IP Library Granted Patent US 10,494,543
Granted Patent B2
US 10,494,543 · App. 15/347,917 · Granted Dec 3, 2019

Shatter-proof glass coating composition, tempered shatter-proof glass using it and method for manufacturing tempered shatter-proof glass

Inventors: Nak Kyoung Kong (Gyeonggi-do, KR); Ki Hong Lee (Seoul, KR); Jong Min Park (Incheon, KR); Tae Soo Jung (Gyeonggi-Do, KR); Bock Ceol Lee (Gyeonggi-Do, KR); Keon Soo Jin (Ulsan, KR); Jae Beom Ahn (Gyeonggi-Do, KR); Young Seok Kim (Chungcheongnam-Do, KR); Yong Chul Lee (Chungcheongnam-Do, KR)
Assignees: Hyundai Motor Company; Noroo Bee Chemical Co., Ltd.
C09D175/04C03C17/30C03C17/322C03C17/324C03C17/3405C08G18/6233C09D133/14C03C2217/78Y10T428/24777Y10T428/24793Y10T428/24802
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Quick Facts
Patent No.
US 10,494,543
App. No.
15/347,917
Granted
Dec 3, 2019
Kind
B2
Abstract

Disclosed are a coating composition applied on a tempered glass, the tempered glass preventing shattering when impacts are applied, and a manufacturing method thereof. The coating composition comprises a caprolactone-modified acryl resin, an acryl polyol, a polyurethane resin and the like, such that the tempered glass has improved strength and the ceramic part can be removed from a conventional tempered glass. Further provided is a vehicle product such as a vehicle glass component, such that passengers in the vehicle can be protected from the shattering of the broken tempered glass.

Claims (50)

1. A coating composition comprising:

(a) an amount of about 50 to 60% by weight of a caprolactone-modified acryl resin component;

(b) an amount of about 10 to 20% by weight of an acryl polyol component;

(c) an amount of about 10 to 20% by weight of a polyurethane resin component;

(d) an amount of about 0.1 to 1.5% by weight of a reaction catalyst;

(e) an amount of about 0.1 to 1.5% by weight of a wet additive;

(f) an amount of about 1.0 to 1.5% by weight of a pigment; and

(g) an amount of about 5 to 20% by weight of a solvent,

all the % by weights based on the total weights of the components (a)-(g),

wherein the coating composition further comprises a hexamethylenediisocyanate trimer resin as a hardener.

2. The coating composition of claim 1 , wherein (a) the caprolactone-modified acryl acrly resin is present in a solid content of about 70 wt % based on the total weight of the caprolactone-modified acryl resin component, and a weight-average molecular weight of the caprolactone-modified acryl resin is of about 8,000 to 20,000, and a hydroxyl group content is of about 1 to 4%.

3. The coating composition of claim 1 , wherein (b) the acryl polyol is present in a solid content of about 55 wt % based on the total weight of the acryl polyol component, a weight-average molecular weight of the acryl polyol is of about 12,000 to 25,000, a hydroxyl group content is of about 0.2 to 2%, and a glass transition temperature of the acryl polyol is of about 70 to 80° C.

4. The coating composition of claim 1 , wherein (c) the polyurethane resin has a hydroxyl group content of about 0.5 to 1.0 wt % based on the total weight of the polyurethane resin, and a weight-average molecular weight of the polyurethane resin is of about 40,000 to 43,000, and the polyurethane resin is present in a solid content of about 70 to 80% based on the total weight of the polyurethane resin component.

5. The coating composition of claim 1 , wherein (d) the reaction catalyst is dibutyltindilaurate.

6. The coating composition of claim 1 , wherein a mixing weight ratio between the total weights of (a) the caprolactone-modified acryl resin component; (b) the acryl polyol component; (c) the polyurethane resin component; (d) the reaction catalyst; (e) the wet additive; (f) the pigment; and (g) the solvent to the hardener is of about 2 to 4:1.

