IP Library › Granted Patent US 10,072,319
Granted Patent B2
US 10,072,319 · App. 15/484,595 · Granted Sep 11, 2018

Multi-phase covetic and methods of synthesis thereof

Inventors: Michael Dennis Braydich (Beavercreek, OH); Harry Couch (Beavercreek, OH); Louis A. Luedtke (Centerville, OH)
Assignee: GDC Industries, LLC
C22C1/026C22C21/00
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Quick Facts
Patent No.
US 10,072,319
App. No.
15/484,595
Granted
Sep 11, 2018
Kind
B2
Abstract

There are provided methods and systems for creating multi-phase covetics. For example, there is provided a process for making a composite material. The process includes forming a multi-phase covetic. The forming includes heating a melt including a metal in a molten state and a carbon source to a first temperature threshold to form metal-carbon bonds. The forming further includes subsequently heating the melt to a second temperature threshold, the second temperature threshold being greater than the first temperature threshold. The second temperature threshold is a temperature at or above which ordered multi-phase covetics form in the melt.

Claims (33)

1. A process for making a composite material, the process comprising:

forming a multi-phase covetic, the forming including:

heating a melt including a metal in a molten state and a carbon source to a first temperature threshold to form metal-carbon bonds; and

subsequently heating the melt to a second temperature threshold, the second temperature threshold corresponding to a plateau in a heat profile of the melt;

wherein the second temperature threshold is greater than the first temperature threshold;

wherein the second temperature threshold is a temperature at or above which an ordered network of nanocarbons forms in the melt.

2. The process of claim 1 , further comprising at least one of (i) energizing the melt with an electrical current and (ii) mixing the melt using a vertical vortex.

3. The process of claim 2 , wherein the energizing includes inserting a pair of electrodes into the melt, said pair of electrodes serving as a current path to the electrical current.

4. The process of claim 2 , wherein the electrical current is at least 200 Amperes.

5. The process of claim 2 , wherein the mixing includes creating the vertical vortex by way of shear mixing.

6. The process of claim 1 , wherein the carbon source is amorphous carbon.

7. The process of claim 1 , further comprising extruding the multi-phase covetic.

8. The process of claim 1 , wherein the metal located in one of group III, IV, or V of the periodic table.

9. The process of claim 1 , wherein the metal is a transition metal.

10. The process of claim 1 , wherein the multi-phase covetic has a property that is enhanced with respect to the same property in one of the metal and the carbon source.

11. The process of claim 10 , wherein the property is thermal conductivity.

12. The process of claim 1 , wherein the metal is aluminum and the first threshold is about 100 degrees Fahrenheit above the metal melt temperature and the second threshold is reached after full carbon addition is achieved, with the hold time being about 5 minutes.

13. The process of claim 1 , wherein the first threshold is about 100 degrees Fahrenheit above the metal melt temperature and the second threshold is reached after full carbon addition is achieved, with the hold time being about 5 minutes.

14. A process for making a composite material, the process comprising:

forming a multi-phase covetic, the forming including:

heating a melt that includes a metal in a molten state and a carbon source to a first temperature threshold to form metal-carbon bonds; and

subsequently heating the melt to a second temperature threshold, the second temperature threshold being greater than the first temperature threshold, wherein the second temperature threshold is a temperature at or above which ordered multi-phase covetic domains form in the melt; and

wherein the metal is aluminum and the first threshold is about 100 degrees Fahrenheit above the metal melt temperature and the second threshold is about a 5-minute hold time after full carbon addition is achieved.

15. The process of claim 14 , further comprising at least one of (i) energizing the melt with an electrical current and (ii) mixing the melt using a vertical vortex.

16. The process of claim 15 , wherein the energizing includes inserting a pair of electrodes into the melt, said pair of electrodes serving as a current path to the electrical current.

17. The process of claim 15 , wherein the electrical current is at least 200 Amperes.

18. The process of claim 14 , wherein the carbon source is amorphous carbon.

19. A process for making a composite material, the process comprising:

forming a multi-phase covetic, the forming including:

heating a melt that includes a metal in a molten state and a carbon source to a first temperature threshold to form metal-carbon bonds; and

subsequently heating the melt to a second temperature threshold, the second temperature threshold being greater than the first temperature threshold, wherein the second temperature threshold is a temperature at or above which ordered multi-phase covetic domains form in the melt; and

wherein the first threshold is about 100 degrees Fahrenheit above the metal melt temperature and the second threshold is about a 5-minute hold time after full carbon addition is achieved.

20. The process of claim 19 , wherein the carbon source is amorphous carbon.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 11, 2017
From: BRAYDICH, MICHAEL DENNIS; COUCH, HARRY; LUEDTKE, LOUIS A
To: GDC INDUSTRIES, LLC
Reel/Frame 041970/0049 →
Continuity (3)
Provisional Application 62321192 · Apr 11, 2016
Provisional Application 62410705 · Oct 20, 2016
Related Publication 20170298476A1 · Oct 19, 2017