IP Library Granted Patent US 10,125,131
Granted Patent B2
US 10,125,131 · App. 15/389,838 · Granted Nov 13, 2018

Selective HDAC3 inhibitors

Inventors: John H. van Duzer (Georgetown, MA); Ralph Mazitschek (Belmont, MA)
Assignee: REGENACY PHARMACEUTICALS, LLC
C07D471/04A61K31/415A61K31/495A61K31/497A61K31/5377C07D209/34C07D215/38C07D215/54C07D217/26C07D231/56C07D235/06C07D235/08C07D241/44
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Quick Facts
Patent No.
US 10,125,131
App. No.
15/389,838
Granted
Nov 13, 2018
Kind
B2
Abstract

Provided herein are HDAC3 inhibitors, as well as methods of treatment comprising administering these compounds to a subject in need thereof.

Claims (49)

1. A compound of Formula I:

or a pharmaceutically acceptable salt thereof,

wherein

A is bicyclic heteroaryl or bicyclic heterocycloalkyl;

R 1 and R 2 are each independently selected from H or halo;

R 3 is H, heterocycloalkyl, or C 1-6 -alkyl-heterocycloalkyl, wherein the heterocycloalkyl or C 1-6 -alkyl-heterocycloalkyl groups are optionally substituted;

R 4 and R 5 are each independently selected from H, C 1-6 -alkyl, C 2-6 -alkenyl, C 2-6 -alkynyl, C 3-6 -cycloalkyl, C 1-6 -alkyl-C 3-6 -cyclo alkyl, heterocycloalkyl, C 1-6 -alkyl-heterocycloalkyl, NR 6 R 7 , O—C 1-6 -alkyl-OR 8 , C 1-6 -alkyl-OR 8 , aryl, C 1-6 -alkyl-aryl, heteroaryl, C 1-6 -alkyl-heteroaryl, C(O)N(R 6 )-heteroaryl, C(O)N(R 6 )-heterocycloalkyl, C(O)N(R 6 )-aryl, C(O)—NR 6 R 7 , C(O)-heteroaryl, C(O)-heterocycloalkyl, C(O)-aryl, C(O)—C 1-6 -alkyl, CO 2 -heteroaryl, CO 2 -heterocycloalkyl, CO 2 -aryl, CO 2 —C 1-6 -alkyl, or C(O)—C 1-6 -alkyl-heterocycloalkyl, wherein the cycloalkyl, heterocycloalkyl, aryl, or heteroaryl groups are optionally substituted;

R 6 and R 7 are each independently selected from H, C 1-6 -alkyl, C 1-6 -alkyl-OR 8 , CO 2 R 8 , or C 1 -C 6 -alkyl-aryl; and

R 8 is H or C 1-6 -alkyl.

2. The compound of claim 1 ,

wherein

the heterocycloalkyl or C 1-6 -alkyl-heterocycloalkyl groups of R 3 are optionally substituted with C 1-4 -alkyl; and

the cycloalkyl, heterocycloalkyl, aryl, or heteroaryl groups of R 4 and R 5 are optionally substituted with C 1-4 -alkyl, CO 2 R 8 , C(O)R 8 , or C 1-6 -alkyl-OR 8 .

3. The compound of claim 1 ,

wherein

A is a bicyclic heteroaryl or bicyclic heterocycloalkyl selected from the group consisting of

4. The compound of claim 1 ,

wherein

A is a bicyclic heteroaryl or bicyclic heterocycloalkyl selected from the group consisting of

5. The compound of claim 1 , wherein R 1 is halo.

6. The compound of claim 1 , wherein R 1 is fluoro.

7. The compound of claim 1 , wherein R 2 is halo.

8. The compound of claim 1 , wherein R 2 is chloro.

9. The compound of claim 1 , wherein R 3 is heterocycloalkyl, or C 1-6 -alkyl-heterocycloalkyl wherein the heterocycloalkyl or C 1-6 -alkyl-heterocycloalkyl groups are optionally substituted with C 1-4 -alkyl.

