IP Library Granted Patent US 10,882,770
Granted Patent B2
US 10,882,770 · App. 15/324,320 · Granted Jan 5, 2021

Biogeochemical transformations of flue gas desulfurization waste using sulfur oxidizing bacteria

Inventors: Duane Graves (Maryville, TN); Allison Kreinberg (Columbus, OH); Robby White (Greenville, SC); Brianna Wallace (Greenville, SC); Brian Adair (Charlotte, NC); Linxi Chen (Knoxville, TN); Sarah Marie Herr (Central, SC)
Assignee: Geosyntec Consultants, Inc.
C02F3/345B01D53/48B01D53/84B01D53/96C01F11/46C02F3/02C12N1/20C12N1/24C12P3/00B01D2251/404B01D2251/95B01D2258/0283C02F2101/101Y02A50/20
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Quick Facts
Patent No.
US 10,882,770
App. No.
15/324,320
Granted
Jan 5, 2021
Kind
B2
Abstract

In some embodiments, the invention provides a method for converting of a flue gas desulfurization (FGD) waste product to a gypsum-enriched product by fostering growth of sulfur oxidizing bacteria (SOB) in the FGD waste product. Also provided are isolated sulfur oxidizing bacteria cultures as well as kits comprising an isolated sulfur oxidizing bacteria culture and written instructions for fostering the growth of the isolated sulfur oxidizing bacteria culture in FGD waste product to product a gypsum-enriched product.

Claims (18)

1. A method for converting a flue gas desulfurization (FGD) waste product comprising calcium sulfite, the FGD waste product selected from the group consisting of an FGD waste-containing slurry, FGD waste in solid state, and waste-water containing FGD solids, into a gypsum-enriched product, the method comprising:

fostering growth of sulfur oxidizing bacteria (SOB) in the FGD waste product under conditions whereby the sulfur oxidizing bacteria convert calcium sulfite in the FGD waste product to produce a gypsum-enriched product,

wherein fostering growth of SOB includes supplementing the FGD waste product with chemolithoautotrophic SOB derived from FGD waste product, the FGD waste product comprising calcium sulfite and selected from the group consisting of an FGD waste-containing slurry, FGD waste in solid state, and waste-water containing FGD solids.

2. The method of claim 1 , wherein fostering growth of sulfur oxidizing bacteria includes supplementing the FGD waste product with an SOB growth medium.

3. The method of claim 1 , wherein the chemolithoautotrophic sulfur oxidizing bacteria derived from FGD waste product is an isolated SOB culture or a recycled sulfur oxidizing bacteria biomass from a previously treated batch of FGD waste product.

4. The method of claim 1 , wherein fostering growth of sulfur oxidizing bacteria includes supplementing the FGD waste product with both an SOB growth medium and an isolated SOB culture derived from FGD waste.

5. The method of claim 4 , wherein the FGD waste product is supplemented with at least 1×10 7 cells of the isolated SOB culture.

6. A method according to claim 4 , wherein the isolated sulfur oxidizing bacteria culture is isolated according to a method comprising:

obtaining a culture of chemolithoautotrophic SOB derived from FGD waste;

propagating the culture of SOB in a sulfur-supplemented SOB growth medium for at least fifteen generations.

7. A method according to claim 6 , wherein the culture is propagated in sulfur-supplemented SOB growth medium for at least twenty generations.

8. The method of claim 6 , wherein the culture converts sulfite to sulfate in a sulfur-supplemented SOB growth medium at the rate of at least 0.1% per day.

9. The method of claim 6 , wherein the culture converts sulfite to sulfate in a sulfur-supplemented SOB growth medium at the rate selected from the group consisting of at least 0.25% per day, at least about 0.5% per day, and at least about 0.75% per day.

10. The method of claim 6 , wherein the culture converts sulfite to sulfate in a biostimulated FGD slurry at least 1.5 times faster than endogenous SOB in the FGD slurry.

11. The method of claim 6 , wherein the culture converts sulfite to sulfate in a biostimulated FGD slurry at least two times faster than endogenous SOB in the FGD slurry.

12. The method of claim 1 , wherein the conditions comprise fostering growth at a temperature between about 25° C. to about 35° C.

13. The method of claim 1 , wherein the conditions comprise fostering growth in a presence of ammonium, phosphate, and oxygen.

14. The method of claim 1 , wherein the conditions comprise a pH of between about 5 to about 8.

Assignments (4)
SECURITY INTEREST Recorded Aug 15, 2024
From: GEOSYNTEC CONSULTANTS, INC.
To: BANK OF MONTREAL, AS COLLATERAL AGENT
Reel/Frame 068289/0704 →
RELEASE OF SECURITY INTEREST Recorded Aug 2, 2024
From: BSP AGENCY, LLC, AS COLLATERAL AGENT
To: GEOSYNTEC CONSULTANTS, INC.; APPLIED TECHNOLOGY AND MANAGEMENT, INC.; GRADCO, LLC
Reel/Frame 068164/0552 →
SECURITY INTEREST Recorded May 18, 2022
From: GEOSYNTEC CONSULTANTS, INC.
To: BSP AGENCY, LLC, AS COLLATERAL AGENT
Reel/Frame 059949/0783 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 21, 2017
From: GRAVES, DUANE; KREINBERG, ALLISON; WHITE, ROBBY; WALLACE, BRIANNA; ADAIR, BRIAN; CHEN, LINXI; HERR, SARAH MARIE
To: GEOSYNTEC CONSULTANTS, INC.
Reel/Frame 041320/0498 →
Continuity (2)
Provisional Application 62021505 · Jul 7, 2014
Related Publication 20170203985A1 · Jul 20, 2017
Cited By (1)
US 12,411,123