a discharge zone.

15. The method of claim 14 , wherein

the feed zone comprises at least 100° of the work path; and

the dry zone comprises less than 50° of the work path.

16. The method of claim 14 , wherein

the feed zone comprises at least 120° of the work path; and

the dry zone comprises less than 40° of the work path.

17. The method of claim 1 , wherein

the solid/liquid mixture is filtered at a rate sufficient to form at least 5000 kg of filter cake per square meter of cumulative filter area per hour, calculated on a dry-weight basis; and

the wet filter cake comprises at least 12 wt % wash fluid.

18. The method of claim 1 , wherein

the solid/liquid mixture is filtered at a rate sufficient to form at least 8000 kg of filter cake per square meter of cumulative filter area per hour, calculated on a dry-weight basis; and

the wet filter cake comprises at least 15 wt % wash fluid.

19. The method of claim 1 , wherein

the solid/liquid mixture is filtered at a rate sufficient to form at least 5000 kg of filter cake per square meter of cumulative filter area per hour, calculated on a dry-weight basis;

the wet filter cake comprises at least 12 wt % wash fluid; and

a circumference of the rotary pressure apparatus defines a 360° work path, and the at least one dry zone comprises less than 50° of the work path.

20. The method of claim 1 , wherein

the solid/liquid mixture is filtered at a rate sufficient to form at least 8000 kg of filter cake per square meter of cumulative filter area per hour, calculated on a dry-weight basis; and

the wet filter cake comprises at least 15 wt % wash fluid; and

a circumference of the rotary pressure apparatus defines a 360° work path, and the at least one dry zone comprises less than 40° of the work path.

Assignments (4)
FIRST LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Apr 30, 2021
From: INEOS US CHEMICALS COMPANY
To: HSBC CORPORATE TRUSTEE COMPANY (UK) LIMITED
Reel/Frame 056103/0127 →
CHANGE OF NAME Recorded Mar 26, 2021
From: BP AMOCO CHEMICAL COMPANY
To: INEOS US CHEMICALS COMPANY
Reel/Frame 055735/0674 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 26, 2021
From: BP CORPORATION NORTH AMERICA INC.
To: BP AMOCO CHEMICAL COMPANY
Reel/Frame 055745/0824 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 19, 2017
From: BARTOS, THOMAS; BITSCH-LARSEN, ANDERS; KEYES, TIMOTHY
To: BP CORPORATION NORTH AMERICA INC.
Reel/Frame 041018/0136 →
Continuity (2)
Provisional Application 62035652 · Aug 11, 2014
Related Publication 20180207559A1 · Jul 26, 2018
Cited By (1)
US 12,551,825