10. The compound of claim 1 , wherein R 3 is piperazinyl or piperazinyl-CH 3 .

11. The compound of claim 1 , wherein R 3 is CH 2 CH 2 -morpholinyl.

12. The compound of claim 1 ,

wherein

R 4 is independently selected from H, C 3-6 -cycloalkyl, C 1-6 -alkyl-C 3-6 -cycloalkyl, heterocycloalkyl, or C 1-6 -alkyl-heterocycloalkyl.

13. The compound of claim 1 , wherein R 4 is H or C 3-6 -cycloalkyl.

14. The compound of claim 1 , wherein R 4 is H.

15. The compound of claim 1 , wherein R 4 is cyclopropyl.

16. The compound of claim 1 , wherein R 5 is H.

17. The compound of claim 1 , of Formula III:

or a pharmaceutically acceptable salt thereof,

wherein

A is bicyclic heteroaryl or bicyclic heterocycloalkyl;

R 1 and R 2 are halo;

R 3 is H, heterocycloalkyl, or C 1-6 -alkyl-heterocycloalkyl;

R 4 and R 5 are each independently selected from H, C 1-6 -alkyl, C 2-6 -alkenyl, C 2-6 -alkynyl, C 3-6 -cycloalkyl, C 1-6 -alkyl-C 3-6 -cyclo alkyl, heterocycloalkyl, C 1-6 -alkyl-heterocycloalkyl, NR 6 R 7 , O—C 1-6 -alkyl-OR 8 , C 1-6 -alkyl-OR 8 , aryl, C 1-6 -alkyl-aryl, heteroaryl, C 1-6 -alkyl-heteroaryl, C(O)N(R 6 )-heteroaryl, C(O)N(R 6 )-heterocycloalkyl, C(O)N(R 6 )-aryl, C(O)—NR 6 R 7 , C(O)-heteroaryl, C(O)-heterocycloalkyl, C(O)-aryl, C(O)—C 1-6 -alkyl, CO 2 -heteroaryl, CO 2 -heterocycloalkyl, CO 2 -aryl, CO 2 —C 1-6 -alkyl, or C(O)—C 1-6 -alkyl-heterocycloalkyl, wherein the cycloalkyl, heterocycloalkyl, aryl, or heteroaryl groups are optionally substituted;

R 6 and R 7 are each independently selected from H, C 1-6 -alkyl, C 1-6 -alkyl-OR 8 , CO 2 R 8 , or C 1 -C 6 -alkyl-aryl; and

R 8 is H or C 1-6 -alkyl.

18. The compound of claim 17 , wherein R 1 is chloro and R 2 is fluoro.

19. The compound of claim 17 , wherein R 3 is H, R 4 is H, and R 5 is H.

20. The compound of claim 1 , selected from the following:

or pharmaceutically acceptable salts thereof.

21. A pharmaceutical composition comprising a compound of claim 1 , or a pharmaceutically acceptable salt thereof, together with a pharmaceutically acceptable carrier.

22. A method of inhibiting the activity of HDAC3 in a subject in need thereof, comprising administering to the subject a compound of claim 1 or a pharmaceutically acceptable salt thereof.

23. A method of treating a disease mediated by HDAC3 in a subject in need thereof comprising administering to the subject the pharmaceutical composition of claim 21 .

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 23, 2018
From: ACETYLON PHARMACEUTICALS, INC.
To: REGENACY PHARMACEUTICALS, LLC
Reel/Frame 045023/0677 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 27, 2016
From: VAN DUZER, JOHN H.; MAZITSCHEK, RALPH
To: ACETYLON PHARMACEUTICALS, INC.
Reel/Frame 040774/0991 →
Continuity (5)
Continuation 14753913 · Jun 29, 2015
Continuation 14169732 · Jan 31, 2014
Provisional Application 61923023 · Jan 2, 2014
Provisional Application 61759732 · Feb 1, 2013
Related Publication 20170204094A1 · Jul 20, 2017