IP Library Granted Patent US 10,186,710
Granted Patent B2
US 10,186,710 · App. 15/461,709 · Granted Jan 22, 2019

Methods of fabricating solid oxide fuel cells

Inventors: Ke-Ji Pan (Ellicott City, MD); Mohammed Hussain Abdul Jabbar (College Park, MD); Dong Ding (Idaho Falls, ID); Eric Wachsman (Fulton, MD)
Assignees: REDOX POWER SYSTEMS, LLC; UNIVERSITY OF MARYLAND, COLLEGE PARK
H01M4/8663H01M4/9033H01M4/9066H01M8/126H01M8/1213H01M8/1246H01M8/1253B05D3/0254B05D7/50H01M2008/1293H01M2250/30Y02E60/525Y02P70/56
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Quick Facts
Patent No.
US 10,186,710
App. No.
15/461,709
Granted
Jan 22, 2019
Kind
B2
Abstract

In various embodiments, a solid oxide fuel cell is fabricated in part by disposing a functional layer between the cathode and the solid electrolyte.

Claims (26)

1. A method of fabricating and utilizing a solid oxide fuel cell, the method comprising:

providing an anode layer;

disposing a solid electrolyte layer over the anode layer;

depositing a functional layer over the solid electrolyte layer, wherein a thickness of the functional layer is selected from the range of 0.1 μm to 20 μm;

disposing a cathode layer over the functional layer, thereby forming the solid oxide fuel cell; and

operating the solid oxide fuel cell to generate electricity by:

ionizing oxygen at the cathode layer, thereby producing oxygen ions, conducting the oxygen ions from the cathode layer to the anode layer, and reacting the oxygen ions with a hydrogen-containing fuel at the anode layer at an operating temperature;

selecting as the operating temperature a temperature less than 550° C. and greater than 400° C. when the thickness of the functional layer is 0.1 um to 5 μm; and

selecting as the operating temperature a temperature greater than 550° C. and less than 800° C. when the thickness of the functional layer is to 20 um 5 μm.

2. The method of claim 1 , wherein the solid electrolyte layer is disposed over the anode layer before the functional layer is deposited.

3. The method of claim 1 , wherein the anode layer is provided by tape casting.

4. The method of claim 1 , wherein disposing the solid electrolyte layer over the anode layer comprises laminating the solid electrolyte layer to the anode layer.

5. The method of claim 1 , further comprising providing the solid electrolyte layer before disposing the solid electrolyte layer over the anode layer.

6. The method of claim 5 , wherein providing the solid electrolyte layer comprises tape casting.

7. The method of claim 1 , further comprising annealing at least a portion of the solid oxide fuel cell before the cathode layer is disposed over the functional layer.

8. The method of claim 7 , wherein the at least a portion of the solid oxide fuel cell is annealed at a temperature ranging from approximately 800° C. to approximately 1100° C. for a time period ranging from approximately 0.5 hour to approximately 5 hours before the solid electrolyte layer is disposed over the anode layer.

9. The method of claim 1 , wherein the functional layer comprises at least one of cobalt-doped gadolinium-doped ceria or cobalt-doped samarium-doped ceria.

10. The method of claim 1 , wherein the functional layer contains cobalt at a composition ranging from approximately 0.5 mol % to 5 mol %.

11. The method of claim 1 , wherein (i) the functional layer contains cobalt and (ii) at least a portion of the solid electrolyte layer contains cobalt.

12. The method of claim 11 , wherein a concentration of cobalt in the at least a portion of the solid electrolyte layer is less than a concentration of cobalt in the functional layer.

13. The method of claim 1 , further comprising annealing the functional layer and the cathode layer together after the cathode layer is disposed over the functional layer.

14. The method of claim 13 , wherein the annealing is performed at a temperature ranging from approximately 800° C. to approximately 1100° C. for a time period ranging from approximately 0.5 hour to approximately 5 hours.

15. The method of claim 11 , wherein a first portion of the solid electrolyte layer contains cobalt and a second portion of the solid electrolyte layer does not contain cobalt.

16. The method of claim 1 , wherein the hydrogen-containing fuel comprises at least one of hydrogen or a hydrocarbon.

17. The method of claim 1 , wherein the thickness of the functional layer is selected from the range of 0.1 μm to 1 μm.

18. The method of claim 1 , wherein the thickness of the functional layer is selected from the range of 6 μm to 20 μm.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 6, 2019
From: WACHSMAN, ERIC D
To: UNIVERSITY OF MARYLAND, COLLEGE PARK
Reel/Frame 048519/0641 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 20, 2018
From: ABDUL JABBAR, MOHAMMED HUSSAIN; PAN, KE-JI
To: UNIVERSITY OF MARYLAND, COLLEGE PARK
Reel/Frame 047550/0412 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 26, 2018
From: DING, DONG
To: REDOX POWER SYSTEMS, LLC
Reel/Frame 047325/0531 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 26, 2018
From: PAN, KE-JI; JABBAR, MOHAMMED HUSSAIN ABDUL; WACHSMAN, ERIC
To: UNIVERSITY OF MARYLAND, COLLEGE PARK
Reel/Frame 047325/0551 →
SECURITY INTEREST Recorded Oct 16, 2018
From: REDOX POWER SYSTEMS, LLC
To: CLAY, RICH
Reel/Frame 047186/0029 →
Continuity (2)
Provisional Application 62310358 · Mar 18, 2016
Related Publication 20170271700A1 · Sep 21, 2017