IP Library Granted Patent US 9,988,312
Granted Patent B2
US 9,988,312 · App. 15/460,570 · Granted Jun 5, 2018

Cation-enhanced chemical stability of ion-conducting zirconium-based ceramics

Inventors: Erik David Spoerke (Albuquerque, NM); Paul G. Clem (Albuquerque, NM); Jill S. Wheeler (Albuquerque, NM); Leo J. Small (Albuquerque, NM); Jon Ihlefeld (Charlottesville, VA)
Assignee: National Technology & Engineering Solutions of Sandia, LLC
C04B35/481C01G25/006C01G27/006C04B35/16C04B35/447C04B35/48C04B41/00C01P2002/50C01P2004/80C04B2235/3201C04B2235/3203C04B2235/3227C04B2235/3244C04B2235/447
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Quick Facts
Patent No.
US 9,988,312
App. No.
15/460,570
Granted
Jun 5, 2018
Kind
B2
Abstract

At least partial substitution of zirconium by hafnium in ion-conducting zirconium-based ceramics provides enhanced chemical stability in alkaline and acid environments.

Claims (10)

1. An ion conducting ceramic comprising Na 1+x HF 2 P 3-x Si x O 12 .

2. The ion-conducting ceramic of claim 1 , wherein x=0.

3. A protective layer comprising an ion-conducting zirconium-based ceramic, wherein the zirconium is at least partially substituted by hafnium, that is coated onto another ion-conducting material comprising Na 3 Zr 2 PSi 2 O 12 that is susceptible to a different mechanism of degradation than the protective layer.

4. A protective layer comprising an ion-conducting zirconium-based ceramic, wherein the zirconium is at least partially substituted by hafnium, that is coated onto another ion-conducting material comprising Na 3 Zr 2 P 3 O 12 that is susceptible to a different mechanism of degradation than the protective layer.

5. A protective layer comprising an ion-conducting zirconium-based ceramic, wherein the zirconium is at least partially substituted by hafnium, that is coated onto another ion-conducting material comprising Na 1+x Zr 2 P 3-x Si x O 12 , wherein Zr is at least partially substituted by Hf, that is susceptible to a different mechanism of degradation than the protective layer.

6. The protective layer of claim 5 , wherein x=0.

7. A protective layer comprising Na 1+x Hf 2 P 3-x Si x O 12 that is coated onto another ion-conducting material that is susceptible to a different mechanism of degradation than the protective layer.

8. The protective layer of claim 7 , wherein x=0.

9. The protective layer of claim 7 , wherein the other ion-conducting material comprises Na 3 Zr 2 PSi 2 O 12 .

10. The protective layer of claim 7 , wherein the other ion-conducting material comprises Na 3 Zr 2 P 3 O 12 .

Assignments (3)
CHANGE OF NAME Recorded Mar 29, 2018
From: SANDIA CORPORATION
To: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
Reel/Frame 045767/0630 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2017
From: SPOERKE, ERIK DAVID; CLEM, PAUL G.; WHEELER, JILL S.; SMALL, LEO J.; IHLEFELD, JON
To: SANDIA CORPORATION
Reel/Frame 042002/0059 →
CONFIRMATORY LICENSE Recorded Apr 4, 2017
From: SANDIA CORPORATION
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 041837/0602 →
Continuity (2)
Provisional Application 62311523 · Mar 22, 2016
Related Publication 20170275208A1 · Sep 28, 2017