IP Library Granted Patent US 9,808,500
Granted Patent B2
US 9,808,500 · App. 15/334,108 · Granted Nov 7, 2017

Antithrombotic nanoparticle

Inventors: Samuel A. Wickline (St. Louis, MO); Jacob Myerson (St. Louis, MO); Rohun Palekar (St. Louis, MO); Hua Pan (St. Louis, MO)
Assignee: WASHINGTON UNIVERSITY
A61K38/10A61K9/51A61K38/06A61K45/06
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Quick Facts
Patent No.
US 9,808,500
App. No.
15/334,108
Granted
Nov 7, 2017
Kind
B2
Abstract

The present invention encompasses an antithrombotic nanoparticle and use thereof.

Claims (18)

1. A method of inhibiting thrombin activation of a protein-activated receptor (PAR) in a subject, the method comprising administering to the subject an antithrombotic nanoparticle comprising a core and an outer layer,

wherein the core of the antithrombotic nanoparticle comprises a perfluorocarbon that is a liquid at about 37° C. and the outer layer comprises a mixture of a lipid and a surfactant;

wherein the exterior of the antithrombotic nanoparticle comprises a direct thrombin inhibitor covalently conjugated to the exterior via the lipid component of the nanoparticle's outer layer, such that the antithrombotic nanoparticle has a second order kinetic constant for the direct thrombin inhibitor-thrombin interaction that is greater than the same kinetic constant of the direct thrombin inhibitor by itself; and

wherein the antithrombotic nanoparticle is antithrombotic but does not substantially alter the clotting time of a subject's blood plasma.

2. The method of claim 1 , wherein the nanoparticle further comprises an anti-platelet agent.

3. The method of claim 1 , wherein the direct thrombin inhibitor is bivalirudin.

4. The method of claim 1 , wherein the direct thrombin inhibitor is D-phenylalyl-L-prolyl-L-arginyl-chloromethyl ketone (PPACK).

5. The method of claim 1 , wherein the PAR is PAR-1, PAR-3, or PAR-4.

6. The method of claim 1 , wherein the PAR is PAR-1.

7. A method of inhibiting thrombin activation of a protein-activated receptor (PAR) in an organ, the method comprising contacting the organ with an antithrombotic nanoparticle comprising a core and an outer layer,

wherein the core of the antithrombotic nanoparticle comprises a perfluorocarbon that is a liquid at about 37° C. and the outer layer comprises a mixture of a lipid and a surfactant;

wherein the exterior of the antithrombotic nanoparticle comprises a direct thrombin inhibitor covalently conjugated to the exterior via the lipid component of the nanoparticle's outer layer, such that the antithrombotic nanoparticle has a second order kinetic constant for the direct thrombin inhibitor-thrombin interaction that is greater than the same kinetic constant of the direct thrombin inhibitor by itself; and

wherein the antithrombotic nanoparticle is antithrombotic but does not substantially alter the clotting time of a subject's blood plasma.

8. The method of claim 7 , wherein the nanoparticle further comprises an anti-platelet agent.

9. The method of claim 7 , wherein the direct thrombin inhibitor is bivalirudin.

10. The method of claim 7 , wherein the direct thrombin inhibitor is D-phenylalyl-L-prolyl-L-arginyl-chloromethyl ketone (PPACK).

11. The method of claim 7 , wherein the PAR is PAR-1, PAR-3, or PAR-4.

12. The method of claim 7 , wherein the PAR is PAR-1.

Assignments (2)
CONFIRMATORY LICENSE Recorded Jan 22, 2019
From: WASHINGTON UNIVERSITY
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 048107/0196 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 7, 2017
From: WICKLINE, SAMUEL A.; MYERSON, JACOB W.; PAN, HUA; PALEKAR, ROHUN
To: WASHINGTON UNIVERSITY
Reel/Frame 041483/0565 →
Continuity (4)
Continuation In Part 13516528
Provisional Application 62249126 · Oct 30, 2015
Provisional Application 61287582 · Dec 17, 2009
Related Publication 20170065669A1 · Mar 9, 2017