IP Library Granted Patent US 10,011,585
Granted Patent B2
US 10,011,585 · App. 15/329,635 · Granted Jul 3, 2018

Factor XIa inhibitors

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Quick Facts
Patent No.
US 10,011,585
App. No.
15/329,635
Granted
Jul 3, 2018
Kind
B2
Abstract

The present invention provides a compound of Formula (I) and pharmaceutical compositions comprising one or more said compounds, and methods for using said compounds for treating or preventing thromboses, embolisms, hypercoaguability or fibrotic changes. The compounds are selective Factor XIa inhibitors or dual inhibitors of Factor XIa and plasma kallikrein.

Claims (31)

1. A compound of the formula:

wherein X is NH;

Y is N;

R 1 is aryl or C 3-6 cycloalkyl, wherein said aryl and cycloalkyl groups are optionally substituted with one to three substituents independently selected from the group consisting of halo, nitro, cyano, oxo, R 4 , OR 4 , (C═O)R 4 , (C═O)OR 4 , (C═O)NR 4 R 5 , NR 4 R 5 , NH(C═O)R 4 , NH(C═O)OR 4 , C(NH)NR 4 R 5 , C 3-6 cycloalkyl and tetrazolyl which is optionally substituted with R 4 ;

R 2 is hydrogen or CH(R 2a )(R 2b );

R 2a is hydrogen, C 1-6 alkyl, aryl or C 3-6 cycloalkyl, wherein said alkyl group is optionally substituted with one to three substituents independently selected from the group consisting of halo, hydroxy and cyano, and wherein said aryl, and cycloalkyl groups are optionally substituted with one to three substituents independently selected from the group consisting of halo, nitro, cyano, oxo, R 4 and OR 4 ;

R 2b is hydrogen or C 1-6 alkyl, which is optionally substituted with one to three substituents independently selected from the group consisting of halo, hydroxy and cyano;

R 3 is halo, cyano, (C═O)OR 4 or R 6 ;

R 4 is hydrogen or C 1-6 alkyl, which is optionally substituted with one to three groups independently selected from the group consisting of halo and hydroxy;

R 5 is hydrogen or C 1-6 alkyl, which is optionally substituted with one to three groups independently selected from the group consisting of halo and hydroxy;

R 6 is aryl or C 3-10 cycloalkyl, wherein said aryl and cycloalkyl groups are optionally substituted with one to three substituents independently selected from the group consisting of halo, nitro, cyano, oxo, R 4 , OR 4 , (C═O)R 4 , (C═O)OR 4 , (C═O)NR 4 R 5 , NR 4 R 5 , NH(C═O)R 4 , NH(C═O)OR 4 , SO 2 R 4 , SO 2 NR 4 R 5 , NR 4 SO 2 R 5 and PO 3 R 4 ; or a pharmaceutically acceptable salt thereof.

2. The compound of claim 1 of the formula:

wherein R 1 is aryl or C 3-6 cycloalkyl, wherein said aryl and cycloalkyl groups are optionally substituted with one to three substituents independently selected from the group consisting of halo, nitro, cyano, oxo, R 4 , OR 4 , (C═O)R 4 , (C═O)OR 4 , (C═O)OR 4 , NR 4 R 5 , NH(C═O)R 4 , NH(C═O)OR 4 , C(NH)NR 4 R 5 , C 3-6 cycloalkyl and tetrazolyl which is optionally substituted with R 4 ;

R 2a is hydrogen, C 1-6 alkyl, aryl or C 3-6 cycloalkyl, wherein said alkyl group is optionally substituted with one to three substituents independently selected from the group consisting of halo, hydroxy and cyano, and wherein said aryl and cycloalkyl groups are optionally substituted with one to three substituents independently selected from the group consisting of halo, nitro, cyano, oxo, R 4 and OR 4 ;

R 2b is hydrogen or C 1-6 alkyl, which is optionally substituted with one to three substituents independently selected from the group consisting of halo, hydroxy and cyano;

R 3 is halo, cyano, (C═O)OR 4 or R 6 ;

R 4 is hydrogen or C 1-6 alkyl, which is optionally substituted with one to three groups independently selected from the group consisting of halo and hydroxy;

R 5 is hydrogen or C 1-6 alkyl, which is optionally substituted with one to three groups independently selected from the group consisting of halo and hydroxy;

R 6 is aryl or C 3-10 cycloalkyl, wherein said aryl and cycloalkyl groups are optionally substituted with one to three substituents independently selected from the group consisting of halo, nitro, cyano, oxo, R 4 , OR 4 , (C═O)R 4 , (C═O)OR 4 , (C═O)NR 4 R 5 , NR 4 R 5 , NH(C═O)R 4 , NH(C═O)OR 4 , SO 2 R 4 , SO 2 NR 4 R 5 , NR 4 SO 2 R 5 and PO 3 R 4 ;

or a pharmaceutically acceptable salt thereof.

3. The compound of claim 1 wherein R 1 is aryl, which optionally is substituted with one to three substituents independently selected from the group consisting of halo, cyano, OR 4 , R 4 , C 3-6 cycloalkyl and tetrazolyl which is optionally substituted with R 4 ; or a pharmaceutically acceptable salt thereof.

4. The compound of claim 1 wherein R 1 is phenyl, which optionally is substituted with one to three substituents independently selected from the group consisting of halo, C 3-6 cycloalkyl and tetrazolyl; or a pharmaceutically acceptable salt thereof.

5. The compound of claim 1 wherein R 2a is aryl, which optionally is substituted with one to three halo; or a pharmaceutically acceptable salt thereof.

6. The compound of claim 1 wherein R 2b is hydrogen; or a pharmaceutically acceptable salt thereof.

7. The compound of claim 1 wherein R 2a is cyclopropyl; or a pharmaceutically acceptable salt thereof.

8. The compound of claim 1 wherein R 3 is halo, cyano or (C═O)OR 4 ; or a pharmaceutically acceptable salt thereof.

9. The compound of claim 1 wherein R 3 is halo; or a pharmaceutically acceptable salt thereof.

10. The compound of claim 1 wherein R 3 is (C═O)OR 4 ; or a pharmaceutically acceptable salt thereof.

11. The compound selected from:

or a pharmaceutically acceptable salt thereof.

12. A pharmaceutical composition comprising a compound of claim 1 or a pharmaceutically acceptable salt thereof and a pharmaceutically acceptable carrier.

Assignments (2)
MERGER Recorded Aug 8, 2022
From: MERCK SHARP & DOHME CORP.
To: MERCK SHARP & DOHME LLC
Reel/Frame 061102/0145 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 27, 2017
From: LIU, WEIGUO; EDMONDSON, SCOTT D; GUO, ZHUYAN; HRUZA, ALAN; SO, SUNG-SAU; SUN, WANYING; ALI, AMJAD; KUANG, RONGZE; GAO, YING-DUO; OGAWA, ANTHONY K
To: MERCK SHARP & DOHME CORP.
Reel/Frame 041100/0978 →