7. The coating composition of claim 1 , wherein a ford cup (FORD CUP#4, 25° C.) viscosity of the coating composition is of about 18 to 20 seconds.

8. The coating composition of claim 1 , wherein the coating composition is transparent.

9. The coating composition of claim 1 , wherein the coating composition is opaque.

10. The coating composition of claim 1 , consisting essentially of:

(a) an amount of about 50 to 60% by weight of a caprolactone-modified acryl resin component;

(b) an amount of about 10 to 20% by weight of an acryl polyol component;

(c) an amount of about 10 to 20% by weight of a polyurethane resin component;

(d) an amount of about 0.1 to 1.5% by weight of a reaction catalyst;

(e) an amount of about 0.1 to 1.5% by weight of a wet additive;

(f) an amount of about 1.0 to 1.5% by weight of a pigment; and

(g) an amount of about 5 to 20% by weight of a solvent,

all the % by weights based on the total weights of the components (a)-(g) and the hexamethylenediisocyanate trimer resin as a hardener.

11. The coating composition of claim 1 , consisting of:

(a) an amount of about 50 to 60% by weight of a caprolactone-modified acryl resin component;

(b) an amount of about 10 to 20% by weight of an acryl polyol component;

(c) an amount of about 10 to 20% by weight of a polyurethane resin component;

(d) an amount of about 0.1 to 1.5% by weight of a reaction catalyst;

(e) an amount of about 0.1 to 1.5% by weight of a wet additive;

(f) an amount of about 1.0 to 1.5% by weight of a pigment; and

(g) an amount of about 5 to 20% by weight of a solvent,

all the % by weights based on the total weights of the components (a)-(g) and the hexamethylenediisocyanate trimer resin as a hardener.

12. A coated tempered glass comprising:

a tempered glass;

a primer layer formed on a surface of the tempered glass; and

a coating layer formed from the coating composition of claim 1 , wherein the coating layer is on the primer layer.

13. The tempered glass of claim 12 , wherein the primer layer is formed by coating with a silane primer.

14. The tempered glass of claim 12 , wherein a pre-primer layer is formed between the tempered glass and the primer layer, and the pre-primer layer is a transparent layer formed with a silane primer.

15. The tempered glass of claim 12 , wherein the primer layer is formed at a width of about 5 to 15 cm at an outer edge of the tempered glass.

16. The tempered glass of claim 12 , wherein the coating layer has an average thickness of about 50 to 80 μm, and the coating layer is coated on a portion where the primer layer is formed or is coated on a front surface of the tempered glass which includes the primer layer.

17. A method of manufacturing a coated tempered glass, comprising:

coating a primer on a surface of a tempered glass to form a primer layer;

coating a coating composition of claim 1 on the primer layer; and

hardening the coating composition at a temperature of about 70 to 90° C for about 20 to 40 minutes.

18. A vehicle panorama roof comprising a coated tempered glass of claim 12 .

19. A vehicle comprising a coating layer formed from the coating composition of claim 1 .

Assignments (2)
MERGER AND CHANGE OF NAME Recorded Nov 27, 2023
From: NOROO BEE CHEMICAL CO., LTD.; NOROO AUTOMOTIVE COATINGS CO., LTD.
To: NOROO AUTOMOTIVE COATINGS CO., LTD.
Reel/Frame 065677/0522 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 10, 2016
From: KONG, NAK KYOUNG; LEE, KI HONG; PARK, JONG MIN; JUNG, TAE SOO; LEE, BOCK CEOL; JIN, KEON SOO; AHN, JAE BEOM; KIM, YOUNG SEOK; LEE, YONG CHUL
To: HYUNDAI MOTOR COMPANY; NOROO BEE CHEMICAL CO., LTD.
Reel/Frame 040275/0182 →
Priority Claims (1)
KR 10-2015-0178616 · Dec 14, 2015 · national
Continuity (1)
Related Publication 20170166774A1 · Jun 15, 2017