IP Library Granted Patent US 10,899,107
Granted Patent B2
US 10,899,107 · App. 15/454,233 · Granted Jan 26, 2021

Building membrane with porous pressure sensitive adhesive

Inventor: Daniel Bess (Geneva, OH)
B32B5/26B32B5/00B32B5/022B32B7/04B32B7/12B32B27/00B32B27/06B32B27/18B32B27/32B32B27/36B32B37/12C09J7/21C09J7/255C09J7/38C09J133/08E04B1/625E04D5/10E04D12/002B32B37/1284B32B2037/1253B32B2037/243B32B2255/00B32B2255/02B32B2255/10B32B2255/26B32B2262/00B32B2262/0253B32B2305/026B32B2307/3065B32B2307/724B32B2309/02B32B2419/00B32B2419/06C09J2423/10C09J2433/00C09J2467/006Y10T156/10Y10T428/1452Y10T428/249979Y10T442/651
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,899,107
App. No.
15/454,233
Granted
Jan 26, 2021
Kind
B2
Abstract

A breathable multilayer spun bonded polypropylene membrane having a coated pressure sensitive adhesive capable of allowing air and moisture vapor to pass through it. The adhesive is formed of a copolymer comprising a backbone of n-butyl acrylate, 2-ethylhexyl acrylate, and vinyl acetate which is mixed with a surfactant and emulsified to produce bubbles which form pores when the copolymer is set with about 80% to about 90% of the pore sizes ranging from about 200 microns to about 300 microns and a pore density in the cured pressure sensitive adhesive ranging from about 4200 per inch 2 to about 4600 per inch 2 , said pores being uniformly distributed to form a flow path through adhesive.

Claims (41)

1. A process for making a water resistant, air permeable and vapor permeable membrane with a permeable pressure sensitive adhesive (PSA) backing comprising the steps of:

a) adding water in an amount ranging from about 40% to about 50% by weight to an acrylic copolymer pressure sensitive adhesive ranging from about 45% to about 50% by weight and mixing same to reduce the viscosity of the solution;

b) adding at least one solvent-free surfactant to the water copolymer solution and mixing same for a suitable time period to form air bubbles entrained throughout the copolymer pressure sensitive adhesive and surfactant solution;

c) pouring the bubble containing solution of adhesive and surfactant into a coater;

d) coating the bubble containing solution of adhesive and surfactant onto a water resistant vapor permeable polyester membrane to cover a surface of said membrane with a coating having thickness ranging from about 3 mils to about 5 mils;

e) heating the coated membrane at a suitable temperature for a suitable time to cure the pressure sensitive adhesive solution with the entrained bubbles to form interconnected pores in the now permeable coating; and

f) mounting a removable release cover to the coating over the cured pressure sensitive adhesive.

2. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 1 wherein said coating is heated at a temperature ranging from about 165° to about 265° F.

3. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 1 in step b) wherein said mixing is accomplished by a high speed dispersion mixer rotated at about 5000 rpm.

4. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 1 step b) wherein about 80% to about 90% of said formed air bubbles are sized from about 200 to about 300 microns.

5. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 1 wherein after step b) a fire retardant material is added to the copolymer surfactant mixture in the amount of about 2% to about 3% by weight.

6. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 1 wherein the coating of step d) is applied with a blade coater.

7. A process for making a water resistant, air permeable and vapor permeable membrane with a porous pressure sensitive adhesive (PSA) copolymer backing comprising the steps of:

a) adding water in an amount ranging from about 40% to about 50% by weight to a pressure sensitive adhesive copolymer having a backbone of n-butyl acrylate, 2-ethylhexyl acrylate, and vinyl acetate and mixing the water and pressure sensitive adhesive copolymer to form a solution;

b) adding a surfactant to said solution to provide for emulsification;

c) adding a second surfactant to said solution to provide a foaming agent;

d) adding a thickener to said solution of step c) and mixing the solution in a sheer mixer at a rate of speed for a suitable time to form and entrain air bubbles in said solution having a designated size range throughout the solution;

e) transferring the bubble containing solution into a coater feeder;

f) coating the adhesive surfactant thickener solution onto a water resistant vapor permeable spun polypropylene membrane to cover the surface of said membrane with said coating having a thickness ranging from about 3 mils to about 5 mils;

g) heating the coated membrane at a suitable temperature to accomplish curing of the adhesive surfactant thickener composite solution for a suitable time to cure said entrained air bubbles in place forming interconnected pores in the cured pressure sensitive adhesive; and

h) securing a removable release cover to the coated membrane pressure sensitive adhesive.

8. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 7 wherein a fire retardant material is added to the water copolymer surfactant solution after step c).

9. A process for making a water resistant air permeable and vapor permeable membrane with a porous pressure sensitive adhesive (PSA) backing comprising the steps of:

a) adding water in an amount ranging from about 40% to about 50% by weight to a pressure sensitive adhesive to form a water adhesive mixture, said pressure sensitive adhesive having a copolymer backbone of n-butyl acrylate, 2-ethylhexyl acrylate, and vinyl acetate and mixing said water adhesive mixture to form a uniform solution;

b) adding at least one surfactant to the uniform water copolymer solution and mixing same to form a pressure sensitive adhesive solution;

c) mixing said pressure sensitive adhesive solution for a suitable time in a sheer mixer forming air bubbles throughout the water, copolymer pressure sensitive adhesive and surfactant solution;

d) pouring the air bubble containing solution of water, copolymer pressure sensitive adhesive and surfactant into a coater assembly;

e) coating the bubble containing solution onto a water resistant vapor permeable polyester membrane to cover an outer surface of said membrane with a coating having a thickness which will entrain air bubbles ranging from about 200 microns to about 300 microns in size;

f) heating the coated membrane at a suitable temperature for a suitable time to cure the air bubbles in place in the bubble containing solution to form a cured pressure sensitive coating with interconnected pores positioned throughout the coating with some of said interconnected pores penetrating the surface of the coating to create a vapor permeable coating; and

g) mounting a removable release cover to the coated, membrane pressure sensitive adhesive.

10. A process for making a water resistant air permeable and vapor permeable membrane with a porous pressure sensitive adhesive copolymer coating as claimed in claim 9 wherein in step c) 80% to about 90% of said formed air bubbles are sized from about 200 to about 300 microns.

11. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 9 wherein said coated membrane is cured in step f) at a temperature ranging from about 165° F. to about 265° F.

12. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 9 wherein said at least one surfactant are two surfactants, one surfactant to provide emulsion and air bubble size and a second surfactant being a foaming agent.

13. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 9 wherein in step c) said surfactant, water and copolymer pressure sensitive adhesive mixture solution is mixed in a sheer mixer to entrain air bubbles uniformly in said solution.

14. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 9 wherein said at least one surfactant includes a long chain alcohol which creates a stable emulsion.

15. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 9 wherein said coated membrane is cured in step f) at a temperature ranging from about 165° F. to about 265° F.

16. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 9 step c) wherein about 80% to about 90% of said formed air bubbles range in size from about 200 microns to about 300 microns.

17. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 9 wherein said formed pores are generally round and oval in shape and are evenly distributed throughout the adhesive coating and across the coating surface to form a vapor pathway through the adhesive coating.

18. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 9 wherein said mixing in step c) is undertaken by a high speed dispersion mixer mixed at about 5000 RPM for about 10 minutes to about 15 minutes to provide emulsification forming the bubbles throughout the adhesive solution.

19. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 9 wherein said coater assembly is a blade coater.

20. A process for making a water resistant air permeable and vapor permeable membrane as claimed in claim 7 wherein said first surfactant is a solvent-free wetting agent to provide emulsification and bubble size ranging from about 4% by weight to about 6% by weight and said second surfactant is a foaming agent ranging from about 1.5% by weight to about 2.0% by weight.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 12, 2025
From: VAPROSHIELD, LLC
To: VS ACQUISITION, INC.
Reel/Frame 073921/0723 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2017
From: BESS, DANIEL; PIECINSKI, ROBERT
To: VAPROSHIELD, LLC
Reel/Frame 041528/0152 →
Continuity (3)
Division 14121027 · Jul 22, 2014
Provisional Application 61958161 · Jul 22, 2013
Related Publication 20170174952A1 · Jun 22, 2017